IFSS, TG, FT-IR spectra of impregnated sugar palm (Arenga pinnata) fibres and mechanical properties of their composites

This study aimed to investigate the effect of resin impregnation on the interfacial shear strength (IFSS), thermogravimetric (TG) and fourier transform infrared (FT-IR) of sugar palm ( Arenga pinnata ) fibres. In addition, the effect of resin impregnation on the mechanical properties of sugar palm f...

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Veröffentlicht in:Journal of thermal analysis and calorimetry 2013-02, Vol.111 (2), p.1375-1383
Hauptverfasser: Ishak, Mohamad Ridzwan, Leman, Zulkiflle, Salit, Mohd Sapuan, Rahman, Mohd Zaki Abd, Anwar Uyup, Mohd Khairun, Akhtar, Riaz
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container_end_page 1383
container_issue 2
container_start_page 1375
container_title Journal of thermal analysis and calorimetry
container_volume 111
creator Ishak, Mohamad Ridzwan
Leman, Zulkiflle
Salit, Mohd Sapuan
Rahman, Mohd Zaki Abd
Anwar Uyup, Mohd Khairun
Akhtar, Riaz
description This study aimed to investigate the effect of resin impregnation on the interfacial shear strength (IFSS), thermogravimetric (TG) and fourier transform infrared (FT-IR) of sugar palm ( Arenga pinnata ) fibres. In addition, the effect of resin impregnation on the mechanical properties of sugar palm fibre reinforced unsaturated polyester (UP) composites was also studied. The fibres were impregnated with UP via vacuum resin impregnation process at a pressure of 600 mmHg for 5 min. Composites of 10, 20, 30, 40 and 50 % fibre loadings were fabricated and tested for tensile and flexural properties. It was observed that the impregnation process caused the fibres to be enclosed by UP resin and this gave a strong influence to the increase of its interfacial bonding by the increase of its IFSS from single fibre pull-out test. It was also observed with TG and FT-IR spectra that the impregnated fibre had lower moisture uptake than the control and there was no significant increase in thermal stability of the impregnated fibre. The sequence of fibre decomposition started from the evaporation of moisture, hemicelluloses, cellulose, lignin and finally ash content and the presence of these components were proven by FT-IR spectra. For the composite specimens, due to the high interfacial bonding of the impregnated fibre and the matrix, the impregnated composites showed consistently higher tensile strength, tensile modulus, elongation at break, flexural strength, flexural modulus and toughness than the control samples. It was also observed that 30 % fibre loading gave optimum properties.
doi_str_mv 10.1007/s10973-012-2457-5
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In addition, the effect of resin impregnation on the mechanical properties of sugar palm fibre reinforced unsaturated polyester (UP) composites was also studied. The fibres were impregnated with UP via vacuum resin impregnation process at a pressure of 600 mmHg for 5 min. Composites of 10, 20, 30, 40 and 50 % fibre loadings were fabricated and tested for tensile and flexural properties. It was observed that the impregnation process caused the fibres to be enclosed by UP resin and this gave a strong influence to the increase of its interfacial bonding by the increase of its IFSS from single fibre pull-out test. It was also observed with TG and FT-IR spectra that the impregnated fibre had lower moisture uptake than the control and there was no significant increase in thermal stability of the impregnated fibre. The sequence of fibre decomposition started from the evaporation of moisture, hemicelluloses, cellulose, lignin and finally ash content and the presence of these components were proven by FT-IR spectra. For the composite specimens, due to the high interfacial bonding of the impregnated fibre and the matrix, the impregnated composites showed consistently higher tensile strength, tensile modulus, elongation at break, flexural strength, flexural modulus and toughness than the control samples. 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The sequence of fibre decomposition started from the evaporation of moisture, hemicelluloses, cellulose, lignin and finally ash content and the presence of these components were proven by FT-IR spectra. For the composite specimens, due to the high interfacial bonding of the impregnated fibre and the matrix, the impregnated composites showed consistently higher tensile strength, tensile modulus, elongation at break, flexural strength, flexural modulus and toughness than the control samples. 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identifier ISSN: 1388-6150
ispartof Journal of thermal analysis and calorimetry, 2013-02, Vol.111 (2), p.1375-1383
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1588-2926
1572-8943
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subjects Analysis
Analytical Chemistry
Applied sciences
Cellulose
Chemical properties
Chemistry
Chemistry and Materials Science
Composite materials industry
Composites
Exact sciences and technology
Forms of application and semi-finished materials
Inorganic Chemistry
Invisibility
Lignin
Measurement Science and Instrumentation
Mechanical properties
Physical Chemistry
Polymer industry, paints, wood
Polymer Sciences
Technology of polymers
title IFSS, TG, FT-IR spectra of impregnated sugar palm (Arenga pinnata) fibres and mechanical properties of their composites
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