PROCESS FOR PRODUCING PVP-H2O2 PRODUCTS

A process for the production of PVP-H2O2 products in the form of free-flowing powders, or a free-standing, porous solid or foam, is described. To prepare free-flowing powders, a fluidized bed is maintained at a reaction temperature of about room temperature to 60 DEG C and is contacted with finely d...

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Hauptverfasser: BISS, RUSSEL, B, TAYLOR, PAUL, D, COHEN, JEFFREY, M, MERIANOS, JOHN, J
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TAYLOR, PAUL, D
COHEN, JEFFREY, M
MERIANOS, JOHN, J
description A process for the production of PVP-H2O2 products in the form of free-flowing powders, or a free-standing, porous solid or foam, is described. To prepare free-flowing powders, a fluidized bed is maintained at a reaction temperature of about room temperature to 60 DEG C and is contacted with finely divided droplets of a 30 to 85 % by weigth aqueous H2O2 solution. Preferably the fluidized bed temperature is about 35 DEG -45 DEG C, a 5-70 % H2O2 solution is used, and the feed rate of introduction of the H2O2 solution is about 5-50 g/minute/kg PVP present. The PVP-H2O2 product preferably contains about 15-24 %, preferably 18-22 %, H2O2 (1:1 molar ratio) and less than about 5 % water. Procédé de production de produits en PVP-H2O2 sous forme de poudres coulantes ou d'un solide ou une mousse poreux et libre. Pour préparer des poudres coulantes, on maintient un lit fluidisé à une température réactionnelle comprise entre à peu près la température ambiante et 60 °C, puis on le met en contact avec des gouttelettes finement divisées d'une solution aqueuse de H2O2 de 30 à 85 % en poids. De préférence, la température du lit fluidisé est comprise entre environ 35 et 45 °C, on utilise une solution de H2O2 de 5 à 70 %, et l'on introduit la solution de H2O2 à une vitesse d'environ 5 à 50 grammes par minute par kilogramme de PVP. De préférence, le produit en PVP-H2O2 contient environ de 15 à 24 %, et de préférence de 18 à 22 %, de H2O2 (rapport molaire 1:1) et une quantité d'eau inférieure à environ 5 %.
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To prepare free-flowing powders, a fluidized bed is maintained at a reaction temperature of about room temperature to 60 DEG C and is contacted with finely divided droplets of a 30 to 85 % by weigth aqueous H2O2 solution. Preferably the fluidized bed temperature is about 35 DEG -45 DEG C, a 5-70 % H2O2 solution is used, and the feed rate of introduction of the H2O2 solution is about 5-50 g/minute/kg PVP present. The PVP-H2O2 product preferably contains about 15-24 %, preferably 18-22 %, H2O2 (1:1 molar ratio) and less than about 5 % water. Procédé de production de produits en PVP-H2O2 sous forme de poudres coulantes ou d'un solide ou une mousse poreux et libre. Pour préparer des poudres coulantes, on maintient un lit fluidisé à une température réactionnelle comprise entre à peu près la température ambiante et 60 °C, puis on le met en contact avec des gouttelettes finement divisées d'une solution aqueuse de H2O2 de 30 à 85 % en poids. 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To prepare free-flowing powders, a fluidized bed is maintained at a reaction temperature of about room temperature to 60 DEG C and is contacted with finely divided droplets of a 30 to 85 % by weigth aqueous H2O2 solution. Preferably the fluidized bed temperature is about 35 DEG -45 DEG C, a 5-70 % H2O2 solution is used, and the feed rate of introduction of the H2O2 solution is about 5-50 g/minute/kg PVP present. The PVP-H2O2 product preferably contains about 15-24 %, preferably 18-22 %, H2O2 (1:1 molar ratio) and less than about 5 % water. Procédé de production de produits en PVP-H2O2 sous forme de poudres coulantes ou d'un solide ou une mousse poreux et libre. Pour préparer des poudres coulantes, on maintient un lit fluidisé à une température réactionnelle comprise entre à peu près la température ambiante et 60 °C, puis on le met en contact avec des gouttelettes finement divisées d'une solution aqueuse de H2O2 de 30 à 85 % en poids. 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TAYLOR, PAUL, D ; COHEN, JEFFREY, M ; MERIANOS, JOHN, J</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_WO9217158A13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>1992</creationdate><topic>AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G</topic><topic>AGRICULTURE</topic><topic>ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES</topic><topic>ANIMAL HUSBANDRY</topic><topic>BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES</topic><topic>CANDLES</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS BASED THEREON</topic><topic>COMPOSITIONS OF MACROMOLECULAR COMPOUNDS</topic><topic>COMPOUNDS THEREOF</topic><topic>DETERGENT COMPOSITIONS</topic><topic>DETERGENTS</topic><topic>FATTY ACIDS THEREFROM</topic><topic>FISHING</topic><topic>FORESTRY</topic><topic>GENERAL PROCESSES OF COMPOUNDING</topic><topic>HUMAN NECESSITIES</topic><topic>HUNTING</topic><topic>HYGIENE</topic><topic>INORGANIC CHEMISTRY</topic><topic>MEDICAL OR VETERINARY SCIENCE</topic><topic>METALLURGY</topic><topic>NON-METALLIC ELEMENTS</topic><topic>ORGANIC MACROMOLECULAR COMPOUNDS</topic><topic>PEST REPELLANTS OR ATTRACTANTS</topic><topic>PLANT GROWTH REGULATORS</topic><topic>PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES</topic><topic>PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF</topic><topic>RECOVERY OF GLYCEROL</topic><topic>RESIN SOAPS</topic><topic>SOAP OR SOAP-MAKING</topic><topic>SPECIFIC USE OF COSMETICS OR SIMILAR TOILETPREPARATIONS</topic><topic>THEIR PREPARATION OR CHEMICAL WORKING-UP</topic><topic>TRAPPING</topic><topic>USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS</topic><topic>USE OF SINGLE SUBSTANCES AS DETERGENTS</topic><topic>WORKING-UP</topic><toplevel>online_resources</toplevel><creatorcontrib>BISS, RUSSEL, B</creatorcontrib><creatorcontrib>TAYLOR, PAUL, D</creatorcontrib><creatorcontrib>COHEN, JEFFREY, M</creatorcontrib><creatorcontrib>MERIANOS, JOHN, J</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>BISS, RUSSEL, B</au><au>TAYLOR, PAUL, D</au><au>COHEN, JEFFREY, M</au><au>MERIANOS, JOHN, J</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS FOR PRODUCING PVP-H2O2 PRODUCTS</title><date>1992-10-15</date><risdate>1992</risdate><abstract>A process for the production of PVP-H2O2 products in the form of free-flowing powders, or a free-standing, porous solid or foam, is described. To prepare free-flowing powders, a fluidized bed is maintained at a reaction temperature of about room temperature to 60 DEG C and is contacted with finely divided droplets of a 30 to 85 % by weigth aqueous H2O2 solution. Preferably the fluidized bed temperature is about 35 DEG -45 DEG C, a 5-70 % H2O2 solution is used, and the feed rate of introduction of the H2O2 solution is about 5-50 g/minute/kg PVP present. The PVP-H2O2 product preferably contains about 15-24 %, preferably 18-22 %, H2O2 (1:1 molar ratio) and less than about 5 % water. Procédé de production de produits en PVP-H2O2 sous forme de poudres coulantes ou d'un solide ou une mousse poreux et libre. Pour préparer des poudres coulantes, on maintient un lit fluidisé à une température réactionnelle comprise entre à peu près la température ambiante et 60 °C, puis on le met en contact avec des gouttelettes finement divisées d'une solution aqueuse de H2O2 de 30 à 85 % en poids. De préférence, la température du lit fluidisé est comprise entre environ 35 et 45 °C, on utilise une solution de H2O2 de 5 à 70 %, et l'on introduit la solution de H2O2 à une vitesse d'environ 5 à 50 grammes par minute par kilogramme de PVP. De préférence, le produit en PVP-H2O2 contient environ de 15 à 24 %, et de préférence de 18 à 22 %, de H2O2 (rapport molaire 1:1) et une quantité d'eau inférieure à environ 5 %.</abstract><oa>free_for_read</oa></addata></record>
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subjects AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G
AGRICULTURE
ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES
ANIMAL HUSBANDRY
BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
CANDLES
CHEMISTRY
COMPOSITIONS BASED THEREON
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
COMPOUNDS THEREOF
DETERGENT COMPOSITIONS
DETERGENTS
FATTY ACIDS THEREFROM
FISHING
FORESTRY
GENERAL PROCESSES OF COMPOUNDING
HUMAN NECESSITIES
HUNTING
HYGIENE
INORGANIC CHEMISTRY
MEDICAL OR VETERINARY SCIENCE
METALLURGY
NON-METALLIC ELEMENTS
ORGANIC MACROMOLECULAR COMPOUNDS
PEST REPELLANTS OR ATTRACTANTS
PLANT GROWTH REGULATORS
PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF
RECOVERY OF GLYCEROL
RESIN SOAPS
SOAP OR SOAP-MAKING
SPECIFIC USE OF COSMETICS OR SIMILAR TOILETPREPARATIONS
THEIR PREPARATION OR CHEMICAL WORKING-UP
TRAPPING
USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS
USE OF SINGLE SUBSTANCES AS DETERGENTS
WORKING-UP
title PROCESS FOR PRODUCING PVP-H2O2 PRODUCTS
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