A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate
The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent se...
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creator | BAUER, Ralf KLAUBER, Eric George SCHROEDER, Jochen NIEMES, Reinhold FRASSETTO, Timo |
description | The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent selected from alcohols and ketons; b) the addition of water.
La présente invention concerne un procédé de préparation de N-[2-[[[1-(4-chlorophényl)-1H-pyrazol-3-yl]oxy]méthyl]phényl]-N-méthoxycarbamate de méthyle cristallin (I), comprenant a) la mise en réaction d'un composé de formule (II) avec un agent d'alkylation en présence d'une base en présence d'un solvant polaire sélectionné parmi les alcools et les cétones ; b) l'ajout d'eau. |
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La présente invention concerne un procédé de préparation de N-[2-[[[1-(4-chlorophényl)-1H-pyrazol-3-yl]oxy]méthyl]phényl]-N-méthoxycarbamate de méthyle cristallin (I), comprenant a) la mise en réaction d'un composé de formule (II) avec un agent d'alkylation en présence d'une base en présence d'un solvant polaire sélectionné parmi les alcools et les cétones ; b) l'ajout d'eau.</description><language>eng ; fre</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2017</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170216&DB=EPODOC&CC=WO&NR=2017025377A1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20170216&DB=EPODOC&CC=WO&NR=2017025377A1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>BAUER, Ralf</creatorcontrib><creatorcontrib>KLAUBER, Eric George</creatorcontrib><creatorcontrib>SCHROEDER, Jochen</creatorcontrib><creatorcontrib>NIEMES, Reinhold</creatorcontrib><creatorcontrib>FRASSETTO, Timo</creatorcontrib><title>A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate</title><description>The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent selected from alcohols and ketons; b) the addition of water.
La présente invention concerne un procédé de préparation de N-[2-[[[1-(4-chlorophényl)-1H-pyrazol-3-yl]oxy]méthyl]phényl]-N-méthoxycarbamate de méthyle cristallin (I), comprenant a) la mise en réaction d'un composé de formule (II) avec un agent d'alkylation en présence d'une base en présence d'un solvant polaire sélectionné parmi les alcools et les cétones ; b) l'ajout d'eau.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2017</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNi70KwjAUhbs4iPoOARcdLvRH6VxE6VQXwSGEEsOtLdwmISli3HxzK_UBnM7hfN-ZR--CafNAYtYZhd6zxrixo5Wu03emXPCDJOo0sh6HNhCrgKfAOU9gswPVknHGtqgDbSEpwQYnX4Ygg0DCPIOYXmJSBFTwHUagpLvJXg64jGaNJI-rXy6i9el4OZSA1tTorVSocaiv5zRO8jjdZ3leJNl_1gcnFUn8</recordid><startdate>20170216</startdate><enddate>20170216</enddate><creator>BAUER, Ralf</creator><creator>KLAUBER, Eric George</creator><creator>SCHROEDER, Jochen</creator><creator>NIEMES, Reinhold</creator><creator>FRASSETTO, Timo</creator><scope>EVB</scope></search><sort><creationdate>20170216</creationdate><title>A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate</title><author>BAUER, Ralf ; KLAUBER, Eric George ; SCHROEDER, Jochen ; NIEMES, Reinhold ; FRASSETTO, Timo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_WO2017025377A13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; fre</language><creationdate>2017</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>BAUER, Ralf</creatorcontrib><creatorcontrib>KLAUBER, Eric George</creatorcontrib><creatorcontrib>SCHROEDER, Jochen</creatorcontrib><creatorcontrib>NIEMES, Reinhold</creatorcontrib><creatorcontrib>FRASSETTO, Timo</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>BAUER, Ralf</au><au>KLAUBER, Eric George</au><au>SCHROEDER, Jochen</au><au>NIEMES, Reinhold</au><au>FRASSETTO, Timo</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate</title><date>2017-02-16</date><risdate>2017</risdate><abstract>The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent selected from alcohols and ketons; b) the addition of water.
La présente invention concerne un procédé de préparation de N-[2-[[[1-(4-chlorophényl)-1H-pyrazol-3-yl]oxy]méthyl]phényl]-N-méthoxycarbamate de méthyle cristallin (I), comprenant a) la mise en réaction d'un composé de formule (II) avec un agent d'alkylation en présence d'une base en présence d'un solvant polaire sélectionné parmi les alcools et les cétones ; b) l'ajout d'eau.</abstract><oa>free_for_read</oa></addata></record> |
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subjects | CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
title | A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate |
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