A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate

The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent se...

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Hauptverfasser: BAUER, Ralf, KLAUBER, Eric George, SCHROEDER, Jochen, NIEMES, Reinhold, FRASSETTO, Timo
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KLAUBER, Eric George
SCHROEDER, Jochen
NIEMES, Reinhold
FRASSETTO, Timo
description The present invention relates to a process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate (I), comprising a) reacting a compound of formula (II) with an alkylating agent in the presence of a base in the presence of a polar solvent selected from alcohols and ketons; b) the addition of water. La présente invention concerne un procédé de préparation de N-[2-[[[1-(4-chlorophényl)-1H-pyrazol-3-yl]oxy]méthyl]phényl]-N-méthoxycarbamate de méthyle cristallin (I), comprenant a) la mise en réaction d'un composé de formule (II) avec un agent d'alkylation en présence d'une base en présence d'un solvant polaire sélectionné parmi les alcools et les cétones ; b) l'ajout d'eau.
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HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
title A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate
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