PROCESS FOR THE PREPARATION OF 4-METHYL-THIAZOLE-5-CARBALDEHYDE INTERMEDIATE
The present invention provides a process for the preparation of 4-methyl-5-formyl-thiazole of the formula (I), which comprises reducing the thiazole ester of the formula (III) to thiazole alcohol of the formula (IV), using a sodium borohydride in the presence of AlCl3 in a solvent and oxidising the...
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| creator | LUTHRA, PARVEN, KUMAR VYAS, RAJESH KAMMA, RAMAKRISHNA DESHPANDE, PANDURANG, BALWANT |
| description | The present invention provides a process for the preparation of 4-methyl-5-formyl-thiazole of the formula (I), which comprises reducing the thiazole ester of the formula (III) to thiazole alcohol of the formula (IV), using a sodium borohydride in the presence of AlCl3 in a solvent and oxidising the thiazole alcohol of the formula (IV) to obtain 4-methyl-5-formyl-thiazole of the formula (I) using an oxidizing agent.
La présente invention concerne un procédé de préparation de 4-méthyl-5-formylthiazole correspondant à la formule (I), ce procédé comprenant les opérations consistant à réduire l'ester de thiazole de formule (III) en alcool de thiazole de formule (IV), à utiliser un borohydrure de sodium en présence d'AlCl3, dans un solvant, et à oxyder l'alcool de thiazole de formule (IV) pour obtenir le 4-méthyl-5-formyl-thiazole de formule (I), cela à l'aide d'un agent oxydant. |
| format | Patent |
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La présente invention concerne un procédé de préparation de 4-méthyl-5-formylthiazole correspondant à la formule (I), ce procédé comprenant les opérations consistant à réduire l'ester de thiazole de formule (III) en alcool de thiazole de formule (IV), à utiliser un borohydrure de sodium en présence d'AlCl3, dans un solvant, et à oxyder l'alcool de thiazole de formule (IV) pour obtenir le 4-méthyl-5-formyl-thiazole de formule (I), cela à l'aide d'un agent oxydant.</description><edition>7</edition><language>eng ; fre</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2003</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20031106&DB=EPODOC&CC=WO&NR=03091230A1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20031106&DB=EPODOC&CC=WO&NR=03091230A1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LUTHRA, PARVEN, KUMAR</creatorcontrib><creatorcontrib>VYAS, RAJESH</creatorcontrib><creatorcontrib>KAMMA, RAMAKRISHNA</creatorcontrib><creatorcontrib>DESHPANDE, PANDURANG, BALWANT</creatorcontrib><title>PROCESS FOR THE PREPARATION OF 4-METHYL-THIAZOLE-5-CARBALDEHYDE INTERMEDIATE</title><description>The present invention provides a process for the preparation of 4-methyl-5-formyl-thiazole of the formula (I), which comprises reducing the thiazole ester of the formula (III) to thiazole alcohol of the formula (IV), using a sodium borohydride in the presence of AlCl3 in a solvent and oxidising the thiazole alcohol of the formula (IV) to obtain 4-methyl-5-formyl-thiazole of the formula (I) using an oxidizing agent.
La présente invention concerne un procédé de préparation de 4-méthyl-5-formylthiazole correspondant à la formule (I), ce procédé comprenant les opérations consistant à réduire l'ester de thiazole de formule (III) en alcool de thiazole de formule (IV), à utiliser un borohydrure de sodium en présence d'AlCl3, dans un solvant, et à oxyder l'alcool de thiazole de formule (IV) pour obtenir le 4-méthyl-5-formyl-thiazole de formule (I), cela à l'aide d'un agent oxydant.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2003</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNyjEKwjAUANAsDqLeIR4gkBodHL_JDwmkTfj9IHUpReIkWqj3x8UDOL3lrUUqlC32vfSZJAeUhbAAAcfcyezlUbXIYUiKQ4RbTqhOygJdIDkMg0MZO0Zq0UVg3IrVY3oudfdzI_Ye2QZV5_dYl3m611f9jNesjT43B6OhMf-cL6_RLec</recordid><startdate>20031106</startdate><enddate>20031106</enddate><creator>LUTHRA, PARVEN, KUMAR</creator><creator>VYAS, RAJESH</creator><creator>KAMMA, RAMAKRISHNA</creator><creator>DESHPANDE, PANDURANG, BALWANT</creator><scope>EVB</scope></search><sort><creationdate>20031106</creationdate><title>PROCESS FOR THE PREPARATION OF 4-METHYL-THIAZOLE-5-CARBALDEHYDE INTERMEDIATE</title><author>LUTHRA, PARVEN, KUMAR ; VYAS, RAJESH ; KAMMA, RAMAKRISHNA ; DESHPANDE, PANDURANG, BALWANT</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_WO03091230A13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; fre</language><creationdate>2003</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>LUTHRA, PARVEN, KUMAR</creatorcontrib><creatorcontrib>VYAS, RAJESH</creatorcontrib><creatorcontrib>KAMMA, RAMAKRISHNA</creatorcontrib><creatorcontrib>DESHPANDE, PANDURANG, BALWANT</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LUTHRA, PARVEN, KUMAR</au><au>VYAS, RAJESH</au><au>KAMMA, RAMAKRISHNA</au><au>DESHPANDE, PANDURANG, BALWANT</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS FOR THE PREPARATION OF 4-METHYL-THIAZOLE-5-CARBALDEHYDE INTERMEDIATE</title><date>2003-11-06</date><risdate>2003</risdate><abstract>The present invention provides a process for the preparation of 4-methyl-5-formyl-thiazole of the formula (I), which comprises reducing the thiazole ester of the formula (III) to thiazole alcohol of the formula (IV), using a sodium borohydride in the presence of AlCl3 in a solvent and oxidising the thiazole alcohol of the formula (IV) to obtain 4-methyl-5-formyl-thiazole of the formula (I) using an oxidizing agent.
La présente invention concerne un procédé de préparation de 4-méthyl-5-formylthiazole correspondant à la formule (I), ce procédé comprenant les opérations consistant à réduire l'ester de thiazole de formule (III) en alcool de thiazole de formule (IV), à utiliser un borohydrure de sodium en présence d'AlCl3, dans un solvant, et à oxyder l'alcool de thiazole de formule (IV) pour obtenir le 4-méthyl-5-formyl-thiazole de formule (I), cela à l'aide d'un agent oxydant.</abstract><edition>7</edition><oa>free_for_read</oa></addata></record> |
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| subjects | CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
| title | PROCESS FOR THE PREPARATION OF 4-METHYL-THIAZOLE-5-CARBALDEHYDE INTERMEDIATE |
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