Process for the purification of aromatic amines

Aromatic amines which have been obtained by reduction of aromatic nitro compounds are purified by mixing the crude amine obtained after phase separation with an aqueous, alkali metal hydroxide solution and subsequent distillation of this mixture over a distillation column. The distillation column ha...

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Hauptverfasser: SOMMER KNUT, DUEX ANDRE, LEHNER PETER, MAROTZ BENIE, GEHLEN FRANZ-ULRICH
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creator SOMMER KNUT
DUEX ANDRE
LEHNER PETER
MAROTZ BENIE
GEHLEN FRANZ-ULRICH
description Aromatic amines which have been obtained by reduction of aromatic nitro compounds are purified by mixing the crude amine obtained after phase separation with an aqueous, alkali metal hydroxide solution and subsequent distillation of this mixture over a distillation column. The distillation column has at least an upper and a lower rectifying part and a stripping part. The bottom product of the distillation column is partly to completely sluiced out and is partly evaporated in a main evaporator and at least one downstream re-evaporator and partly recycled back into the column.
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title Process for the purification of aromatic amines
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