Process for preparing organically modified aerogels in which the salts formed are precipitated out
The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of
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creator | SCHWERTFEGER FRITZ |
description | The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of |
format | Patent |
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preparation of a silicic acid sol having a pH of <=4.0 from an aqueous water glass solution, with the aid of at least one organic and/or inorganic acid;b) polycondensation of the resulting silicic acid sol to a SiO2 gel by the addition of a base;c) washing the gel obtained in Step b) with an organic solvent until the water content of the gel is <=5% by weight;d) surface-silylating the gel obtained in Step c), ande) drying the surface-silylated gel obtained in Step d), characterized in that at least one acid forms difficultly soluble salts with the cations of the water glass in the silicic acid sol, and that before Step b) the resulting difficultly soluble salts are extensively precipitated and separated from the silicic acid sol.</description><edition>7</edition><language>eng</language><subject>ARTIFICIAL STONE ; CEMENTS ; CERAMICS ; CHEMISTRY ; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS ; COMPOUNDS THEREOF ; CONCRETE ; INORGANIC CHEMISTRY ; LIME, MAGNESIA ; 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out</title><description>The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of <=4.0 from an aqueous water glass solution, with the aid of at least one organic and/or inorganic acid;b) polycondensation of the resulting silicic acid sol to a SiO2 gel by the addition of a base;c) washing the gel obtained in Step b) with an organic solvent until the water content of the gel is <=5% by weight;d) surface-silylating the gel obtained in Step c), ande) drying the surface-silylated gel obtained in Step d), characterized in that at least one acid forms difficultly soluble salts with the cations of the water glass in the silicic acid sol, and that before Step b) the resulting difficultly soluble salts are extensively precipitated and separated from the silicic acid sol.</description><subject>ARTIFICIAL STONE</subject><subject>CEMENTS</subject><subject>CERAMICS</subject><subject>CHEMISTRY</subject><subject>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</subject><subject>COMPOUNDS THEREOF</subject><subject>CONCRETE</subject><subject>INORGANIC CHEMISTRY</subject><subject>LIME, MAGNESIA</subject><subject>METALLURGY</subject><subject>NON-METALLIC ELEMENTS</subject><subject>REFRACTORIES</subject><subject>SLAG</subject><subject>TREATMENT OF NATURAL STONE</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2001</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjEEKAjEMRbtxIeodcgHBKupeUVwK6nqInUwb6DQlrYi31xEP4OrB5_03NveziqNSoBOFrJRROXkQ9ZjYYYwv6KXljqkFJBVPsQAneAZ2AWogKBjr994PitJQcZy5Yv0M8qhTM-owFpr9ODFwPFz3pzllaahkdJSoNrfLZmkX27Xd2dUfyhsM4T4Y</recordid><startdate>20010403</startdate><enddate>20010403</enddate><creator>SCHWERTFEGER FRITZ</creator><scope>EVB</scope></search><sort><creationdate>20010403</creationdate><title>Process for preparing organically modified aerogels in which the salts formed are precipitated out</title><author>SCHWERTFEGER FRITZ</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_US6210751B13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>2001</creationdate><topic>ARTIFICIAL STONE</topic><topic>CEMENTS</topic><topic>CERAMICS</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS</topic><topic>COMPOUNDS THEREOF</topic><topic>CONCRETE</topic><topic>INORGANIC CHEMISTRY</topic><topic>LIME, MAGNESIA</topic><topic>METALLURGY</topic><topic>NON-METALLIC ELEMENTS</topic><topic>REFRACTORIES</topic><topic>SLAG</topic><topic>TREATMENT OF NATURAL STONE</topic><toplevel>online_resources</toplevel><creatorcontrib>SCHWERTFEGER FRITZ</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>SCHWERTFEGER FRITZ</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Process for preparing organically modified aerogels in which the salts formed are precipitated out</title><date>2001-04-03</date><risdate>2001</risdate><abstract>The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of <=4.0 from an aqueous water glass solution, with the aid of at least one organic and/or inorganic acid;b) polycondensation of the resulting silicic acid sol to a SiO2 gel by the addition of a base;c) washing the gel obtained in Step b) with an organic solvent until the water content of the gel is <=5% by weight;d) surface-silylating the gel obtained in Step c), ande) drying the surface-silylated gel obtained in Step d), characterized in that at least one acid forms difficultly soluble salts with the cations of the water glass in the silicic acid sol, and that before Step b) the resulting difficultly soluble salts are extensively precipitated and separated from the silicic acid sol.</abstract><edition>7</edition><oa>free_for_read</oa></addata></record> |
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subjects | ARTIFICIAL STONE CEMENTS CERAMICS CHEMISTRY COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS COMPOUNDS THEREOF CONCRETE INORGANIC CHEMISTRY LIME, MAGNESIA METALLURGY NON-METALLIC ELEMENTS REFRACTORIES SLAG TREATMENT OF NATURAL STONE |
title | Process for preparing organically modified aerogels in which the salts formed are precipitated out |
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