Process for preparing organically modified aerogels in which the salts formed are precipitated out

The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of

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1. Verfasser: SCHWERTFEGER FRITZ
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creator SCHWERTFEGER FRITZ
description The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of
format Patent
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preparation of a silicic acid sol having a pH of &lt;=4.0 from an aqueous water glass solution, with the aid of at least one organic and/or inorganic acid;b) polycondensation of the resulting silicic acid sol to a SiO2 gel by the addition of a base;c) washing the gel obtained in Step b) with an organic solvent until the water content of the gel is &lt;=5% by weight;d) surface-silylating the gel obtained in Step c), ande) drying the surface-silylated gel obtained in Step d), characterized in that at least one acid forms difficultly soluble salts with the cations of the water glass in the silicic acid sol, and that before Step b) the resulting difficultly soluble salts are extensively precipitated and separated from the silicic acid sol.</description><edition>7</edition><language>eng</language><subject>ARTIFICIAL STONE ; CEMENTS ; CERAMICS ; CHEMISTRY ; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS ; COMPOUNDS THEREOF ; CONCRETE ; INORGANIC CHEMISTRY ; LIME, 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which the salts formed are precipitated out</title><description>The present invention relates to a process for the preparation of organically modified aerogels, comprisinga) the preparation of a silicic acid sol having a pH of &lt;=4.0 from an aqueous water glass solution, with the aid of at least one organic and/or inorganic acid;b) polycondensation of the resulting silicic acid sol to a SiO2 gel by the addition of a base;c) washing the gel obtained in Step b) with an organic solvent until the water content of the gel is &lt;=5% by weight;d) surface-silylating the gel obtained in Step c), ande) drying the surface-silylated gel obtained in Step d), characterized in that at least one acid forms difficultly soluble salts with the cations of the water glass in the silicic acid sol, and that before Step b) the resulting difficultly soluble salts are extensively precipitated and separated from the silicic acid sol.</description><subject>ARTIFICIAL 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surface-silylated gel obtained in Step d), characterized in that at least one acid forms difficultly soluble salts with the cations of the water glass in the silicic acid sol, and that before Step b) the resulting difficultly soluble salts are extensively precipitated and separated from the silicic acid sol.</abstract><edition>7</edition><oa>free_for_read</oa></addata></record>
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subjects ARTIFICIAL STONE
CEMENTS
CERAMICS
CHEMISTRY
COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS
COMPOUNDS THEREOF
CONCRETE
INORGANIC CHEMISTRY
LIME, MAGNESIA
METALLURGY
NON-METALLIC ELEMENTS
REFRACTORIES
SLAG
TREATMENT OF NATURAL STONE
title Process for preparing organically modified aerogels in which the salts formed are precipitated out
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