Method for distilling hexamethylcyclotrisiloxane
The invention relates to an improved distillation method wherein hexamethylcyclotrisiloxane is isolated from a crude blend thereof by mixing the crude blend with a hydrocarbon co-solvent having a normal boiling point of 125 DEG C. to 150 DEG C. and distilling the resulting mixture in an apparatus ha...
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creator | VOCI ROCCO JOSEPH GORNOWICZ GERALD ALPHONSE |
description | The invention relates to an improved distillation method wherein hexamethylcyclotrisiloxane is isolated from a crude blend thereof by mixing the crude blend with a hydrocarbon co-solvent having a normal boiling point of 125 DEG C. to 150 DEG C. and distilling the resulting mixture in an apparatus having a reboiler, a fractionating column and a condenser, whereby deposition of solid hexamethylcyclotrisiloxane in the condenser is eliminated. |
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subjects | ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM CHEMISTRY METALLURGY ORGANIC CHEMISTRY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL SEPARATION TRANSPORTING |
title | Method for distilling hexamethylcyclotrisiloxane |
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