Method for distilling hexamethylcyclotrisiloxane

The invention relates to an improved distillation method wherein hexamethylcyclotrisiloxane is isolated from a crude blend thereof by mixing the crude blend with a hydrocarbon co-solvent having a normal boiling point of 125 DEG C. to 150 DEG C. and distilling the resulting mixture in an apparatus ha...

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Hauptverfasser: VOCI, ROCCO JOSEPH, GORNOWICZ, GERALD ALPHONSE
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creator VOCI
ROCCO JOSEPH
GORNOWICZ
GERALD ALPHONSE
description The invention relates to an improved distillation method wherein hexamethylcyclotrisiloxane is isolated from a crude blend thereof by mixing the crude blend with a hydrocarbon co-solvent having a normal boiling point of 125 DEG C. to 150 DEG C. and distilling the resulting mixture in an apparatus having a reboiler, a fractionating column and a condenser, whereby deposition of solid hexamethylcyclotrisiloxane in the condenser is eliminated.
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subjects ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
SEPARATION
TRANSPORTING
title Method for distilling hexamethylcyclotrisiloxane
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