ARC TUBE FOR A DISCHARGE LAMP

A sealing composition is provided for joining ceramic or cermet parts, eg in an arc tube for a discharge lamp. The sealing composition comprises, as starting materials, a mixture of alumina (Al2O3), silica (SiO2) and magnesia (MgO), the mixture comprising in the ranges of from 22% to 24.5% by weight...

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Hauptverfasser: HING, PETER, COXON, GEORGE E, PARKER, KEITH E
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creator HING
PETER
COXON
GEORGE E
PARKER
KEITH E
description A sealing composition is provided for joining ceramic or cermet parts, eg in an arc tube for a discharge lamp. The sealing composition comprises, as starting materials, a mixture of alumina (Al2O3), silica (SiO2) and magnesia (MgO), the mixture comprising in the ranges of from 22% to 24.5% by weight of Al2O3, from 45.5% to 49.5% by weight of SiO2, and from 26.0% to to 32.5% by weight of MgO. The sealing composition contains less than 40% by weight (expressed as the percentage of the total weight of the mixture) of the crystalline phase alpha -Cordierite when subjected to a test procedure comprising the following steps: (i) thoroughly mixing the constituents of the sealing composition and sintering the mixture at 1200C for 10 hours to produce a friable lump which is crushed, transferred to a platinum (10% Rhodium) crucible, and heated in a muffle furnace at 1550C for 2 hours while the glass is in a molten condition; (ii) pouring the contents of the crucible into distilled water to form a brittle frit or cullet and, after drying at 160C, grinding the glass in an Agate Cone Grinder to form a powder of particle size less than 180 mu m; (iii) mixing the powdered glass with 4% by weight of a binder comprising a solution in toluene of methyl/butyl methacrylate, and pressing the mixture in a 16 mm diameter die at 100 MPa to produce 1g samples; (iv) sintering a sample continuously for 6 hours at a sintering tempterature equal to or greater than the temperature a seal made from the sealing composition is intended to withstand; and (v) evaluating, by X-ray Diffractometry, the proportion by weight (expressed as a percentage of the total weight of alumina, silica and magnesia) of the crystalline phase alpha -Cordierite in the samples sintered at the sintering temperature. o
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The sealing composition comprises, as starting materials, a mixture of alumina (Al2O3), silica (SiO2) and magnesia (MgO), the mixture comprising in the ranges of from 22% to 24.5% by weight of Al2O3, from 45.5% to 49.5% by weight of SiO2, and from 26.0% to to 32.5% by weight of MgO. The sealing composition contains less than 40% by weight (expressed as the percentage of the total weight of the mixture) of the crystalline phase alpha -Cordierite when subjected to a test procedure comprising the following steps: (i) thoroughly mixing the constituents of the sealing composition and sintering the mixture at 1200C for 10 hours to produce a friable lump which is crushed, transferred to a platinum (10% Rhodium) crucible, and heated in a muffle furnace at 1550C for 2 hours while the glass is in a molten condition; (ii) pouring the contents of the crucible into distilled water to form a brittle frit or cullet and, after drying at 160C, grinding the glass in an Agate Cone Grinder to form a powder of particle size less than 180 mu m; (iii) mixing the powdered glass with 4% by weight of a binder comprising a solution in toluene of methyl/butyl methacrylate, and pressing the mixture in a 16 mm diameter die at 100 MPa to produce 1g samples; (iv) sintering a sample continuously for 6 hours at a sintering tempterature equal to or greater than the temperature a seal made from the sealing composition is intended to withstand; and (v) evaluating, by X-ray Diffractometry, the proportion by weight (expressed as a percentage of the total weight of alumina, silica and magnesia) of the crystalline phase alpha -Cordierite in the samples sintered at the sintering temperature. o</abstract><oa>free_for_read</oa></addata></record>
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subjects ARTIFICIAL STONE
CEMENTS
CERAMICS
CHEMICAL COMPOSITION OF GLASSES, GLAZES, OR VITREOUSENAMELS
CHEMISTRY
COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS
CONCRETE
GLASS
JOINING GLASS TO GLASS OR OTHER MATERIALS
LIME, MAGNESIA
METALLURGY
MINERAL OR SLAG WOOL
REFRACTORIES
SLAG
SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS,MINERALS OR SLAGS
SURFACE TREATMENT OF GLASS
TREATMENT OF NATURAL STONE
title ARC TUBE FOR A DISCHARGE LAMP
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