Continuous process for the production of organic isocyanates

Organic mono- or poly-isocyanates are produced on a continuous basis by phosgenating the corresponding amines. A solution of the amine to be phosgenated is continuously sprayed through a smooth-jet nozzle into a solution of phosgene continuously flowing through a mixing chamber. The mixing chamber i...

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Hauptverfasser: HENNIG, HANS-JOACHIM, LAHRS, JUERGEN, LIEBSCH, DIETRICH
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creator HENNIG
HANS-JOACHIM
LAHRS
JUERGEN
LIEBSCH
DIETRICH
description Organic mono- or poly-isocyanates are produced on a continuous basis by phosgenating the corresponding amines. A solution of the amine to be phosgenated is continuously sprayed through a smooth-jet nozzle into a solution of phosgene continuously flowing through a mixing chamber. The mixing chamber is maintained at a temperature of 120 DEG to 300 DEG C. and a pressure of from 10 to 1000 bars. The molar ratio of phosgene to primary amino groups is generally from 2:1 to 30:1.
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMPOSITIONS BASED THEREON
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
METALLURGY
ORGANIC CHEMISTRY
ORGANIC MACROMOLECULAR COMPOUNDS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR PREPARATION OR CHEMICAL WORKING-UP
THEIR RELEVANT APPARATUS
TRANSPORTING
title Continuous process for the production of organic isocyanates
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