Synthesis of polyol bis(allyl carbonate) utilizing reagent recovery and recycle

Synthesis of polyol bis(allyl carbonate) utilizing reagent recovery and recycle

Disclosed is an improved method of forming polyol (allyl carbonate) monomers. In the disclosed method, the organic by-products as diallyl carbonate and unreacted reagents as allyl alcohol are separated from the brine and wash water derived aqueous phase and returned to the allyl carbonate synthesis...

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Hauptverfasser: YOUNG, ELGIN E
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ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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ELGIN E
description Disclosed is an improved method of forming polyol (allyl carbonate) monomers. In the disclosed method, the organic by-products as diallyl carbonate and unreacted reagents as allyl alcohol are separated from the brine and wash water derived aqueous phase and returned to the allyl carbonate synthesis reaction. The aqueous phase is further separated to recover allyl alcohol therefrom, which is returned to the allyl carbonate synthesis reactor as an azeotrope.
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CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title Synthesis of polyol bis(allyl carbonate) utilizing reagent recovery and recycle
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