Method of purifying a neon-helium mixture

A method of purifying a neon-helium mixture containing 2 to 7 vol.% of neon, 1 to 3 vol.% of helium, 0.5 to 1.5 vol.% of hydrogen, 88.5 to 96.5 vol.% of nitrogen, traces of oxygen and traces of hydrocarbons having from 1 to 5 carbon atoms by freeing said mixture from nitrogen, oxygen, hydrogen and h...

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Hauptverfasser: IGNATOV, JURY YAKOVLEVICH, GOLOVKO, GEORGY ANATOLIEVICH
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creator IGNATOV
JURY YAKOVLEVICH
GOLOVKO
GEORGY ANATOLIEVICH
description A method of purifying a neon-helium mixture containing 2 to 7 vol.% of neon, 1 to 3 vol.% of helium, 0.5 to 1.5 vol.% of hydrogen, 88.5 to 96.5 vol.% of nitrogen, traces of oxygen and traces of hydrocarbons having from 1 to 5 carbon atoms by freeing said mixture from nitrogen, oxygen, hydrogen and hydrocarbons, which comprises removing nitrogen by dephlegmation at a temperature of from 67 DEG to 77 DEG K. and a pressure of 4 to 7 kgf/sq.cm. to give a mixture containing 68 to 74 vol.% of neon, 22 to 74 vol.% of helium, 1.5 to 2 vol.% of hydrogen, 1 to 8 vol.% of nitrogen and trace amounts of oxygen and hydrocarbons. The latter mixture is passed at a pressure of from 4 to 7 kgf/sq.cm. through microporous adsorbents having 3 to 9-A micropores, adsorbing the remaining nitrogen, oxygen, hydrogen and hydrocarbons. Then said impurities are desorbed by gradually reducing the pressure of the mixture from 4 to 7 kgf/sq.cm. down to 101 to 102 mm Hg. The adsorption and desorption steps are effected with the microporous adsorbents being thermostated with liquid nitrogen.
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The latter mixture is passed at a pressure of from 4 to 7 kgf/sq.cm. through microporous adsorbents having 3 to 9-A micropores, adsorbing the remaining nitrogen, oxygen, hydrogen and hydrocarbons. Then said impurities are desorbed by gradually reducing the pressure of the mixture from 4 to 7 kgf/sq.cm. down to 10&lt;-&gt;1 to 102 mm Hg. 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subjects BLASTING
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMBINED HEATING AND REFRIGERATION SYSTEMS
COMPOUNDS THEREOF
HEAT PUMP SYSTEMS
HEATING
INORGANIC CHEMISTRY
LIGHTING
LIQUEFACTION SOLIDIFICATION OF GASES
LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS
MANUFACTURE OR STORAGE OF ICE
MECHANICAL ENGINEERING
METALLURGY
MIXTURES BY PRESSURE AND COLD TREATMENT
NON-METALLIC ELEMENTS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
REFRIGERATION OR COOLING
SEPARATION
THEIR RELEVANT APPARATUS
TRANSPORTING
WEAPONS
title Method of purifying a neon-helium mixture
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