PROCESS OF MAKING AMORPHOUS HIGHLY DISPERSED GERMANIUM DIOXIDE AND PRODUCT OBTAINED THEREBY
1277592 Germanium dioxide DEUTSCHE GOLDUND SILBER-SCHEIDEANSTALT 4 Sept 1969 [20 Sept 1968] 43879/69 Heading C1A Amorphous highly dispersed germanium dioxide is prepared by reacting a volatile tetravalent germanium compound or a sprayable solution thereof under hydrolysing or oxidizing conditions in...
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creator | DUESING G,DT HECKEL E,DT RENNGARDT F,DT MEYER SIMON E,DT |
description | 1277592 Germanium dioxide DEUTSCHE GOLDUND SILBER-SCHEIDEANSTALT 4 Sept 1969 [20 Sept 1968] 43879/69 Heading C1A Amorphous highly dispersed germanium dioxide is prepared by reacting a volatile tetravalent germanium compound or a sprayable solution thereof under hydrolysing or oxidizing conditions in the gas phase or as an aerosol at a temperature above 1300 C., allowing the germanium dioxide formed to coagulate at a temperature of from 200 to 1000 C., and separating the gaseous reaction products. The germanium compound is preferably a halide or a volatile organo-germanium compound. The reaction is preferably carried out at a temperature of from 1400 to 1700 C. using a fuel gas of high calorific value with a free oxygen containing gas or pure oxygen, the mixture being reacted after passage through a nozzle. The germanium dioxide formed is preferably coagulated and separated at a temperature of from 400 to 700 C. |
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The germanium compound is preferably a halide or a volatile organo-germanium compound. The reaction is preferably carried out at a temperature of from 1400 to 1700 C. using a fuel gas of high calorific value with a free oxygen containing gas or pure oxygen, the mixture being reacted after passage through a nozzle. 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The germanium compound is preferably a halide or a volatile organo-germanium compound. The reaction is preferably carried out at a temperature of from 1400 to 1700 C. using a fuel gas of high calorific value with a free oxygen containing gas or pure oxygen, the mixture being reacted after passage through a nozzle. The germanium dioxide formed is preferably coagulated and separated at a temperature of from 400 to 700 C.</abstract><oa>free_for_read</oa></addata></record> |
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subjects | CHEMISTRY COMPOSITIONS BASED THEREON COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F INORGANIC CHEMISTRY MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS METALLURGY ORGANIC MACROMOLECULAR COMPOUNDS THEIR PREPARATION OR CHEMICAL WORKING-UP |
title | PROCESS OF MAKING AMORPHOUS HIGHLY DISPERSED GERMANIUM DIOXIDE AND PRODUCT OBTAINED THEREBY |
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