Method for preparing lithium bis(fluorosulfonyl)imide salt

Method for preparing lithium bis(fluorosulfonyl)imide salt

The present invention relates to a method for preparing a lithium bis(fluorosulfonyl)imide salt, including a step of dissolving bis(chlorosulfonyl)imide in an organic solvent in a non-glass vessel to prepare a first reaction solution; a step of injecting lithium fluoride (LiF) to the first reaction...

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Hauptverfasser: Lee, Chui Haeng, Lim, Young Min, Lee, Won Jae, Lee, Hyun Jik, Kang, Byung Soo
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Sprache:eng
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CHEMISTRY
COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM,RUBIDIUM, CAESIUM, OR FRANCIUM
INORGANIC CHEMISTRY
METALLURGY
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creator Lee, Chui Haeng
Lim, Young Min
Lee, Won Jae
Lee, Hyun Jik
Kang, Byung Soo
description The present invention relates to a method for preparing a lithium bis(fluorosulfonyl)imide salt, including a step of dissolving bis(chlorosulfonyl)imide in an organic solvent in a non-glass vessel to prepare a first reaction solution; a step of injecting lithium fluoride (LiF) to the first reaction solution in the non-glass vessel and refluxing while heating to prepare a second reaction solution; a step of separating a product including a lithium bis(fluorosulfonyl)imide salt and the organic solvent from the second reaction solution; and a step of obtaining the lithium bis(fluorosulfonyl)imide salt in a solid phase from the product, wherein the organic solvent is at least one or more selected from the group consisting of ethyl acetate, butyl acetate, chloroform, dichloromethane, dichloroethane, benzene, xylene and acetonitrile.
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subjects CHEMISTRY
COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM,RUBIDIUM, CAESIUM, OR FRANCIUM
INORGANIC CHEMISTRY
METALLURGY
title Method for preparing lithium bis(fluorosulfonyl)imide salt
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