METHOD FOR THE SYNTHESIS OF 4-CHLOROFENOXYACETIC ACID

A method for the synthesis of 4-chlorofenoxyacetic acid (4CFOC), which method provides the fusion of chloroacetic acid with 4-chlorophenol with an addition of concentrated solution of alkali, keeping and isolation of acid in the form of sodium slat with subsequent conversion thereof in a free state...

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1. Verfasser: LIASHENKO YEVHEN VOLODYMYROVYCH
Format: Patent
Sprache:eng
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Zusammenfassung:A method for the synthesis of 4-chlorofenoxyacetic acid (4CFOC), which method provides the fusion of chloroacetic acid with 4-chlorophenol with an addition of concentrated solution of alkali, keeping and isolation of acid in the form of sodium slat with subsequent conversion thereof in a free state by mineral acid. Between stages 4CFOC salt precipitation and isolation of acid in the free state, the stage of reprecipitation of salt from water is in addition introduced.