METHOD OF TELLURIUM PURIFICATION FROM IMPURITIES

FIELD: inorganic chemistry, metals. SUBSTANCE: technical tellurium is dissolved in hydrogen peroxide following by boiling of prepared acid at tellurium addition and isolation of purified tellurium by electrolysis. Solution purified by ionic exchange is crystallized before electrolysis, and mother li...

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Hauptverfasser: GERASIMOVA T.A, NIKOLAEVA G.V, ARTEM'EVA N.P, GERASIMOV V.S
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creator GERASIMOVA T.A
NIKOLAEVA G.V
ARTEM'EVA N.P
GERASIMOV V.S
description FIELD: inorganic chemistry, metals. SUBSTANCE: technical tellurium is dissolved in hydrogen peroxide following by boiling of prepared acid at tellurium addition and isolation of purified tellurium by electrolysis. Solution purified by ionic exchange is crystallized before electrolysis, and mother liquor is recovered at dissolving stage. Mother liquor formed by electrolysis is recovered at the stage of potassium tellurate preparing up to the content of potassium tellurate in solution 50-60 g/l. EFFECT: improved method of tellurium purification. 2 dwg Использование: очистка теллура от примесей. Сущность: растворяют технический теллур в перекиси водорода, проводят кипячение полученной кислоты при добавлении теллура и последующее выделение очищенного теллура электролизом раствора теллурата калия, причем очищенный ионным обменом раствор перед электролизом кристаллизуют с возвратом маточника на стадию растворения, а образовавшийся при электролизе маточник возвращают на стадию приготовления раствора теллурата калия до содержания в растворе теллурата калия 50-60 г/л. 2 ил.
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subjects CHEMISTRY
CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS
FERROUS OR NON-FERROUS ALLOYS
GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC
GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS
METALLURGY
PRETREATMENT OF RAW MATERIALS
PRODUCTION AND REFINING OF METALS
TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE
TREATMENT OF ALLOYS OR NON-FERROUS METALS
title METHOD OF TELLURIUM PURIFICATION FROM IMPURITIES
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