METHOD OF PREPARING ZIRCONIUM DIOXIDE NANOPOWDER

FIELD: chemistry. ^ SUBSTANCE: zirconium hydroxide is precipitated and then simultaneously dried and calcined under microwave radiation in the frequency range 50-20000 MHz with continuous power of 3.0-50.0 kW for 5-60 minutes. ^ EFFECT: invention reduces aggregation of zirconium dioxide nanopowder a...

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Hauptverfasser: DMITRIEV MAKSIM SERGEEVICH, KOCHETOVA NINA ANATOL'EVNA, KOLJASKIN ALEKSANDR DAVIDOVICH, PETRUNIN VADIM FEDOROVICH, DIDENKO ANDREJ NIKOLAEVICH, KOROVIN SERGEJ ALEKSANDROVICH, POPOV VIKTOR VLADIMIROVICH
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creator DMITRIEV MAKSIM SERGEEVICH
KOCHETOVA NINA ANATOL'EVNA
KOLJASKIN ALEKSANDR DAVIDOVICH
PETRUNIN VADIM FEDOROVICH
DIDENKO ANDREJ NIKOLAEVICH
KOROVIN SERGEJ ALEKSANDROVICH
POPOV VIKTOR VLADIMIROVICH
description FIELD: chemistry. ^ SUBSTANCE: zirconium hydroxide is precipitated and then simultaneously dried and calcined under microwave radiation in the frequency range 50-20000 MHz with continuous power of 3.0-50.0 kW for 5-60 minutes. ^ EFFECT: invention reduces aggregation of zirconium dioxide nanopowder and increases specific surface area of the powder. ^ 2 dwg, 1 tbl, 4 ex Изобретение может быть использовано при изготовлении керамики, катализаторов, сорбентов. Осаждают гидроксид циркония, затем его сушку и прокаливание проводят одновременно под действием СВЧ-излучения в частотном диапазоне 500-20000 МГц с непрерывной мощностью 3,0-50,0 кВт в течение 5-60 мин. Изобретение позволяет снизить агрегацию нанопорошков диоксида циркония и получать порошки с удельной поверхностью до 39,8 м2/г, 2 ил., 1 табл.
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subjects CHEMISTRY
COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F
INORGANIC CHEMISTRY
MANUFACTURE OR TREATMENT THEREOF
METALLURGY
NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS,MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES ASDISCRETE UNITS
NANOTECHNOLOGY
PERFORMING OPERATIONS
TRANSPORTING
title METHOD OF PREPARING ZIRCONIUM DIOXIDE NANOPOWDER
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