INTEGRATED SERPENTINITE PROCESSING METHOD RESULTING IN PURE SILICA PRODUCTION
FIELD: industrial inorganic synthesis. ^ SUBSTANCE: invention comprises processing of serpentinite to produce following commercial products: pure silica, magnesium compounds, including magnesium chloride, magnesium metal, carnallite, iron- and nickel-containing concentrates. Serpentinite is leached...
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creator | FREJDLINA R.G GULJAKIN A.I TETERIN V.V KOZLOV JU.A KOCHELAEV V.A SHCHELKONOGOV A.A JAKOVLEVA S.A SHIROKOV JU.I SABUROV L.N |
description | FIELD: industrial inorganic synthesis. ^ SUBSTANCE: invention comprises processing of serpentinite to produce following commercial products: pure silica, magnesium compounds, including magnesium chloride, magnesium metal, carnallite, iron- and nickel-containing concentrates. Serpentinite is leached with hydrochloric acid solution containing 10-21% HCl at 60-100 and liquid-to-solids ratio (3-10):1 for 2 to 6 h under discontinuous or continuous countercurrent conditions to yield magnesium chloride solution and silica. The former is purified via two-step neutralization: first with brucite or caustic magnesite at 80-90 to pH 3.5-4.0 and then with sodium hydroxide solution to pH 6-7 including addition of sodium sulfide or hydrosulfide. ^ EFFECT: increased purity of silica product and enlarged number of commercial products and/or semiproducts. ^ 4 cl |
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Serpentinite is leached with hydrochloric acid solution containing 10-21% HCl at 60-100 and liquid-to-solids ratio (3-10):1 for 2 to 6 h under discontinuous or continuous countercurrent conditions to yield magnesium chloride solution and silica. The former is purified via two-step neutralization: first with brucite or caustic magnesite at 80-90 to pH 3.5-4.0 and then with sodium hydroxide solution to pH 6-7 including addition of sodium sulfide or hydrosulfide. ^ EFFECT: increased purity of silica product and enlarged number of commercial products and/or semiproducts. ^ 4 cl</description><edition>7</edition><language>eng ; rus</language><subject>CHEMISTRY ; COMPOUNDS THEREOF ; INORGANIC CHEMISTRY ; METALLURGY ; NON-METALLIC ELEMENTS</subject><creationdate>2004</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20041227&DB=EPODOC&CC=RU&NR=2243154C2$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76516</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20041227&DB=EPODOC&CC=RU&NR=2243154C2$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>FREJDLINA R.G</creatorcontrib><creatorcontrib>GULJAKIN A.I</creatorcontrib><creatorcontrib>TETERIN V.V</creatorcontrib><creatorcontrib>KOZLOV JU.A</creatorcontrib><creatorcontrib>KOCHELAEV V.A</creatorcontrib><creatorcontrib>SHCHELKONOGOV A.A</creatorcontrib><creatorcontrib>JAKOVLEVA S.A</creatorcontrib><creatorcontrib>SHIROKOV JU.I</creatorcontrib><creatorcontrib>SABUROV L.N</creatorcontrib><title>INTEGRATED SERPENTINITE PROCESSING METHOD RESULTING IN PURE SILICA PRODUCTION</title><description>FIELD: industrial inorganic synthesis. ^ SUBSTANCE: invention comprises processing of serpentinite to produce following commercial products: pure silica, magnesium compounds, including magnesium chloride, magnesium metal, carnallite, iron- and nickel-containing concentrates. Serpentinite is leached with hydrochloric acid solution containing 10-21% HCl at 60-100 and liquid-to-solids ratio (3-10):1 for 2 to 6 h under discontinuous or continuous countercurrent conditions to yield magnesium chloride solution and silica. The former is purified via two-step neutralization: first with brucite or caustic magnesite at 80-90 to pH 3.5-4.0 and then with sodium hydroxide solution to pH 6-7 including addition of sodium sulfide or hydrosulfide. ^ EFFECT: increased purity of silica product and enlarged number of commercial products and/or semiproducts. ^ 4 cl</description><subject>CHEMISTRY</subject><subject>COMPOUNDS THEREOF</subject><subject>INORGANIC CHEMISTRY</subject><subject>METALLURGY</subject><subject>NON-METALLIC ELEMENTS</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2004</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNykEKwjAQQNFsXIh6h7mAi6b1ACUZ24F2EiaTdSkSV2IL9f5IwQO4-vB5RzMSK3bSKnpIKBFZiUkRogSHKRF3MKL2wYNgyoPugxhiFoREA7l2pz47pcBnc3jOr61cfj0ZuKO6_lrWZSrbOj_Ku3wmydY2dXVrnK3_IF_aUC57</recordid><startdate>20041227</startdate><enddate>20041227</enddate><creator>FREJDLINA R.G</creator><creator>GULJAKIN A.I</creator><creator>TETERIN V.V</creator><creator>KOZLOV JU.A</creator><creator>KOCHELAEV V.A</creator><creator>SHCHELKONOGOV A.A</creator><creator>JAKOVLEVA S.A</creator><creator>SHIROKOV JU.I</creator><creator>SABUROV L.N</creator><scope>EVB</scope></search><sort><creationdate>20041227</creationdate><title>INTEGRATED SERPENTINITE PROCESSING METHOD RESULTING IN PURE SILICA PRODUCTION</title><author>FREJDLINA R.G ; GULJAKIN A.I ; TETERIN V.V ; KOZLOV JU.A ; KOCHELAEV V.A ; SHCHELKONOGOV A.A ; JAKOVLEVA S.A ; SHIROKOV JU.I ; SABUROV L.N</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_RU2243154C23</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; rus</language><creationdate>2004</creationdate><topic>CHEMISTRY</topic><topic>COMPOUNDS THEREOF</topic><topic>INORGANIC CHEMISTRY</topic><topic>METALLURGY</topic><topic>NON-METALLIC ELEMENTS</topic><toplevel>online_resources</toplevel><creatorcontrib>FREJDLINA R.G</creatorcontrib><creatorcontrib>GULJAKIN A.I</creatorcontrib><creatorcontrib>TETERIN V.V</creatorcontrib><creatorcontrib>KOZLOV JU.A</creatorcontrib><creatorcontrib>KOCHELAEV V.A</creatorcontrib><creatorcontrib>SHCHELKONOGOV A.A</creatorcontrib><creatorcontrib>JAKOVLEVA S.A</creatorcontrib><creatorcontrib>SHIROKOV JU.I</creatorcontrib><creatorcontrib>SABUROV L.N</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>FREJDLINA R.G</au><au>GULJAKIN A.I</au><au>TETERIN V.V</au><au>KOZLOV JU.A</au><au>KOCHELAEV V.A</au><au>SHCHELKONOGOV A.A</au><au>JAKOVLEVA S.A</au><au>SHIROKOV JU.I</au><au>SABUROV L.N</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>INTEGRATED SERPENTINITE PROCESSING METHOD RESULTING IN PURE SILICA PRODUCTION</title><date>2004-12-27</date><risdate>2004</risdate><abstract>FIELD: industrial inorganic synthesis. ^ SUBSTANCE: invention comprises processing of serpentinite to produce following commercial products: pure silica, magnesium compounds, including magnesium chloride, magnesium metal, carnallite, iron- and nickel-containing concentrates. Serpentinite is leached with hydrochloric acid solution containing 10-21% HCl at 60-100 and liquid-to-solids ratio (3-10):1 for 2 to 6 h under discontinuous or continuous countercurrent conditions to yield magnesium chloride solution and silica. The former is purified via two-step neutralization: first with brucite or caustic magnesite at 80-90 to pH 3.5-4.0 and then with sodium hydroxide solution to pH 6-7 including addition of sodium sulfide or hydrosulfide. ^ EFFECT: increased purity of silica product and enlarged number of commercial products and/or semiproducts. ^ 4 cl</abstract><edition>7</edition><oa>free_for_read</oa></addata></record> |
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subjects | CHEMISTRY COMPOUNDS THEREOF INORGANIC CHEMISTRY METALLURGY NON-METALLIC ELEMENTS |
title | INTEGRATED SERPENTINITE PROCESSING METHOD RESULTING IN PURE SILICA PRODUCTION |
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