METHOD FOR PREPARING CYCLOHEXYL NITRATE

FIELD: organic chemistry, chemical technology. ^ SUBSTANCE: invention relates to the improved method for preparing cyclohexyl nitrate. Invention describes a method for preparing cyclohexyl nitrate by treatment of cyclohexanol with nitric acid and acetic anhydride in the presence of additive in the m...

Ausführliche Beschreibung

Gespeichert in:

Bibliographische Detailangaben
Hauptverfasser:	VODOLAZHSKIJ S.V, SOKOLOV B.G, MITIN N.A, UTROBIN N.P, NOVATSKIJ G.N, KOBZEV JU.P
Format:	Patent
Sprache:	eng ; rus
Schlagworte:	ACYCLIC OR CARBOCYCLIC COMPOUNDS CHEMISTRY METALLURGY ORGANIC CHEMISTRY
Online-Zugang:	Volltext bestellen
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	FIELD: organic chemistry, chemical technology. ^ SUBSTANCE: invention relates to the improved method for preparing cyclohexyl nitrate. Invention describes a method for preparing cyclohexyl nitrate by treatment of cyclohexanol with nitric acid and acetic anhydride in the presence of additive in the molar ratio of reagents = 1:(1-1.5):(1-1.5), respectively. For treatment cyclohexanol containing 1-5 wt.-% of cyclohexyl nitrate and/or water is taken and process is carried out with continuous feeding reagents by parallel flows. Method provides enhancing quality of the end product, simplified technology and development of the more safe method for manufacturing. ^ EFFECT: improved preparing method. ^ 1 tbl, 12 ex