METHOD OF PREPARING MIXED CHROMIUM-METAL-CONTAINING LIGNOSULFONATES REAGENTS FOR TREATMENT OF DRILLING MUDS
oil and gas production. SUBSTANCE: in a method of preparing compositionally and qualitatively stable chromium-metal-containing lignosulfonate reagents for efficiently controlling properties of drilling muds, including stage of oxidation of lignosulfonates with chromium(VI) compounds in acidic medium...
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creator | IVANOV V.D RASTEGAEV B.A ARKHIPOV A.I PEN'KOV A.I DUBAKIN A.S KOSHELEV V.N VAKHRUSHEV L.P |
description | oil and gas production. SUBSTANCE: in a method of preparing compositionally and qualitatively stable chromium-metal-containing lignosulfonate reagents for efficiently controlling properties of drilling muds, including stage of oxidation of lignosulfonates with chromium(VI) compounds in acidic medium and interaction of resulting chromium-lignosulfonate with multivalent metal salts followed by alkalinization and drying, after above- mentioned oxidation stage, metal-containing lignosulfonates (products of interaction of multivalent metals with lignosulfonates) are added to reaction mixture. Metal-containing lignosulfonates can be products of interaction of lignosulfonates with aluminum and/or iron salts taken in amount sufficient to achieve Cr/Al, Cr/Fe, or Cr/(Al+Fe) weight ratio in final product 1: (0.05-0.5), preferably 1: (0.05-0.1), summary chromium and aluminum and/or iron content 2.5-3.5%, and Al/Fe weight ratio (0.1- 99.9):(99.9-0.1), preferably (40:60):(60-40). EFFECT: enabled controlled process of acidic polycondensation of lignosulfonates with formaldehyde and cocondensation agent. 6 cl, 3 tbl, 2 ex |
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SUBSTANCE: in a method of preparing compositionally and qualitatively stable chromium-metal-containing lignosulfonate reagents for efficiently controlling properties of drilling muds, including stage of oxidation of lignosulfonates with chromium(VI) compounds in acidic medium and interaction of resulting chromium-lignosulfonate with multivalent metal salts followed by alkalinization and drying, after above- mentioned oxidation stage, metal-containing lignosulfonates (products of interaction of multivalent metals with lignosulfonates) are added to reaction mixture. Metal-containing lignosulfonates can be products of interaction of lignosulfonates with aluminum and/or iron salts taken in amount sufficient to achieve Cr/Al, Cr/Fe, or Cr/(Al+Fe) weight ratio in final product 1: (0.05-0.5), preferably 1: (0.05-0.1), summary chromium and aluminum and/or iron content 2.5-3.5%, and Al/Fe weight ratio (0.1- 99.9):(99.9-0.1), preferably (40:60):(60-40). EFFECT: enabled controlled process of acidic polycondensation of lignosulfonates with formaldehyde and cocondensation agent. 6 cl, 3 tbl, 2 ex</description><edition>7</edition><language>eng</language><subject>ADHESIVES ; CHEMISTRY ; DYES ; MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE ; METALLURGY ; MISCELLANEOUS APPLICATIONS OF MATERIALS ; MISCELLANEOUS COMPOSITIONS ; NATURAL RESINS ; PAINTS ; POLISHES</subject><creationdate>2000</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20000710&DB=EPODOC&CC=RU&NR=2152420C1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,778,883,25547,76298</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20000710&DB=EPODOC&CC=RU&NR=2152420C1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>IVANOV V.D</creatorcontrib><creatorcontrib>RASTEGAEV B.A</creatorcontrib><creatorcontrib>ARKHIPOV A.I</creatorcontrib><creatorcontrib>PEN'KOV A.I</creatorcontrib><creatorcontrib>DUBAKIN A.S</creatorcontrib><creatorcontrib>KOSHELEV V.N</creatorcontrib><creatorcontrib>VAKHRUSHEV L.P</creatorcontrib><title>METHOD OF PREPARING MIXED CHROMIUM-METAL-CONTAINING LIGNOSULFONATES REAGENTS FOR TREATMENT OF DRILLING MUDS</title><description>oil and gas production. SUBSTANCE: in a method of preparing compositionally and qualitatively stable chromium-metal-containing lignosulfonate reagents for efficiently controlling properties of drilling muds, including stage of oxidation of lignosulfonates with chromium(VI) compounds in acidic medium and interaction of resulting chromium-lignosulfonate with multivalent metal salts followed by alkalinization and drying, after above- mentioned oxidation stage, metal-containing lignosulfonates (products of interaction of multivalent metals with lignosulfonates) are added to reaction mixture. Metal-containing lignosulfonates can be products of interaction of lignosulfonates with aluminum and/or iron salts taken in amount sufficient to achieve Cr/Al, Cr/Fe, or Cr/(Al+Fe) weight ratio in final product 1: (0.05-0.5), preferably 1: (0.05-0.1), summary chromium and aluminum and/or iron content 2.5-3.5%, and Al/Fe weight ratio (0.1- 99.9):(99.9-0.1), preferably (40:60):(60-40). 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SUBSTANCE: in a method of preparing compositionally and qualitatively stable chromium-metal-containing lignosulfonate reagents for efficiently controlling properties of drilling muds, including stage of oxidation of lignosulfonates with chromium(VI) compounds in acidic medium and interaction of resulting chromium-lignosulfonate with multivalent metal salts followed by alkalinization and drying, after above- mentioned oxidation stage, metal-containing lignosulfonates (products of interaction of multivalent metals with lignosulfonates) are added to reaction mixture. Metal-containing lignosulfonates can be products of interaction of lignosulfonates with aluminum and/or iron salts taken in amount sufficient to achieve Cr/Al, Cr/Fe, or Cr/(Al+Fe) weight ratio in final product 1: (0.05-0.5), preferably 1: (0.05-0.1), summary chromium and aluminum and/or iron content 2.5-3.5%, and Al/Fe weight ratio (0.1- 99.9):(99.9-0.1), preferably (40:60):(60-40). EFFECT: enabled controlled process of acidic polycondensation of lignosulfonates with formaldehyde and cocondensation agent. 6 cl, 3 tbl, 2 ex</abstract><edition>7</edition><oa>free_for_read</oa></addata></record> |
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subjects | ADHESIVES CHEMISTRY DYES MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE METALLURGY MISCELLANEOUS APPLICATIONS OF MATERIALS MISCELLANEOUS COMPOSITIONS NATURAL RESINS PAINTS POLISHES |
title | METHOD OF PREPARING MIXED CHROMIUM-METAL-CONTAINING LIGNOSULFONATES REAGENTS FOR TREATMENT OF DRILLING MUDS |
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