METHOD OF PREPARING SUBSTITUTED 2-(PHENYLAMINO)-2- IMIDAZOLINES
FIELD: chemical industry. SUBSTANCE: substituted 2-(phenylamino)-2-imidazolines of formula I: wherein R1= R2= Cl and R3= H, CH3, F, are prepared by condensation of anilines with 1-benzoylimidazolidin-2-one in phosphorus oxychloride in the presence of lithium halides or quaternary ammonium bases. Pre...
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creator | NIKOL'SKAJA S.K VITVITSKAJA A.S KARAVAN V.S SHAVVA A.G BELOV V.N BOGDANOV E.G SOKOLOV A.E SHCHEDROVICH K.I KATSNEL'SON E.Z |
description | FIELD: chemical industry. SUBSTANCE: substituted 2-(phenylamino)-2-imidazolines of formula I: wherein R1= R2= Cl and R3= H, CH3, F, are prepared by condensation of anilines with 1-benzoylimidazolidin-2-one in phosphorus oxychloride in the presence of lithium halides or quaternary ammonium bases. Presence of lithium salts reduces reaction time up to 20-24 hours. EFFECT: high quality of the desired compounds. 6 ex |
format | Patent |
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SUBSTANCE: substituted 2-(phenylamino)-2-imidazolines of formula I: wherein R1= R2= Cl and R3= H, CH3, F, are prepared by condensation of anilines with 1-benzoylimidazolidin-2-one in phosphorus oxychloride in the presence of lithium halides or quaternary ammonium bases. Presence of lithium salts reduces reaction time up to 20-24 hours. EFFECT: high quality of the desired compounds. 6 ex</description><edition>6</edition><language>eng ; rus</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; HUMAN NECESSITIES ; HYGIENE ; MEDICAL OR VETERINARY SCIENCE ; METALLURGY ; ORGANIC CHEMISTRY ; PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES</subject><creationdate>1999</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19990620&DB=EPODOC&CC=RU&NR=2131872C1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,777,882,25545,76296</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19990620&DB=EPODOC&CC=RU&NR=2131872C1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>NIKOL'SKAJA S.K</creatorcontrib><creatorcontrib>VITVITSKAJA A.S</creatorcontrib><creatorcontrib>KARAVAN V.S</creatorcontrib><creatorcontrib>SHAVVA A.G</creatorcontrib><creatorcontrib>BELOV V.N</creatorcontrib><creatorcontrib>BOGDANOV E.G</creatorcontrib><creatorcontrib>SOKOLOV A.E</creatorcontrib><creatorcontrib>SHCHEDROVICH K.I</creatorcontrib><creatorcontrib>KATSNEL'SON E.Z</creatorcontrib><title>METHOD OF PREPARING SUBSTITUTED 2-(PHENYLAMINO)-2- IMIDAZOLINES</title><description>FIELD: chemical industry. SUBSTANCE: substituted 2-(phenylamino)-2-imidazolines of formula I: wherein R1= R2= Cl and R3= H, CH3, F, are prepared by condensation of anilines with 1-benzoylimidazolidin-2-one in phosphorus oxychloride in the presence of lithium halides or quaternary ammonium bases. Presence of lithium salts reduces reaction time up to 20-24 hours. 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SUBSTANCE: substituted 2-(phenylamino)-2-imidazolines of formula I: wherein R1= R2= Cl and R3= H, CH3, F, are prepared by condensation of anilines with 1-benzoylimidazolidin-2-one in phosphorus oxychloride in the presence of lithium halides or quaternary ammonium bases. Presence of lithium salts reduces reaction time up to 20-24 hours. EFFECT: high quality of the desired compounds. 6 ex</abstract><edition>6</edition><oa>free_for_read</oa></addata></record> |
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subjects | CHEMISTRY HETEROCYCLIC COMPOUNDS HUMAN NECESSITIES HYGIENE MEDICAL OR VETERINARY SCIENCE METALLURGY ORGANIC CHEMISTRY PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES |
title | METHOD OF PREPARING SUBSTITUTED 2-(PHENYLAMINO)-2- IMIDAZOLINES |
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