PROCESS FOR PREPARING COPPER POWDER

The invention relates to a process for preparing copper powders by atomizing molten metal with high-pressure water and to a copper powder which is used as a starting material for producing filters, sleeves, toothed wheels, bearings, sparking plugs, Cu-graphite composite materials or brake pads for m...

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Hauptverfasser: LUNGU DĂIAN-HORAŢIU, GNANDT FRANCISC, VASIU IOAN RADU
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creator LUNGU DĂIAN-HORAŢIU
GNANDT FRANCISC
VASIU IOAN RADU
description The invention relates to a process for preparing copper powders by atomizing molten metal with high-pressure water and to a copper powder which is used as a starting material for producing filters, sleeves, toothed wheels, bearings, sparking plugs, Cu-graphite composite materials or brake pads for motor vehicles, by sintering or sinter-moulding. The claimed process has the following stages : smelting a charge of copper wastes in an induction furnace, pouring the molten mass with a temperature of 1300°C in a pouring gate provided at its lower part with a nozzle with the diameter of 10 mm having the role of forming a vein of molten metal with the same diameter which flows in the atomizing tower wherein it is disintegrated by the high-pressure water jets of a multi-jet type atomizing system with 12 nozzles, circularly arranged, so that the axis of water jets forms angles of 11° with the vertical of the molten mass axis of flow, the water jet having a diameter of 1 mm and a pressure of 9 MPa, with a flow rate of the atomized water of Q= 0.1 m/min ensured by Woma-type pump, followed by drying the metal particles in an electric furnace at a temperature of 200°C and by granulometric sifting with the retention of particles < 425 μ m, followed by the thermochemical treatment of reduction in dissociated NHat a temperature T= 550°C and grinding the resulting copper sponge in a Chilean mill at a speed of 12 rpm. The claimed Cu powder has the following composition: 0.013...0.01% Si, 0.096...0.12% Fe, 0.025...0.06% Ni, 0.06...0.9% Sn, 0.023...0.3% Zn, 0.043...0.06% Pb, 0.24...0.25% O, 98.3...99.5% Cu, the grain shape is irregular, the granulometric fraction < 212 μ m =70%, the flow rate V=36s/100 g and the apparent density ρ= 4.15 g/cm. Invenţia se referă la un procedeu de obţinere a pulberilor de cupru, prin pulverizarea metalului topit cu apă sub presiune, şi la o pulbere de cupru care este utilizată ca materie primă pentru realizarea, prin sinterizare sau prin sintermatriţare, a filtrelor, bucşelor, roţilor dinţate, lagărelor, bujiilor, materialelor compozite Cu - Grafit sau a plăcuţelor de frână pentru autoturisme. Procedeul conform invenţiei are următoarele etape: elaborarea, într-un cuptor cu inducţie, a unei şarje formate din deşeuri de cupru, turnarea topiturii cu temperatura de 1300°C într-o pâlnie de turnare prevăzută, la partea inferioară, cu o duză cu diametrul de 10 mm, ce are rolul să formeze o vână de metal topit cu acelaşi diametru, care curge în turnul
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fullrecord <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_RO127082A8</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>RO127082A8</sourcerecordid><originalsourceid>FETCH-epo_espacenet_RO127082A83</originalsourceid><addsrcrecordid>eNrjZFAOCPJ3dg0OVnDzD1IICHINcAzy9HNXcPYPCHAFCviHu7gG8TCwpiXmFKfyQmluBnk31xBnD93Ugvz41OKCxOTUvNSS-CB_QyNzAwsjRwtjwioA5ZEiJg</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>PROCESS FOR PREPARING COPPER POWDER</title><source>esp@cenet</source><creator>LUNGU DĂIAN-HORAŢIU ; GNANDT FRANCISC ; VASIU IOAN RADU</creator><creatorcontrib>LUNGU DĂIAN-HORAŢIU ; GNANDT FRANCISC ; VASIU IOAN RADU</creatorcontrib><description>The invention relates to a process for preparing copper powders by atomizing molten metal with high-pressure water and to a copper powder which is used as a starting material for producing filters, sleeves, toothed wheels, bearings, sparking plugs, Cu-graphite composite materials or brake pads for motor vehicles, by sintering or sinter-moulding. The claimed process has the following stages : smelting a charge of copper wastes in an induction furnace, pouring the molten mass with a temperature of 1300°C in a pouring gate provided at its lower part with a nozzle with the diameter of 10 mm having the role of forming a vein of molten metal with the same diameter which flows in the atomizing tower wherein it is disintegrated by the high-pressure water jets of a multi-jet type atomizing system with 12 nozzles, circularly arranged, so that the axis of water jets forms angles of 11° with the vertical of the molten mass axis of flow, the water jet having a diameter of 1 mm and a pressure of 9 MPa, with a flow rate of the atomized water of Q= 0.1 m/min ensured by Woma-type pump, followed by drying the metal particles in an electric furnace at a temperature of 200°C and by granulometric sifting with the retention of particles &lt; 425 μ m, followed by the thermochemical treatment of reduction in dissociated NHat a temperature T= 550°C and grinding the resulting copper sponge in a Chilean mill at a speed of 12 rpm. The claimed Cu powder has the following composition: 0.013...0.01% Si, 0.096...0.12% Fe, 0.025...0.06% Ni, 0.06...0.9% Sn, 0.023...0.3% Zn, 0.043...0.06% Pb, 0.24...0.25% O, 98.3...99.5% Cu, the grain shape is irregular, the granulometric fraction &lt; 212 μ m =70%, the flow rate V=36s/100 g and the apparent density ρ= 4.15 g/cm. Invenţia se referă la un procedeu de obţinere a pulberilor de cupru, prin pulverizarea metalului topit cu apă sub presiune, şi la o pulbere de cupru care este utilizată ca materie primă pentru realizarea, prin sinterizare sau prin sintermatriţare, a filtrelor, bucşelor, roţilor dinţate, lagărelor, bujiilor, materialelor compozite Cu - Grafit sau a plăcuţelor de frână pentru autoturisme. Procedeul conform invenţiei are următoarele etape: elaborarea, într-un cuptor cu inducţie, a unei şarje formate din deşeuri de cupru, turnarea topiturii cu temperatura de 1300°C într-o pâlnie de turnare prevăzută, la partea inferioară, cu o duză cu diametrul de 10 mm, ce are rolul să formeze o vână de metal topit cu acelaşi diametru, care curge în turnul de pulverizare, unde este dezintegrată de jeturile de apă sub presiune ale unui sistem de pulverizare tip multijet cu 12 ajutaje, dispuse circular, astfel încât axa jeturilor de apă să formeze unghiuri de 11° cu verticala axei de curgere a metalului topit, jetul de apă având diametrul de 1 mm şi o presiune de 9 MPa, cu un debit al apei pulverizate de Q= 0,1 m/min, asigurat de o pompă tip Woma; urmează uscarea particulelor de metal într-un cuptor electric, la 200°C, şi sitarea granulometrică, cu reţinerea particulelor &lt; 425 μ m, urmată de tratamentul termochimic de reducere în NHdisociat, la T = 550°C, şi măcinarea buretelui de Cu rezultat în mori chiliene, la turaţia de 12 rot/min. Pulberea de Cu, conform invenţiei, are următoarea compoziţie chimică: 0,013...0,01% Si, 0,096...0,12% Fe, 0,025...0,06% Ni, 0,06...0,9% Sn, 0,023...0,3% Zn, 0,043...0,06% Pb, 0,24...0,25% O, 98,3...99,5% Cu, forma granulelor neregulată, fracţia granulometrică &lt; 212 μ m = 70%, viteza de curgere V= 36 s/100g şi densitatea aparentă rho= 4,15 g/cm.</description><language>eng ; rum</language><subject>CASTING ; CASTING OF METALS ; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES ; MAKING METALLIC POWDER ; MANUFACTURE OF ARTICLES FROM METALLIC POWDER ; PERFORMING OPERATIONS ; POWDER METALLURGY ; TRANSPORTING ; WORKING METALLIC POWDER</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20150730&amp;DB=EPODOC&amp;CC=RO&amp;NR=127082A8$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76290</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20150730&amp;DB=EPODOC&amp;CC=RO&amp;NR=127082A8$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LUNGU DĂIAN-HORAŢIU</creatorcontrib><creatorcontrib>GNANDT FRANCISC</creatorcontrib><creatorcontrib>VASIU IOAN RADU</creatorcontrib><title>PROCESS FOR PREPARING COPPER POWDER</title><description>The invention relates to a process for preparing copper powders by atomizing molten metal with high-pressure water and to a copper powder which is used as a starting material for producing filters, sleeves, toothed wheels, bearings, sparking plugs, Cu-graphite composite materials or brake pads for motor vehicles, by sintering or sinter-moulding. The claimed process has the following stages : smelting a charge of copper wastes in an induction furnace, pouring the molten mass with a temperature of 1300°C in a pouring gate provided at its lower part with a nozzle with the diameter of 10 mm having the role of forming a vein of molten metal with the same diameter which flows in the atomizing tower wherein it is disintegrated by the high-pressure water jets of a multi-jet type atomizing system with 12 nozzles, circularly arranged, so that the axis of water jets forms angles of 11° with the vertical of the molten mass axis of flow, the water jet having a diameter of 1 mm and a pressure of 9 MPa, with a flow rate of the atomized water of Q= 0.1 m/min ensured by Woma-type pump, followed by drying the metal particles in an electric furnace at a temperature of 200°C and by granulometric sifting with the retention of particles &lt; 425 μ m, followed by the thermochemical treatment of reduction in dissociated NHat a temperature T= 550°C and grinding the resulting copper sponge in a Chilean mill at a speed of 12 rpm. The claimed Cu powder has the following composition: 0.013...0.01% Si, 0.096...0.12% Fe, 0.025...0.06% Ni, 0.06...0.9% Sn, 0.023...0.3% Zn, 0.043...0.06% Pb, 0.24...0.25% O, 98.3...99.5% Cu, the grain shape is irregular, the granulometric fraction &lt; 212 μ m =70%, the flow rate V=36s/100 g and the apparent density ρ= 4.15 g/cm. Invenţia se referă la un procedeu de obţinere a pulberilor de cupru, prin pulverizarea metalului topit cu apă sub presiune, şi la o pulbere de cupru care este utilizată ca materie primă pentru realizarea, prin sinterizare sau prin sintermatriţare, a filtrelor, bucşelor, roţilor dinţate, lagărelor, bujiilor, materialelor compozite Cu - Grafit sau a plăcuţelor de frână pentru autoturisme. Procedeul conform invenţiei are următoarele etape: elaborarea, într-un cuptor cu inducţie, a unei şarje formate din deşeuri de cupru, turnarea topiturii cu temperatura de 1300°C într-o pâlnie de turnare prevăzută, la partea inferioară, cu o duză cu diametrul de 10 mm, ce are rolul să formeze o vână de metal topit cu acelaşi diametru, care curge în turnul de pulverizare, unde este dezintegrată de jeturile de apă sub presiune ale unui sistem de pulverizare tip multijet cu 12 ajutaje, dispuse circular, astfel încât axa jeturilor de apă să formeze unghiuri de 11° cu verticala axei de curgere a metalului topit, jetul de apă având diametrul de 1 mm şi o presiune de 9 MPa, cu un debit al apei pulverizate de Q= 0,1 m/min, asigurat de o pompă tip Woma; urmează uscarea particulelor de metal într-un cuptor electric, la 200°C, şi sitarea granulometrică, cu reţinerea particulelor &lt; 425 μ m, urmată de tratamentul termochimic de reducere în NHdisociat, la T = 550°C, şi măcinarea buretelui de Cu rezultat în mori chiliene, la turaţia de 12 rot/min. Pulberea de Cu, conform invenţiei, are următoarea compoziţie chimică: 0,013...0,01% Si, 0,096...0,12% Fe, 0,025...0,06% Ni, 0,06...0,9% Sn, 0,023...0,3% Zn, 0,043...0,06% Pb, 0,24...0,25% O, 98,3...99,5% Cu, forma granulelor neregulată, fracţia granulometrică &lt; 212 μ m = 70%, viteza de curgere V= 36 s/100g şi densitatea aparentă rho= 4,15 g/cm.</description><subject>CASTING</subject><subject>CASTING OF METALS</subject><subject>CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES</subject><subject>MAKING METALLIC POWDER</subject><subject>MANUFACTURE OF ARTICLES FROM METALLIC POWDER</subject><subject>PERFORMING OPERATIONS</subject><subject>POWDER METALLURGY</subject><subject>TRANSPORTING</subject><subject>WORKING METALLIC POWDER</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZFAOCPJ3dg0OVnDzD1IICHINcAzy9HNXcPYPCHAFCviHu7gG8TCwpiXmFKfyQmluBnk31xBnD93Ugvz41OKCxOTUvNSS-CB_QyNzAwsjRwtjwioA5ZEiJg</recordid><startdate>20150730</startdate><enddate>20150730</enddate><creator>LUNGU DĂIAN-HORAŢIU</creator><creator>GNANDT FRANCISC</creator><creator>VASIU IOAN RADU</creator><scope>EVB</scope></search><sort><creationdate>20150730</creationdate><title>PROCESS FOR PREPARING COPPER POWDER</title><author>LUNGU DĂIAN-HORAŢIU ; GNANDT FRANCISC ; VASIU IOAN RADU</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_RO127082A83</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; rum</language><creationdate>2015</creationdate><topic>CASTING</topic><topic>CASTING OF METALS</topic><topic>CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES</topic><topic>MAKING METALLIC POWDER</topic><topic>MANUFACTURE OF ARTICLES FROM METALLIC POWDER</topic><topic>PERFORMING OPERATIONS</topic><topic>POWDER METALLURGY</topic><topic>TRANSPORTING</topic><topic>WORKING METALLIC POWDER</topic><toplevel>online_resources</toplevel><creatorcontrib>LUNGU DĂIAN-HORAŢIU</creatorcontrib><creatorcontrib>GNANDT FRANCISC</creatorcontrib><creatorcontrib>VASIU IOAN RADU</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LUNGU DĂIAN-HORAŢIU</au><au>GNANDT FRANCISC</au><au>VASIU IOAN RADU</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS FOR PREPARING COPPER POWDER</title><date>2015-07-30</date><risdate>2015</risdate><abstract>The invention relates to a process for preparing copper powders by atomizing molten metal with high-pressure water and to a copper powder which is used as a starting material for producing filters, sleeves, toothed wheels, bearings, sparking plugs, Cu-graphite composite materials or brake pads for motor vehicles, by sintering or sinter-moulding. The claimed process has the following stages : smelting a charge of copper wastes in an induction furnace, pouring the molten mass with a temperature of 1300°C in a pouring gate provided at its lower part with a nozzle with the diameter of 10 mm having the role of forming a vein of molten metal with the same diameter which flows in the atomizing tower wherein it is disintegrated by the high-pressure water jets of a multi-jet type atomizing system with 12 nozzles, circularly arranged, so that the axis of water jets forms angles of 11° with the vertical of the molten mass axis of flow, the water jet having a diameter of 1 mm and a pressure of 9 MPa, with a flow rate of the atomized water of Q= 0.1 m/min ensured by Woma-type pump, followed by drying the metal particles in an electric furnace at a temperature of 200°C and by granulometric sifting with the retention of particles &lt; 425 μ m, followed by the thermochemical treatment of reduction in dissociated NHat a temperature T= 550°C and grinding the resulting copper sponge in a Chilean mill at a speed of 12 rpm. The claimed Cu powder has the following composition: 0.013...0.01% Si, 0.096...0.12% Fe, 0.025...0.06% Ni, 0.06...0.9% Sn, 0.023...0.3% Zn, 0.043...0.06% Pb, 0.24...0.25% O, 98.3...99.5% Cu, the grain shape is irregular, the granulometric fraction &lt; 212 μ m =70%, the flow rate V=36s/100 g and the apparent density ρ= 4.15 g/cm. Invenţia se referă la un procedeu de obţinere a pulberilor de cupru, prin pulverizarea metalului topit cu apă sub presiune, şi la o pulbere de cupru care este utilizată ca materie primă pentru realizarea, prin sinterizare sau prin sintermatriţare, a filtrelor, bucşelor, roţilor dinţate, lagărelor, bujiilor, materialelor compozite Cu - Grafit sau a plăcuţelor de frână pentru autoturisme. Procedeul conform invenţiei are următoarele etape: elaborarea, într-un cuptor cu inducţie, a unei şarje formate din deşeuri de cupru, turnarea topiturii cu temperatura de 1300°C într-o pâlnie de turnare prevăzută, la partea inferioară, cu o duză cu diametrul de 10 mm, ce are rolul să formeze o vână de metal topit cu acelaşi diametru, care curge în turnul de pulverizare, unde este dezintegrată de jeturile de apă sub presiune ale unui sistem de pulverizare tip multijet cu 12 ajutaje, dispuse circular, astfel încât axa jeturilor de apă să formeze unghiuri de 11° cu verticala axei de curgere a metalului topit, jetul de apă având diametrul de 1 mm şi o presiune de 9 MPa, cu un debit al apei pulverizate de Q= 0,1 m/min, asigurat de o pompă tip Woma; urmează uscarea particulelor de metal într-un cuptor electric, la 200°C, şi sitarea granulometrică, cu reţinerea particulelor &lt; 425 μ m, urmată de tratamentul termochimic de reducere în NHdisociat, la T = 550°C, şi măcinarea buretelui de Cu rezultat în mori chiliene, la turaţia de 12 rot/min. Pulberea de Cu, conform invenţiei, are următoarea compoziţie chimică: 0,013...0,01% Si, 0,096...0,12% Fe, 0,025...0,06% Ni, 0,06...0,9% Sn, 0,023...0,3% Zn, 0,043...0,06% Pb, 0,24...0,25% O, 98,3...99,5% Cu, forma granulelor neregulată, fracţia granulometrică &lt; 212 μ m = 70%, viteza de curgere V= 36 s/100g şi densitatea aparentă rho= 4,15 g/cm.</abstract><oa>free_for_read</oa></addata></record>
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subjects CASTING
CASTING OF METALS
CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
MAKING METALLIC POWDER
MANUFACTURE OF ARTICLES FROM METALLIC POWDER
PERFORMING OPERATIONS
POWDER METALLURGY
TRANSPORTING
WORKING METALLIC POWDER
title PROCESS FOR PREPARING COPPER POWDER
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