PROCESS FOR THE SYNTHESIS OF A KNOWN TETRAZOL DERIVATIVE

A Process is disclosed for preparing a compound of the Formula (I)which comprises the steps of:(a) detritylating a compound of the Formula (III)with 0.1 to 1 equivalent of potassium hydroxide in a C1 to C4 straight chain alcohol solvent to obtain a reaction mixture containing the compound of the For...

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Hauptverfasser: FARKAS JENONE, HEGEDUS ISTVAN, FISCHER JANOS, WERKNE PAPP EVA, DEUTSCHNE JUHASZ IDA, BALLO ILDIKO, PETENYL ENDRENE, KREIDL JANOS, CZIBULA LASZLO, NAGYNE BAGDY JUDIT, NEMES ANDRAS
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creator FARKAS JENONE
HEGEDUS ISTVAN
FISCHER JANOS
WERKNE PAPP EVA
DEUTSCHNE JUHASZ IDA
BALLO ILDIKO
PETENYL ENDRENE
KREIDL JANOS
CZIBULA LASZLO
NAGYNE BAGDY JUDIT
NEMES ANDRAS
description A Process is disclosed for preparing a compound of the Formula (I)which comprises the steps of:(a) detritylating a compound of the Formula (III)with 0.1 to 1 equivalent of potassium hydroxide in a C1 to C4 straight chain alcohol solvent to obtain a reaction mixture containing the compound of the Formula (I),(b) changing the C1 to C4 straight chain alcohol solvent in the reaction mixture to an aprotic solvent or a weakly protic solvent, and(c) following step (b) crystallizing out the compound of the Formula (I) from the reaction mixture.
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subjects CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
title PROCESS FOR THE SYNTHESIS OF A KNOWN TETRAZOL DERIVATIVE
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