Fremgangsmåte ved fremstilling av en cellulose-opplösning

For producing solutions of cellulose in water-containing tertiary amine oxides from a suspension of cellulose in an aqueous solution of the tertiary amine oxide by supplying heat under reduced pressure, the suspension having a viscosity between 50 and 15,000 Pas.sec, measured in a relative system, i...

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Hauptverfasser: FIRGO, HEINRICH, WOLSCHNER, BERND, JURKOVIC, RAIMUND, ZIKELI, STEFAN, EICHINGER, DIETER
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creator FIRGO, HEINRICH
WOLSCHNER, BERND
JURKOVIC, RAIMUND
ZIKELI, STEFAN
EICHINGER, DIETER
description For producing solutions of cellulose in water-containing tertiary amine oxides from a suspension of cellulose in an aqueous solution of the tertiary amine oxide by supplying heat under reduced pressure, the suspension having a viscosity between 50 and 15,000 Pas.sec, measured in a relative system, is spread as a layer or film over a heating surface and transported until a homogeneous solution of the cellulose is formed, the feeding of the suspension and the take-off of the homogeneous solution being carried out continuously. These solutions can be produced in an indirectly heated vessel which is provided with a stirring device and can be evacuated and which is designed as a cylindrical container (2) with a centrally mounted stirrer shaft (7) and stirrer blades (8) attached thereto, the radial distance (13) of the stirrer blades (8) from the inside wall (1) of the container (2) being at most 20 mm, and an inlet (11) for the cellulose suspension being provided in the upper part of the container and an outlet (12) for the homogeneous cellulose solution being provided at the lower end.
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subjects AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G
APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBONFILAMENTS
CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS,THREADS, FIBRES, BRISTLES OR RIBBONS
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMPOSITIONS BASED THEREON
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
DERIVATIVES THEREOF
GENERAL PROCESSES OF COMPOUNDING
MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OFARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES ORRIBBONS
METALLURGY
MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
NATURAL OR ARTIFICIAL THREADS OR FIBRES
ORGANIC MACROMOLECULAR COMPOUNDS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
POLYSACCHARIDES
SPINNING
TEXTILES
THEIR PREPARATION OR CHEMICAL WORKING-UP
THEIR RELEVANT APPARATUS
TRANSPORTING
WORKING-UP
title Fremgangsmåte ved fremstilling av en cellulose-opplösning
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