FREMGANGSMAATE FOR FREMSTILLING AV 3,3`-AZO-BIS-(6-HYDROKSYBENZOSYRE)

A method of preparing 3,3'-azo-bis-(6-hydroxy benzoic acid) of formula I I and salts thereof in at least 98% purity for treating inflammatory intestinal diseases. According to the invention a compound II II is diazotized, and the diazonium salt obtained is coupled with a compound III III The fo...

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Hauptverfasser: AGBACK, KARL HUBERT, NYGREN, ALF SIGURD
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creator AGBACK, KARL HUBERT
NYGREN, ALF SIGURD
description A method of preparing 3,3'-azo-bis-(6-hydroxy benzoic acid) of formula I I and salts thereof in at least 98% purity for treating inflammatory intestinal diseases. According to the invention a compound II II is diazotized, and the diazonium salt obtained is coupled with a compound III III The formed intermediate IV, which is also comprised by the invention, IV is hydrolized in alkaline medium to form the compound I. R1, R2 and R3 signify lower alkyl, R2 also possibly substituted phenyl.
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According to the invention a compound II II is diazotized, and the diazonium salt obtained is coupled with a compound III III The formed intermediate IV, which is also comprised by the invention, IV is hydrolized in alkaline medium to form the compound I. 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According to the invention a compound II II is diazotized, and the diazonium salt obtained is coupled with a compound III III The formed intermediate IV, which is also comprised by the invention, IV is hydrolized in alkaline medium to form the compound I. R1, R2 and R3 signify lower alkyl, R2 also possibly substituted phenyl.</abstract><edition>4</edition><oa>free_for_read</oa></addata></record>
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
ADHESIVES
CHEMISTRY
DYES
HUMAN NECESSITIES
HYGIENE
LAKES
MEDICAL OR VETERINARY SCIENCE
METALLURGY
MISCELLANEOUS APPLICATIONS OF MATERIALS
MISCELLANEOUS COMPOSITIONS
MORDANTS
NATURAL RESINS
ORGANIC CHEMISTRY
ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES
PAINTS
POLISHES
PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS ORMEDICINAL PREPARATIONS
title FREMGANGSMAATE FOR FREMSTILLING AV 3,3`-AZO-BIS-(6-HYDROKSYBENZOSYRE)
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