METHOD FOR PRODUCING FATTY ACID LOWER ALKYL ESTER

A METHOD FOR PRODUCING LOWER ALKYL ESTERS OF FATTY ACIDS FROM A MATERIAL CONTAINING AN ANIMAL OR VEGETABLE FAT AND OIL, THE METHOD INCLUDING AN ESTERIFICATION STEP (A) IN WHICH FATTY ACIDS IN THE MATERIAL ARE ESTERIFIED WITH A LOWER ALKYL ALCOHOL USING A CATION EXCHANGE RESIN TO OBTAIN A REACTION MI...

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Hauptverfasser: MATSUO TAKAYUKI, TANAKA YOSHIRO, IZUMI JIRO
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creator MATSUO TAKAYUKI
TANAKA YOSHIRO
IZUMI JIRO
description A METHOD FOR PRODUCING LOWER ALKYL ESTERS OF FATTY ACIDS FROM A MATERIAL CONTAINING AN ANIMAL OR VEGETABLE FAT AND OIL, THE METHOD INCLUDING AN ESTERIFICATION STEP (A) IN WHICH FATTY ACIDS IN THE MATERIAL ARE ESTERIFIED WITH A LOWER ALKYL ALCOHOL USING A CATION EXCHANGE RESIN TO OBTAIN A REACTION MIXTURE CONTAINING AN ESTER-MIXED OIL HAVING AN ACID VALUE OF 2 OR LESS; A TRANSESTERIFICATION STEP (B) WHICH INCLUDES AT LEAST A FIRST INTERMEDIATE STEP TO TRANSESTERIFY A FAT AND OIL IN THE ESTER-MIXED OIL WITH A LOWER ALKYL ALCOHOL WHILE ADJUSTING AN AMOUNT OF AN ALKALINE CATALYST WITHIN A RANGE OF 0.1 TO 1 PARTS BY MASS RELATIVE TO 100 PARTS BY MASS OF THE ESTER-MIXED OIL BASED ON THE ACID VALUE; A DISTILLATION STEP (C) IN WHICH A DISTILLATE THAT CONTAINS A GROUP OF LOWER ALKYL ESTERS OF FATTY ACIDS HAVING A SMALLER NUMBER OF CARBON ATOMS IS REMOVED BY DISTILLATION FROM AN OIL PHASE OBTAINED IN THE TRANSESTERIFICATION STEP (B), THEREBY RETAINING A RESIDUE THAT CONTAINS A GROUP OF LOWER ALKYL ESTERS OF FATTY ACIDS HAVING A LARGER NUMBER OF CARBON ATOMS; AND A FRACTIONAL DISTILLATION STEP (D) WHICH INCLUDES AT LEAST A STEP TO SEPARATE A GROUP OF LOWER ALKYL ESTERS OF FATTY ACIDS HAVING A LARGER NUMBER OF CARBON ATOMS CONTAINED IN THE RESIDUE INTO DIFFERENT FRACTIONS BASED ON THE NUMBER OF THEIR CARBON ATOMS BY DISTILLATION. (FIG. 1)
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subjects ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES
CANDLES
CHEMISTRY
DETERGENTS
ESSENTIAL OILS
FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS,OILS, OR FATTY ACIDS OBTAINED THEREFROM
FATTY ACIDS FROM FATS, OILS OR WAXES
FATTY ACIDS THEREFROM
METALLURGY
PERFUMES
PRODUCING (PRESSING, EXTRACTION), REFINING AND PRESERVINGFATS, FATTY SUBSTANCES (e.g. LANOLIN), FATTY OILS AND WAXES,INCLUDING EXTRACTION FROM WASTE MATERIALS
title METHOD FOR PRODUCING FATTY ACID LOWER ALKYL ESTER
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