UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO
A process for purifying caprolactame by continuous and/or discontinuous (or batch) vacuum distillation comprises a first stage fast vacuum distillation of the raw caprolactame possibly in the presence of an alkaline and/or alkaline-earth hydroxide, a second stage consisting of a vacuum rectification...
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creator | DOMENICO ASTARITA PAOLO SENNY |
description | A process for purifying caprolactame by continuous and/or discontinuous (or batch) vacuum distillation comprises a first stage fast vacuum distillation of the raw caprolactame possibly in the presence of an alkaline and/or alkaline-earth hydroxide, a second stage consisting of a vacuum rectification distillation of the caprolactame obtained in the first stage and a third stage consisting of the fast vacuum distillation of the caprolactame yielded from the second stage, in the presence of an alkaline and/or alkaline-earth hydroxide. The hydroxide amount in the third and possibly the first stage distillation as well varies from 0.05 to 5% preferably from 0.1% to 1%. |
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The hydroxide amount in the third and possibly the first stage distillation as well varies from 0.05 to 5% preferably from 0.1% to 1%.</description><edition>3</edition><language>spa</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>1985</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19850619&DB=EPODOC&CC=MX&NR=152276A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19850619&DB=EPODOC&CC=MX&NR=152276A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>DOMENICO ASTARITA</creatorcontrib><creatorcontrib>PAOLO SENNY</creatorcontrib><title>UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO</title><description>A process for purifying caprolactame by continuous and/or discontinuous (or batch) vacuum distillation comprises a first stage fast vacuum distillation of the raw caprolactame possibly in the presence of an alkaline and/or alkaline-earth hydroxide, a second stage consisting of a vacuum rectification distillation of the caprolactame obtained in the first stage and a third stage consisting of the fast vacuum distillation of the caprolactame yielded from the second stage, in the presence of an alkaline and/or alkaline-earth hydroxide. The hydroxide amount in the third and possibly the first stage distillation as well varies from 0.05 to 5% preferably from 0.1% to 1%.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>1985</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqFyr0KwjAUxfEsDqK-gtwXcLCizofkFq80H6SpuJUicRIt1PfHCO5O58_hN1dt5yhEr9mIFXbJk-WzjzCeAiIodFFq0YikUVwDnWBRkBG4xGS4TVJe8Y7Q0OVbSzW7D48pr367UOuakz5t8vjq8zQOt_zM795et_uqOh6w-ws-7qMutg</recordid><startdate>19850619</startdate><enddate>19850619</enddate><creator>DOMENICO ASTARITA</creator><creator>PAOLO SENNY</creator><scope>EVB</scope></search><sort><creationdate>19850619</creationdate><title>UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO</title><author>DOMENICO ASTARITA ; PAOLO SENNY</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_MX152276A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>spa</language><creationdate>1985</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>DOMENICO ASTARITA</creatorcontrib><creatorcontrib>PAOLO SENNY</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>DOMENICO ASTARITA</au><au>PAOLO SENNY</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO</title><date>1985-06-19</date><risdate>1985</risdate><abstract>A process for purifying caprolactame by continuous and/or discontinuous (or batch) vacuum distillation comprises a first stage fast vacuum distillation of the raw caprolactame possibly in the presence of an alkaline and/or alkaline-earth hydroxide, a second stage consisting of a vacuum rectification distillation of the caprolactame obtained in the first stage and a third stage consisting of the fast vacuum distillation of the caprolactame yielded from the second stage, in the presence of an alkaline and/or alkaline-earth hydroxide. 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subjects | CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
title | UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO |
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