UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO

A process for purifying caprolactame by continuous and/or discontinuous (or batch) vacuum distillation comprises a first stage fast vacuum distillation of the raw caprolactame possibly in the presence of an alkaline and/or alkaline-earth hydroxide, a second stage consisting of a vacuum rectification...

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Hauptverfasser: DOMENICO ASTARITA, PAOLO SENNY
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creator DOMENICO ASTARITA
PAOLO SENNY
description A process for purifying caprolactame by continuous and/or discontinuous (or batch) vacuum distillation comprises a first stage fast vacuum distillation of the raw caprolactame possibly in the presence of an alkaline and/or alkaline-earth hydroxide, a second stage consisting of a vacuum rectification distillation of the caprolactame obtained in the first stage and a third stage consisting of the fast vacuum distillation of the caprolactame yielded from the second stage, in the presence of an alkaline and/or alkaline-earth hydroxide. The hydroxide amount in the third and possibly the first stage distillation as well varies from 0.05 to 5% preferably from 0.1% to 1%.
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subjects CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
title UN PROCEDIMIENTO MEJORADO PARA PURIFICAR CAPROLACTAMA MEDIANTE DESTILACION AL VACIO
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