METHOD OF TREATING NICKELAINING ETCHING WASTE FLUID

A method of regenerating an etching waste fluid, includes the steps of (a) dissolving HC l gas in an etching waste fluid at a temperature falling within a range of 20 DEG C to 50 DEG C and crystallizing NiC l 2 and FeC l 2 crystals, the etching waste fluid containing NiC l 2, FeC l 3, and FeC l 2 an...

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Hauptverfasser: KURIHARA, TOSHIAKI, AKIYOSHI, EIICHI, HIRABAYASHI, TERUHIKO, MAEGAWA, RYOICHI, IMAGARE, YOSHIYUKI
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Sprache:eng ; kor
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creator KURIHARA, TOSHIAKI
AKIYOSHI, EIICHI
HIRABAYASHI, TERUHIKO
MAEGAWA, RYOICHI
IMAGARE, YOSHIYUKI
description A method of regenerating an etching waste fluid, includes the steps of (a) dissolving HC l gas in an etching waste fluid at a temperature falling within a range of 20 DEG C to 50 DEG C and crystallizing NiC l 2 and FeC l 2 crystals, the etching waste fluid containing NiC l 2, FeC l 3, and FeC l 2 and being obtained by etching Ni or an Ni alloy with an etching solution consisting of an aqueous solution containing FeC l 3, (b) distilling a mother liquor at the atmospheric pressure upon crystallization to reduce the HC l concentration in the mother liquor, and (c) distilling, at a reduced pressure, a condensate obtained upon distillation at the atmospheric pressure to further reduce the HC l concentration, thereby obtaining an aqueous solution containing FeC l 3, or bringing the condensate obtained by distillation at the atmospheric pressure into contact with an iron oxide to cause HC l in the condensate to react with the iron oxide to further reduce the HC l concentration in the condensate, thereby obtaining the aqueous solution containing FeC l 3.
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subjects CHEMICAL SURFACE TREATMENT
CHEMISTRY
COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATIONOR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
COATING MATERIAL WITH METALLIC MATERIAL
COATING METALLIC MATERIAL
COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F
DIFFUSION TREATMENT OF METALLIC MATERIAL
INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION INGENERAL
INORGANIC CHEMISTRY
METALLURGY
MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLICMATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASSC23 AND AT LEAST ONEPROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE
title METHOD OF TREATING NICKELAINING ETCHING WASTE FLUID
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