1-(N--1-데옥시-베타-D-글루코피라누론산유도체의 제조 방법

본 발명은, (i) 메탄올을 사용한 화학식 I의 조 화합물의 가용화 단계, 이어서 물을 사용한 침전 단계, 및 (ii) 30℃ 이하의 온도하에 건조 단계를 포함하는, 화학식 I의 조 화합물의 단리 단계를 포함하는, 화학식 I의 조 화합물의 정제 공정에 관한 것이다: [화학식 I] JPEGpct00043.jpg5086 본원에서는 화학식 I의 화합물을 제조하는 제조 공정이 추가로 제공된다. The present invention relates to a process of purification of a crude compound of...

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Hauptverfasser: ROSE SEBASTIEN, MAGUEUR GUILLAUME, DENIS JEROME
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creator ROSE SEBASTIEN
MAGUEUR GUILLAUME
DENIS JEROME
description 본 발명은, (i) 메탄올을 사용한 화학식 I의 조 화합물의 가용화 단계, 이어서 물을 사용한 침전 단계, 및 (ii) 30℃ 이하의 온도하에 건조 단계를 포함하는, 화학식 I의 조 화합물의 단리 단계를 포함하는, 화학식 I의 조 화합물의 정제 공정에 관한 것이다: [화학식 I] JPEGpct00043.jpg5086 본원에서는 화학식 I의 화합물을 제조하는 제조 공정이 추가로 제공된다. The present invention relates to a process of purification of a crude compound of formula (I)wherein it comprises an isolation step of said crude compound of formula (I) including: (i) a solubilization step of said crude compound of formula (I) with methanol followed by a precipitation step with water, and (ii) a drying step under a temperature inferior or equal to 30°C.Herein is further provided a m manufacturing process for preparing a compound of formula (I).
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The present invention relates to a process of purification of a crude compound of formula (I)wherein it comprises an isolation step of said crude compound of formula (I) including: (i) a solubilization step of said crude compound of formula (I) with methanol followed by a precipitation step with water, and (ii) a drying step under a temperature inferior or equal to 30°C.Herein is further provided a m manufacturing process for preparing a compound of formula (I).</abstract><oa>free_for_read</oa></addata></record>
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subjects CHEMISTRY
DERIVATIVES THEREOF
HUMAN NECESSITIES
HYGIENE
MEDICAL OR VETERINARY SCIENCE
METALLURGY
NUCLEIC ACIDS
NUCLEOSIDES
NUCLEOTIDES
ORGANIC CHEMISTRY
PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
SUGARS
title 1-(N--1-데옥시-베타-D-글루코피라누론산유도체의 제조 방법
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