PROCESS FOR PREPARING 1,2-BENZISOTHIAZOLIN-3-ONES

소듐 설파이드 하이드레이트는 N-메틸 2-피롤리돈과 가열함으로써 적어도 부분적으로 탈수된다. 2-클로로벤즈아마이드는 혼합물에 첨가되어, 추가로 가열된다. 혼합물은 냉각되고 수성 과산화수소로 처리되어 우수한 수율로 1,2-벤조이소티아졸린-3-온의 소듐 염을 제공한다. 원하는 경우 산성화가 유리 1,2-벤조이소티아졸린-3-온의 증가를 제공한다....

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Hauptverfasser: BERG CARSTEN, SINGH SANGITA, MARSH IAN ROGER
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creator BERG CARSTEN
SINGH SANGITA
MARSH IAN ROGER
description 소듐 설파이드 하이드레이트는 N-메틸 2-피롤리돈과 가열함으로써 적어도 부분적으로 탈수된다. 2-클로로벤즈아마이드는 혼합물에 첨가되어, 추가로 가열된다. 혼합물은 냉각되고 수성 과산화수소로 처리되어 우수한 수율로 1,2-벤조이소티아졸린-3-온의 소듐 염을 제공한다. 원하는 경우 산성화가 유리 1,2-벤조이소티아졸린-3-온의 증가를 제공한다.
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subjects AGRICULTURE
ANIMAL HUSBANDRY
BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES
CHEMISTRY
FISHING
FORESTRY
HETEROCYCLIC COMPOUNDS
HUMAN NECESSITIES
HUNTING
METALLURGY
ORGANIC CHEMISTRY
PEST REPELLANTS OR ATTRACTANTS
PLANT GROWTH REGULATORS
PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF
TRAPPING
title PROCESS FOR PREPARING 1,2-BENZISOTHIAZOLIN-3-ONES
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