REACTOR AND AGITATOR USEFUL IN A PROCESS FOR MAKING 1-CHLORO-3,3,3-TRIFLUOROPROPENE

본 발명에서는, 1,1,1,3,3-펜타클로로프로판(240fa)과 HF의 반응으로부터 1-클로로-3,3,3-트리플루오로프로펜(1233zd)을 제조하기 위한 고압 공정에서 유용한 반응기 및 교반기로서, 상기 교반기는 하기 디자인 개선점: (a) 불활성 배리어 유체(barrier fluid)를 갖는 이중 메카니칼 시일(seal) 또는 단일 시일; (b) 시일의 회전 면(rotating face) 상의 세라믹; (c) 시일의 고정 면(static face) 상의 세라믹; (d) PTFE 웨지(wedge) 또는 동적 O-링(o-ring) 디...

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description 본 발명에서는, 1,1,1,3,3-펜타클로로프로판(240fa)과 HF의 반응으로부터 1-클로로-3,3,3-트리플루오로프로펜(1233zd)을 제조하기 위한 고압 공정에서 유용한 반응기 및 교반기로서, 상기 교반기는 하기 디자인 개선점: (a) 불활성 배리어 유체(barrier fluid)를 갖는 이중 메카니칼 시일(seal) 또는 단일 시일; (b) 시일의 회전 면(rotating face) 상의 세라믹; (c) 시일의 고정 면(static face) 상의 세라믹; (d) PTFE 웨지(wedge) 또는 동적 O-링(o-ring) 디자인 및 스프링 보강(spring-energized) 테플론으로 제작된 습윤 O-링; 및 (e) 내부식성 합금으로 제작된, 교반기의 습윤 금속 표면 중 하나 이상을 포함하는 것인 반응기 및 교반기가 개시되어 있다. Disclosed is a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.
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Disclosed is a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.</description><language>eng ; kor</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS ; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC ; GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS ; METALLURGY ; MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING ; ORGANIC CHEMISTRY ; PERFORMING OPERATIONS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS ; TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE ; THEIR RELEVANT APPARATUS ; TRANSPORTING</subject><creationdate>2015</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20150513&amp;DB=EPODOC&amp;CC=KR&amp;NR=20150052077A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20150513&amp;DB=EPODOC&amp;CC=KR&amp;NR=20150052077A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>COTTRELL STEPHEN A</creatorcontrib><title>REACTOR AND AGITATOR USEFUL IN A PROCESS FOR MAKING 1-CHLORO-3,3,3-TRIFLUOROPROPENE</title><description>본 발명에서는, 1,1,1,3,3-펜타클로로프로판(240fa)과 HF의 반응으로부터 1-클로로-3,3,3-트리플루오로프로펜(1233zd)을 제조하기 위한 고압 공정에서 유용한 반응기 및 교반기로서, 상기 교반기는 하기 디자인 개선점: (a) 불활성 배리어 유체(barrier fluid)를 갖는 이중 메카니칼 시일(seal) 또는 단일 시일; (b) 시일의 회전 면(rotating face) 상의 세라믹; (c) 시일의 고정 면(static face) 상의 세라믹; (d) PTFE 웨지(wedge) 또는 동적 O-링(o-ring) 디자인 및 스프링 보강(spring-energized) 테플론으로 제작된 습윤 O-링; 및 (e) 내부식성 합금으로 제작된, 교반기의 습윤 금속 표면 중 하나 이상을 포함하는 것인 반응기 및 교반기가 개시되어 있다. Disclosed is a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</subject><subject>CHEMISTRY</subject><subject>CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS</subject><subject>GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC</subject><subject>GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS</subject><subject>METALLURGY</subject><subject>MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING</subject><subject>ORGANIC CHEMISTRY</subject><subject>PERFORMING OPERATIONS</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS</subject><subject>TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE</subject><subject>THEIR RELEVANT APPARATUS</subject><subject>TRANSPORTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2015</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZAgOcnV0DvEPUnD0c1FwdPcMcQRxQoNd3UJ9FDz9FBwVAoL8nV2DgxXcgOK-jt6efu4KhrrOHj7-Qf66xjpAqBsS5OnmEwrkA5UGuPq58jCwpiXmFKfyQmluBmU31xBnD93Ugvz41OKCxOTUvNSSeO8gIwNDUwMDUyMDc3NHY-JUAQBvEjAm</recordid><startdate>20150513</startdate><enddate>20150513</enddate><creator>COTTRELL STEPHEN A</creator><scope>EVB</scope></search><sort><creationdate>20150513</creationdate><title>REACTOR AND AGITATOR USEFUL IN A PROCESS FOR MAKING 1-CHLORO-3,3,3-TRIFLUOROPROPENE</title><author>COTTRELL STEPHEN A</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_KR20150052077A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; kor</language><creationdate>2015</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</topic><topic>CHEMISTRY</topic><topic>CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS</topic><topic>GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC</topic><topic>GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS</topic><topic>METALLURGY</topic><topic>MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING</topic><topic>ORGANIC CHEMISTRY</topic><topic>PERFORMING OPERATIONS</topic><topic>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</topic><topic>TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS</topic><topic>TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE</topic><topic>THEIR RELEVANT APPARATUS</topic><topic>TRANSPORTING</topic><toplevel>online_resources</toplevel><creatorcontrib>COTTRELL STEPHEN A</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>COTTRELL STEPHEN A</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>REACTOR AND AGITATOR USEFUL IN A PROCESS FOR MAKING 1-CHLORO-3,3,3-TRIFLUOROPROPENE</title><date>2015-05-13</date><risdate>2015</risdate><abstract>본 발명에서는, 1,1,1,3,3-펜타클로로프로판(240fa)과 HF의 반응으로부터 1-클로로-3,3,3-트리플루오로프로펜(1233zd)을 제조하기 위한 고압 공정에서 유용한 반응기 및 교반기로서, 상기 교반기는 하기 디자인 개선점: (a) 불활성 배리어 유체(barrier fluid)를 갖는 이중 메카니칼 시일(seal) 또는 단일 시일; (b) 시일의 회전 면(rotating face) 상의 세라믹; (c) 시일의 고정 면(static face) 상의 세라믹; (d) PTFE 웨지(wedge) 또는 동적 O-링(o-ring) 디자인 및 스프링 보강(spring-energized) 테플론으로 제작된 습윤 O-링; 및 (e) 내부식성 합금으로 제작된, 교반기의 습윤 금속 표면 중 하나 이상을 포함하는 것인 반응기 및 교반기가 개시되어 있다. Disclosed is a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal; (b) ceramics on the rotating faces of the seal; (c) ceramics on the static faces of seal; (d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and (e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.</abstract><oa>free_for_read</oa></addata></record>
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language eng ; kor
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION ORPROCESSING OF GOODS
GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC
GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS
METALLURGY
MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINSTCLIMATE CHANGE
THEIR RELEVANT APPARATUS
TRANSPORTING
title REACTOR AND AGITATOR USEFUL IN A PROCESS FOR MAKING 1-CHLORO-3,3,3-TRIFLUOROPROPENE
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