PRODUCTION OF MULTIPLE OXIDE POWDER FOR SOFT FERRITE FROM WASTE PLATING LIQUID

PROBLEM TO BE SOLVED: To provide a production method of a multiple oxide powder for a soft ferrite from a plating waste liq. as a source recycling method of a Fe and a Zn in a high concn. Fe-Zn based plating waste liq. SOLUTION: This method is composed of a stage in which a free sulfuric acid in the...

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Hauptverfasser: MURATA SHIRO, ICHINOSEKI TETSUNORI, MORI TOSHIO, HASHIMOTO KENJI, UJIIE SHINICHI, SETO YASUSHI
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creator MURATA SHIRO
ICHINOSEKI TETSUNORI
MORI TOSHIO
HASHIMOTO KENJI
UJIIE SHINICHI
SETO YASUSHI
description PROBLEM TO BE SOLVED: To provide a production method of a multiple oxide powder for a soft ferrite from a plating waste liq. as a source recycling method of a Fe and a Zn in a high concn. Fe-Zn based plating waste liq. SOLUTION: This method is composed of a stage in which a free sulfuric acid in the Fe-Zn based plating waste liq., is neutralized, and the liq. is further neutralized with an iron powder or an alkali agent to pH3-6 to insolubilize impurity such as Al, Cr, Si, P and heavy metal and the impurity is removed by filtration and separation, the stage in which one or >=2 kinds sulfide crystal or sulfide aq. soln. of Zn, Mn, Ni, Cu and Co are blended to this soln. so as to obtain a composition of a ferrite, then, water content is evaporated to obtain a metal sulfide mixed crystal, the stage in which this metal sulfide mixed crystal is heat-treated at a temp. range of 850-1,000 deg.C and the stage in which the powder obtained by the heat-treatment is washed to remove a sulfuric group or Mg, Ca and Na and the powder is dried.
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subjects CHEMISTRY
COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F
INORGANIC CHEMISTRY
METALLURGY
TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
title PRODUCTION OF MULTIPLE OXIDE POWDER FOR SOFT FERRITE FROM WASTE PLATING LIQUID
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