JPH0631271B
PURPOSE:To obtain the titled compound useful as a raw material for producing silicone oil, etc., in high yield, by reacting an aryl compound with a dihalosilane in the presence of a Lewis acid catalyst and subjecting the reaction product to distillation separation process in the presence of a specif...
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| creator | IMURA TOMOHITO MOMOSE HIROO |
| description | PURPOSE:To obtain the titled compound useful as a raw material for producing silicone oil, etc., in high yield, by reacting an aryl compound with a dihalosilane in the presence of a Lewis acid catalyst and subjecting the reaction product to distillation separation process in the presence of a specific Lewis base compound. CONSTITUTION:An aryl compound (preferably chlorobenzene, etc.) is made to react with a dihalosilane (preferably dichlorosilen) in the presence of a Lewis acid catalyst (preferably boron brichloride, etc.) preferably at 130-300 deg.C. The objective compound can be separated from the reaction product by distilling the product preferably at 50-300 deg.C under atmospheric pressure -10Torr in the presence of the Lewis base compound having acid-base interaction with metallic atom in the above Lewis acid catalyst and having N atom, P atom and/or S atom (preferably a P-containing compound such as methylphosphine). |
| format | Patent |
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CONSTITUTION:An aryl compound (preferably chlorobenzene, etc.) is made to react with a dihalosilane (preferably dichlorosilen) in the presence of a Lewis acid catalyst (preferably boron brichloride, etc.) preferably at 130-300 deg.C. The objective compound can be separated from the reaction product by distilling the product preferably at 50-300 deg.C under atmospheric pressure -10<-2>Torr in the presence of the Lewis base compound having acid-base interaction with metallic atom in the above Lewis acid catalyst and having N atom, P atom and/or S atom (preferably a P-containing compound such as methylphosphine).</description><edition>5</edition><language>eng</language><subject>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM ; APPARATUS THEREFOR ; CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; GENERAL METHODS OF ORGANIC CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY ; PERFORMING OPERATIONS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; THEIR RELEVANT APPARATUS ; TRANSPORTING</subject><creationdate>1994</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19940427&DB=EPODOC&CC=JP&NR=H0631271B2$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,777,882,25545,76296</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19940427&DB=EPODOC&CC=JP&NR=H0631271B2$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>IMURA TOMOHITO</creatorcontrib><creatorcontrib>MOMOSE HIROO</creatorcontrib><title>JPH0631271B</title><description>PURPOSE:To obtain the titled compound useful as a raw material for producing silicone oil, etc., in high yield, by reacting an aryl compound with a dihalosilane in the presence of a Lewis acid catalyst and subjecting the reaction product to distillation separation process in the presence of a specific Lewis base compound. CONSTITUTION:An aryl compound (preferably chlorobenzene, etc.) is made to react with a dihalosilane (preferably dichlorosilen) in the presence of a Lewis acid catalyst (preferably boron brichloride, etc.) preferably at 130-300 deg.C. The objective compound can be separated from the reaction product by distilling the product preferably at 50-300 deg.C under atmospheric pressure -10<-2>Torr in the presence of the Lewis base compound having acid-base interaction with metallic atom in the above Lewis acid catalyst and having N atom, P atom and/or S atom (preferably a P-containing compound such as methylphosphine).</description><subject>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM</subject><subject>APPARATUS THEREFOR</subject><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</subject><subject>CHEMISTRY</subject><subject>GENERAL METHODS OF ORGANIC CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><subject>PERFORMING OPERATIONS</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>THEIR RELEVANT APPARATUS</subject><subject>TRANSPORTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>1994</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZOD2CvAwMDM2NDI3dOJhYE1LzClO5YXS3AxKbq4hzh66qQX58anFBYnJqXmpJfFIOpyMjIlSBAB3yBww</recordid><startdate>19940427</startdate><enddate>19940427</enddate><creator>IMURA TOMOHITO</creator><creator>MOMOSE HIROO</creator><scope>EVB</scope></search><sort><creationdate>19940427</creationdate><title>JPH0631271B</title><author>IMURA TOMOHITO ; MOMOSE HIROO</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_JPH0631271BB23</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>1994</creationdate><topic>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM</topic><topic>APPARATUS THEREFOR</topic><topic>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</topic><topic>CHEMISTRY</topic><topic>GENERAL METHODS OF ORGANIC CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><topic>PERFORMING OPERATIONS</topic><topic>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</topic><topic>THEIR RELEVANT APPARATUS</topic><topic>TRANSPORTING</topic><toplevel>online_resources</toplevel><creatorcontrib>IMURA TOMOHITO</creatorcontrib><creatorcontrib>MOMOSE HIROO</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>IMURA TOMOHITO</au><au>MOMOSE HIROO</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>JPH0631271B</title><date>1994-04-27</date><risdate>1994</risdate><abstract>PURPOSE:To obtain the titled compound useful as a raw material for producing silicone oil, etc., in high yield, by reacting an aryl compound with a dihalosilane in the presence of a Lewis acid catalyst and subjecting the reaction product to distillation separation process in the presence of a specific Lewis base compound. CONSTITUTION:An aryl compound (preferably chlorobenzene, etc.) is made to react with a dihalosilane (preferably dichlorosilen) in the presence of a Lewis acid catalyst (preferably boron brichloride, etc.) preferably at 130-300 deg.C. The objective compound can be separated from the reaction product by distilling the product preferably at 50-300 deg.C under atmospheric pressure -10<-2>Torr in the presence of the Lewis base compound having acid-base interaction with metallic atom in the above Lewis acid catalyst and having N atom, P atom and/or S atom (preferably a P-containing compound such as methylphosphine).</abstract><edition>5</edition><oa>free_for_read</oa></addata></record> |
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| subjects | ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM APPARATUS THEREFOR CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY GENERAL METHODS OF ORGANIC CHEMISTRY METALLURGY ORGANIC CHEMISTRY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL THEIR RELEVANT APPARATUS TRANSPORTING |
| title | JPH0631271B |
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