PROCESS FOR PRODUCING SOLID POLYURETHANE CURING AGENTS

To provide a process for producing a solid, internally and externally blocked polyurethane curing agent based on a (cyclo)aliphatic polyisocyanate.SOLUTION: The present invention relates, in which, in the sequence of steps a) to d), a) i) at least one internally blocked (cyclo)aliphatic polyisocyana...

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Hauptverfasser: ELKE GOLLAN, ANDREA HENSCHKE, NICOLE FRESMANN, JESSIKA SCHUELLER, SPYROU EMMANOUIL DR
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creator ELKE GOLLAN
ANDREA HENSCHKE
NICOLE FRESMANN
JESSIKA SCHUELLER
SPYROU EMMANOUIL DR
description To provide a process for producing a solid, internally and externally blocked polyurethane curing agent based on a (cyclo)aliphatic polyisocyanate.SOLUTION: The present invention relates, in which, in the sequence of steps a) to d), a) i) at least one internally blocked (cyclo)aliphatic polyisocyanate and ii) at least one lactam and/or at least one aliphatic alcohol are dissolved in a solvent to produce a reaction mixture, b) the reaction mixture is heated and reacted, c) the reacted reaction mixture is cooled until product precipitates, and d) liquid solvent and any unreacted dissolved starting materials and precipitated product are mechanically separated from one another.SELECTED DRAWING: None 【課題】(環状)脂肪族ポリイソシアネートをベースとする、内部および外部ブロックされた固体のポリウレタン硬化剤を製造する方法。【解決手段】以下のステップa)~d)の順序で、a)i)少なくとも1種の、内部ブロックされた(環状)脂肪族ポリイソシアネートおよびii)少なくとも1種のラクタムおよび/または少なくとも1種の脂肪族アルコールを、溶媒中に溶解させて、反応混合物を生成させ、b)前記反応混合物を、加熱および反応させ、c)反応させた反応混合物を、生成物が沈殿するまで冷却し、かつd)液状の溶媒、任意に未反応の溶解した出発物質、および沈殿した生成物を、互いに機械的に分離する。【選択図】なし
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subjects CHEMISTRY
COMPOSITIONS BASED THEREON
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
METALLURGY
ORGANIC MACROMOLECULAR COMPOUNDS
THEIR PREPARATION OR CHEMICAL WORKING-UP
title PROCESS FOR PRODUCING SOLID POLYURETHANE CURING AGENTS
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