METHOD FOR REFINING TAR ACID SODA AND TAR ACID SODA REFINING DEVICE

PROBLEM TO BE SOLVED: To provide a method for refining tar acid soda by a light oil cleaning method, reducing the amount of the tar acid soda not recovered as the tar acid soda.SOLUTION: Provided is a method for refining tar acid soda comprising a cleaning separation step where crude tar acid soda i...

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Hauptverfasser: HIRAISHI HARUYOSHI, ARAKI YUTAKA
Format: Patent
Sprache:eng ; jpn
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Zusammenfassung:PROBLEM TO BE SOLVED: To provide a method for refining tar acid soda by a light oil cleaning method, reducing the amount of the tar acid soda not recovered as the tar acid soda.SOLUTION: Provided is a method for refining tar acid soda comprising a cleaning separation step where crude tar acid soda is contacted with light oil to extract oily impurities in the crude tar acid soda into the light oil, thus a mixture of the crude tar acid soda and the light oil is separated into a liquid including the light oil and impurities and the tar acid soda. Further, the method includes: an oil-water separation step where the liquid including the light oil and impurities obtained in the cleaning separation step is subjected to oi-water separation step; and a recovery step where the water layer produced in the oil-water separation step is recovered. Further, the cleaning separation step is performed using the water laer recovered in the recovery step as crude tar acid soda.SELECTED DRAWING: Figure 1 【課題】軽油洗浄法によるタール酸ソーダの精製方法において、精製タール酸ソーダとして回収されないタール酸ソーダの量を低減する。【解決手段】この発明のタール酸ソーダの精製方法は、粗製タール酸ソーダを軽油と接触させて粗製タール酸ソーダ中の油性の不純物を軽油中に抽出することで、粗製タール酸ソーダと軽油との混合物を、軽油および不純物を含む液体とタール酸ソーダとに分離する洗浄分離工程を有する。また、洗浄分離工程で得られた軽油および不純物を含む液体を油水分離する油水分離工程と、油水分離工程で生じた水層を回収する回収工程と、を有する。さらに、回収工程で回収された水層を粗製タール酸ソーダとして用いて洗浄分離工程を行う。【選択図】図1