SYNTHESIS OF METAL ION SEQUESTRATION RESINS FOR WATER TREATMENT IN LIGHT WATER REACTORS

PROBLEM TO BE SOLVED: To provide an organic synthesis of materials to remove low molecular weight ionic species, such as transition metal ions including cobalt, iron, nickel, and zinc, from aqueous solutions.SOLUTION: The synthesis includes the steps of providing a cation exchange resin, functionali...

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Hauptverfasser:	DANIEL MORGAN WELLS, LEON YENGOYAN, PAUL L FRATTINI
Format:	Patent
Sprache:	eng
Schlagworte:	ADHESIVES CHEMISTRY COMPOSITIONS BASED THEREON DECONTAMINATION ARRANGEMENTS THEREFOR DYES MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVINGCARBON-TO-CARBON UNSATURATED BONDS MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE METALLURGY MISCELLANEOUS APPLICATIONS OF MATERIALS MISCELLANEOUS COMPOSITIONS NATURAL RESINS NUCLEAR ENGINEERING NUCLEAR PHYSICS ORGANIC MACROMOLECULAR COMPOUNDS PAINTS PHYSICS POLISHES PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULARRADIATION OR PARTICLE BOMBARDMENT THEIR PREPARATION OR CHEMICAL WORKING-UP TREATING RADIOACTIVELY CONTAMINATED MATERIAL
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Beschreibung
Zusammenfassung:	PROBLEM TO BE SOLVED: To provide an organic synthesis of materials to remove low molecular weight ionic species, such as transition metal ions including cobalt, iron, nickel, and zinc, from aqueous solutions.SOLUTION: The synthesis includes the steps of providing a cation exchange resin, functionalizing the cation exchange resin using a chloride intermediate to form a sulfonyl chloride resin, and reacting a multi-amine based ligand with the sulfonyl chloride resin to form a metal ion sequestration resin. The synthesis further includes the steps of cooling the metal ion sequestration resin, washing and drying the metal ion sequestration resin, and removing any unconverted sulfonate sites from the metal ion sequestration resin.