METHOD FOR PRODUCING METAL POWDER AND SOLDER PASTE USING METAL POWDER OBTAINED BY THE METHOD
PROBLEM TO BE SOLVED: To provide a simple method for collecting a metal powder which is suitable for use as a fine-pitch solder powder and has a volume-cumulative median diameter D50in the range of 1-5 μm, at a high yield. SOLUTION: When producing the metal powder having the volume-cumulative median...
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creator | HISAYOSHI KANJI MURAOKA HIROKI |
description | PROBLEM TO BE SOLVED: To provide a simple method for collecting a metal powder which is suitable for use as a fine-pitch solder powder and has a volume-cumulative median diameter D50in the range of 1-5 μm, at a high yield. SOLUTION: When producing the metal powder having the volume-cumulative median diameter D50of 1-5 μm by mixing a first aqueous solution containing a cation of a base metal with a second aqueous solution containing a divalent chromium ion to cause a reduction reaction therebetween, this method includes: introducing each tip part of first and second supply pipes 12a and 12b into the inside of a reaction vessel 11; arranging each of the tips in parallel at a fixed height from the inner bottom of the vessel with a spacing between the tips; introducing the first aqueous solution and the second aqueous solution from the first supply pipe and the second supply pipe into the vessel at a fixed flow rate to bring both of the aqueous solutions in contact with each other in the vessel; thereby causing the reduction reaction between the solutions to generate nuclei of the metal powder; also retaining a mixture of both of the aqueous solutions in the vessel for a fixed period of time while holding a liquid level 11c at a fixed height to grow the nuclei of the metal powder, which have been formed through the reduction reaction; and then discharging the mixture of both of the aqueous solutions from the bottom of the vessel at a fixed flow rate. COPYRIGHT: (C)2011,JPO&INPIT |
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SOLUTION: When producing the metal powder having the volume-cumulative median diameter D50of 1-5 μm by mixing a first aqueous solution containing a cation of a base metal with a second aqueous solution containing a divalent chromium ion to cause a reduction reaction therebetween, this method includes: introducing each tip part of first and second supply pipes 12a and 12b into the inside of a reaction vessel 11; arranging each of the tips in parallel at a fixed height from the inner bottom of the vessel with a spacing between the tips; introducing the first aqueous solution and the second aqueous solution from the first supply pipe and the second supply pipe into the vessel at a fixed flow rate to bring both of the aqueous solutions in contact with each other in the vessel; thereby causing the reduction reaction between the solutions to generate nuclei of the metal powder; also retaining a mixture of both of the aqueous solutions in the vessel for a fixed period of time while holding a liquid level 11c at a fixed height to grow the nuclei of the metal powder, which have been formed through the reduction reaction; and then discharging the mixture of both of the aqueous solutions from the bottom of the vessel at a fixed flow rate. 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SOLUTION: When producing the metal powder having the volume-cumulative median diameter D50of 1-5 μm by mixing a first aqueous solution containing a cation of a base metal with a second aqueous solution containing a divalent chromium ion to cause a reduction reaction therebetween, this method includes: introducing each tip part of first and second supply pipes 12a and 12b into the inside of a reaction vessel 11; arranging each of the tips in parallel at a fixed height from the inner bottom of the vessel with a spacing between the tips; introducing the first aqueous solution and the second aqueous solution from the first supply pipe and the second supply pipe into the vessel at a fixed flow rate to bring both of the aqueous solutions in contact with each other in the vessel; thereby causing the reduction reaction between the solutions to generate nuclei of the metal powder; also retaining a mixture of both of the aqueous solutions in the vessel for a fixed period of time while holding a liquid level 11c at a fixed height to grow the nuclei of the metal powder, which have been formed through the reduction reaction; and then discharging the mixture of both of the aqueous solutions from the bottom of the vessel at a fixed flow rate. 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SOLUTION: When producing the metal powder having the volume-cumulative median diameter D50of 1-5 μm by mixing a first aqueous solution containing a cation of a base metal with a second aqueous solution containing a divalent chromium ion to cause a reduction reaction therebetween, this method includes: introducing each tip part of first and second supply pipes 12a and 12b into the inside of a reaction vessel 11; arranging each of the tips in parallel at a fixed height from the inner bottom of the vessel with a spacing between the tips; introducing the first aqueous solution and the second aqueous solution from the first supply pipe and the second supply pipe into the vessel at a fixed flow rate to bring both of the aqueous solutions in contact with each other in the vessel; thereby causing the reduction reaction between the solutions to generate nuclei of the metal powder; also retaining a mixture of both of the aqueous solutions in the vessel for a fixed period of time while holding a liquid level 11c at a fixed height to grow the nuclei of the metal powder, which have been formed through the reduction reaction; and then discharging the mixture of both of the aqueous solutions from the bottom of the vessel at a fixed flow rate. COPYRIGHT: (C)2011,JPO&INPIT</abstract><oa>free_for_read</oa></addata></record> |
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subjects | CASTING CLADDING OR PLATING BY SOLDERING OR WELDING CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING MACHINE TOOLS MAKING METALLIC POWDER MANUFACTURE OF ARTICLES FROM METALLIC POWDER METAL-WORKING NOT OTHERWISE PROVIDED FOR PERFORMING OPERATIONS POWDER METALLURGY SOLDERING OR UNSOLDERING TRANSPORTING WELDING WORKING BY LASER BEAM WORKING METALLIC POWDER |
title | METHOD FOR PRODUCING METAL POWDER AND SOLDER PASTE USING METAL POWDER OBTAINED BY THE METHOD |
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