PROCESS FOR PRODUCING CHLOROANILINES FROM CHLORONITROBENZENE BY HETEROGENOUS HYDROGENATION UNDER PRESSURE
3,4-di:chloro-anilines are prepd. from o-, m-, p-, -chloro-nitro-benzenes and 3,4-di:chloro-nitro-benzene by hydrogenation at 50-150 deg. C and 3-15 MPa pressure using fixed bed catalyst. - Hydrogenation is carried out on 60-80% porous gamma-Al2O3 of a specific surface: 120-160 m2/g; average dia. is...
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creator | WAHLNE HORVATH,ILONA,HU SZILAGYI,GYULA,HU BORDAS,ZOLTANNE,HU RAKSI,GYULA,HU KALACSKA,JANOS,HU NEMETH,LASZLO,HU REDEI,JOZSEF,HU KEREKES,FERENC,HU GATI,GYULA,HU SZITA,ISTVAN,HU |
description | 3,4-di:chloro-anilines are prepd. from o-, m-, p-, -chloro-nitro-benzenes and 3,4-di:chloro-nitro-benzene by hydrogenation at 50-150 deg. C and 3-15 MPa pressure using fixed bed catalyst. - Hydrogenation is carried out on 60-80% porous gamma-Al2O3 of a specific surface: 120-160 m2/g; average dia. is 0.8-1.2 mm; average length 3-5 mm and 5-6 N/m breaking strength. The catalyst opt. treated by HCl and tetra-butyl-ammonium-hydroxide contains 0.2-5.0 wt.% Pli |
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C and 3-15 MPa pressure using fixed bed catalyst. - Hydrogenation is carried out on 60-80% porous gamma-Al2O3 of a specific surface: 120-160 m2/g; average dia. is 0.8-1.2 mm; average length 3-5 mm and 5-6 N/m breaking strength. The catalyst opt. treated by HCl and tetra-butyl-ammonium-hydroxide contains 0.2-5.0 wt.% Pli</abstract><edition>5</edition><oa>free_for_read</oa></addata></record> |
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subjects | ACYCLIC OR CARBOCYCLIC COMPOUNDS APPARATUS THEREFOR CHEMISTRY GENERAL METHODS OF ORGANIC CHEMISTRY METALLURGY ORGANIC CHEMISTRY |
title | PROCESS FOR PRODUCING CHLOROANILINES FROM CHLORONITROBENZENE BY HETEROGENOUS HYDROGENATION UNDER PRESSURE |
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