PROCEDIMIENTO PARA LA PRODUCCION DE DERIVADOS DE AZACICLOALCANOS
UN PROCESO PARA LA PRODUCCION DE UN DERIVADO DE AZACICLOALCANO REPRESENTADO POR LA FORMULA GENERAL (II), EN LA CUAL M REPRESENTA UN NUMERO ENTERO DE 1 A 3, N2 REPRESENTA UN NUMERO ENTERO DE 2 A 10, Y R REPRESENTA UN ALQUILO DE C3 A C12. EL PROCESO COMPRENDE LA REACCION DE 1-(N-ALQUENIL)AZACICLOALCAN...
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| creator | INOUE, HISATAKA SAITA, MASARU NODA, KANJI YAHIRO, SHIGENORI HACHIYA, TERUMI |
| description | UN PROCESO PARA LA PRODUCCION DE UN DERIVADO DE AZACICLOALCANO REPRESENTADO POR LA FORMULA GENERAL (II), EN LA CUAL M REPRESENTA UN NUMERO ENTERO DE 1 A 3, N2 REPRESENTA UN NUMERO ENTERO DE 2 A 10, Y R REPRESENTA UN ALQUILO DE C3 A C12. EL PROCESO COMPRENDE LA REACCION DE 1-(N-ALQUENIL)AZACICLOALCAN-2-UNO, REPRESENTADO POR LA FORMULA GENERAL (I) EN LA CUAL M SE DEFINE COMO ANTES Y N1 REPRESENTA UN NUMERO ENTERO ENTRE 0 Y 8, CON UN MERCAPTAN ALQUILO EN PRESENCIA DE UN INICIADOR/CATALISTA RADICAL EN UN SLOVENTE ORGANICO, TRATANDO EL PRODUCTO DE LA REACCION CON UN AGENTE DE REDUCCION EN UN SOLVENTE ORGANICO ACUOSO, SEGUIDO POR LA PURIFICACION MEDIANTE LA DESTILACION.
A process for producing an azacycloalkane derivative represented by general formula (II), wherein m represents an integer of 1 to 3, n2 represents an integer of 2 to 10, and R represents C3 to C12 alkyl, which comprises reacting 1-(n- alkenyl)azacycloalkan-2-one represented by general formula (I) wherein, m is as defined above and n1 represents an integer of 0 to 8, with an alkyl mercaptan in the presence of a radical initiator in an organic solvent, treating the reaction product with a reducing agent in a watery organic solvent, followed by purification through distillation. |
| format | Patent |
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A process for producing an azacycloalkane derivative represented by general formula (II), wherein m represents an integer of 1 to 3, n2 represents an integer of 2 to 10, and R represents C3 to C12 alkyl, which comprises reacting 1-(n- alkenyl)azacycloalkan-2-one represented by general formula (I) wherein, m is as defined above and n1 represents an integer of 0 to 8, with an alkyl mercaptan in the presence of a radical initiator in an organic solvent, treating the reaction product with a reducing agent in a watery organic solvent, followed by purification through distillation.</description><edition>7</edition><language>spa</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2001</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20010416&DB=EPODOC&CC=ES&NR=2154632T3$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20010416&DB=EPODOC&CC=ES&NR=2154632T3$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>INOUE, HISATAKA</creatorcontrib><creatorcontrib>SAITA, MASARU</creatorcontrib><creatorcontrib>NODA, KANJI</creatorcontrib><creatorcontrib>YAHIRO, SHIGENORI</creatorcontrib><creatorcontrib>HACHIYA, TERUMI</creatorcontrib><title>PROCEDIMIENTO PARA LA PRODUCCION DE DERIVADOS DE AZACICLOALCANOS</title><description>UN PROCESO PARA LA PRODUCCION DE UN DERIVADO DE AZACICLOALCANO REPRESENTADO POR LA FORMULA GENERAL (II), EN LA CUAL M REPRESENTA UN NUMERO ENTERO DE 1 A 3, N2 REPRESENTA UN NUMERO ENTERO DE 2 A 10, Y R REPRESENTA UN ALQUILO DE C3 A C12. EL PROCESO COMPRENDE LA REACCION DE 1-(N-ALQUENIL)AZACICLOALCAN-2-UNO, REPRESENTADO POR LA FORMULA GENERAL (I) EN LA CUAL M SE DEFINE COMO ANTES Y N1 REPRESENTA UN NUMERO ENTERO ENTRE 0 Y 8, CON UN MERCAPTAN ALQUILO EN PRESENCIA DE UN INICIADOR/CATALISTA RADICAL EN UN SLOVENTE ORGANICO, TRATANDO EL PRODUCTO DE LA REACCION CON UN AGENTE DE REDUCCION EN UN SOLVENTE ORGANICO ACUOSO, SEGUIDO POR LA PURIFICACION MEDIANTE LA DESTILACION.
A process for producing an azacycloalkane derivative represented by general formula (II), wherein m represents an integer of 1 to 3, n2 represents an integer of 2 to 10, and R represents C3 to C12 alkyl, which comprises reacting 1-(n- alkenyl)azacycloalkan-2-one represented by general formula (I) wherein, m is as defined above and n1 represents an integer of 0 to 8, with an alkyl mercaptan in the presence of a radical initiator in an organic solvent, treating the reaction product with a reducing agent in a watery organic solvent, followed by purification through distillation.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2001</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZHAICPJ3dnXx9PV09QvxVwhwDHJU8HFUAIq6hDo7e_r7Kbi4AlGQZ5iji38wiOMY5ejs6ezj7-jj7OjnH8zDwJqWmFOcyguluRkU3VxDnD10Uwvy41OLCxKTU_NSS-Jdg40MTU3MjI1CQoyNiVEDAKLsKuo</recordid><startdate>20010416</startdate><enddate>20010416</enddate><creator>INOUE, HISATAKA</creator><creator>SAITA, MASARU</creator><creator>NODA, KANJI</creator><creator>YAHIRO, SHIGENORI</creator><creator>HACHIYA, TERUMI</creator><scope>EVB</scope></search><sort><creationdate>20010416</creationdate><title>PROCEDIMIENTO PARA LA PRODUCCION DE DERIVADOS DE AZACICLOALCANOS</title><author>INOUE, HISATAKA ; SAITA, MASARU ; NODA, KANJI ; YAHIRO, SHIGENORI ; HACHIYA, TERUMI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_ES2154632TT33</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>spa</language><creationdate>2001</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>INOUE, HISATAKA</creatorcontrib><creatorcontrib>SAITA, MASARU</creatorcontrib><creatorcontrib>NODA, KANJI</creatorcontrib><creatorcontrib>YAHIRO, SHIGENORI</creatorcontrib><creatorcontrib>HACHIYA, TERUMI</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>INOUE, HISATAKA</au><au>SAITA, MASARU</au><au>NODA, KANJI</au><au>YAHIRO, SHIGENORI</au><au>HACHIYA, TERUMI</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCEDIMIENTO PARA LA PRODUCCION DE DERIVADOS DE AZACICLOALCANOS</title><date>2001-04-16</date><risdate>2001</risdate><abstract>UN PROCESO PARA LA PRODUCCION DE UN DERIVADO DE AZACICLOALCANO REPRESENTADO POR LA FORMULA GENERAL (II), EN LA CUAL M REPRESENTA UN NUMERO ENTERO DE 1 A 3, N2 REPRESENTA UN NUMERO ENTERO DE 2 A 10, Y R REPRESENTA UN ALQUILO DE C3 A C12. EL PROCESO COMPRENDE LA REACCION DE 1-(N-ALQUENIL)AZACICLOALCAN-2-UNO, REPRESENTADO POR LA FORMULA GENERAL (I) EN LA CUAL M SE DEFINE COMO ANTES Y N1 REPRESENTA UN NUMERO ENTERO ENTRE 0 Y 8, CON UN MERCAPTAN ALQUILO EN PRESENCIA DE UN INICIADOR/CATALISTA RADICAL EN UN SLOVENTE ORGANICO, TRATANDO EL PRODUCTO DE LA REACCION CON UN AGENTE DE REDUCCION EN UN SOLVENTE ORGANICO ACUOSO, SEGUIDO POR LA PURIFICACION MEDIANTE LA DESTILACION.
A process for producing an azacycloalkane derivative represented by general formula (II), wherein m represents an integer of 1 to 3, n2 represents an integer of 2 to 10, and R represents C3 to C12 alkyl, which comprises reacting 1-(n- alkenyl)azacycloalkan-2-one represented by general formula (I) wherein, m is as defined above and n1 represents an integer of 0 to 8, with an alkyl mercaptan in the presence of a radical initiator in an organic solvent, treating the reaction product with a reducing agent in a watery organic solvent, followed by purification through distillation.</abstract><edition>7</edition><oa>free_for_read</oa></addata></record> |
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| subjects | CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
| title | PROCEDIMIENTO PARA LA PRODUCCION DE DERIVADOS DE AZACICLOALCANOS |
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