PROCESS FOR PRODUCING MICROPARTICLES LADEN WITH A VOLATILE ORGANIC ACTIVE
The present invention relates to a process for producing microparticles laden with at least one active, wherein the microparticles are formed from a thermoplastic organic, polymeric material and in the unladen state, in their interior, have at least one cavity connected via pores to the surface of t...
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| creator | MOHR, Thorsten GARELLA, Dominik KRAUSE, Wolfgang OSCHMANN, Bernd Dieter FRANCK, Miika |
| description | The present invention relates to a process for producing microparticles laden with at least one active, wherein the microparticles are formed from a thermoplastic organic, polymeric material and in the unladen state, in their interior, have at least one cavity connected via pores to the surface of the microparticles, wherein (a) a composition of unladen microparticles are impregnated with a liquid comprising the active, whereby laden microparticles are obtained, which contain in the interior cavity the liquid, and (b) subjecting the laden microparticles to thermal treatment by passing a stream of free flowing laden microparticles in a carrier gas through a heated zone at a temperature of at least 20 K, in particular at least 40 K, e.g. 20 to 250 K especially 40 to 200 K above the softening temperature of the thermoplastic organic polymeric material, where the average residence time of the laden microparticles in the heated zone is not more than 60 s, in particular not more than 30 s, especially not more than 20 s or not more than 10 s, e.g. in the range of 0.1 to 60 s, in particular in the range of 0.1 to 30 s, more particularly in the range of 0.5 to 20 s and especially in the range of 1 to 10 s. The present invention further relates to compositions of microparticles filled with at least one active, in particular with at least volatile organic active, which is obtainable by a process of the invention, and to the use thereof, especially in a product selected from perfumes, washing and cleaning compositions, cosmetic compositions, personal care compositions, hygiene articles, foods, food supplements, fragrance dispensers and fragrances. The present invention further relates to products comprising an inventive composition of microparticles filled with at least one active, in particular with at least one volatile organic active, and to the use thereof, especially for controlled release of actives of low molecular weight and specifically for controlled release of aroma chemicals. |
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The present invention further relates to compositions of microparticles filled with at least one active, in particular with at least volatile organic active, which is obtainable by a process of the invention, and to the use thereof, especially in a product selected from perfumes, washing and cleaning compositions, cosmetic compositions, personal care compositions, hygiene articles, foods, food supplements, fragrance dispensers and fragrances. The present invention further relates to products comprising an inventive composition of microparticles filled with at least one active, in particular with at least one volatile organic active, and to the use thereof, especially for controlled release of actives of low molecular weight and specifically for controlled release of aroma chemicals.</description><language>eng ; fre ; ger</language><subject>AGRICULTURE ; ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES ; ANIMAL HUSBANDRY ; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES ; CANDLES ; CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; DETERGENT COMPOSITIONS ; DETERGENTS ; FATTY ACIDS THEREFROM ; FISHING ; FOODS OR FOODSTUFFS ; FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BYSUBCLASSES A23B - A23J ; FORESTRY ; HUMAN NECESSITIES ; HUNTING ; HYGIENE ; MEDICAL OR VETERINARY SCIENCE ; METALLURGY ; PERFORMING OPERATIONS ; PEST REPELLANTS OR ATTRACTANTS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; PLANT GROWTH REGULATORS ; PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES ; PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF ; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL ; RECOVERY OF GLYCEROL ; RESIN SOAPS ; SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY ASINGLE OTHER SUBCLASS ; SOAP OR SOAP-MAKING ; SPECIFIC USE OF COSMETICS OR SIMILAR TOILETPREPARATIONS ; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OFNUTRITIVE QUALITIES, PHYSICAL TREATMENT ; THEIR RELEVANT APPARATUS ; THEIR TREATMENT, NOT COVERED BY OTHER CLASSES ; TRANSPORTING ; TRAPPING ; USE OF SINGLE SUBSTANCES AS DETERGENTS</subject><creationdate>2022</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220518&DB=EPODOC&CC=EP&NR=3996660A1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20220518&DB=EPODOC&CC=EP&NR=3996660A1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>MOHR, Thorsten</creatorcontrib><creatorcontrib>GARELLA, Dominik</creatorcontrib><creatorcontrib>KRAUSE, Wolfgang</creatorcontrib><creatorcontrib>OSCHMANN, Bernd Dieter</creatorcontrib><creatorcontrib>FRANCK, Miika</creatorcontrib><title>PROCESS FOR PRODUCING MICROPARTICLES LADEN WITH A VOLATILE ORGANIC ACTIVE</title><description>The present invention relates to a process for producing microparticles laden with at least one active, wherein the microparticles are formed from a thermoplastic organic, polymeric material and in the unladen state, in their interior, have at least one cavity connected via pores to the surface of the microparticles, wherein (a) a composition of unladen microparticles are impregnated with a liquid comprising the active, whereby laden microparticles are obtained, which contain in the interior cavity the liquid, and (b) subjecting the laden microparticles to thermal treatment by passing a stream of free flowing laden microparticles in a carrier gas through a heated zone at a temperature of at least 20 K, in particular at least 40 K, e.g. 20 to 250 K especially 40 to 200 K above the softening temperature of the thermoplastic organic polymeric material, where the average residence time of the laden microparticles in the heated zone is not more than 60 s, in particular not more than 30 s, especially not more than 20 s or not more than 10 s, e.g. in the range of 0.1 to 60 s, in particular in the range of 0.1 to 30 s, more particularly in the range of 0.5 to 20 s and especially in the range of 1 to 10 s. The present invention further relates to compositions of microparticles filled with at least one active, in particular with at least volatile organic active, which is obtainable by a process of the invention, and to the use thereof, especially in a product selected from perfumes, washing and cleaning compositions, cosmetic compositions, personal care compositions, hygiene articles, foods, food supplements, fragrance dispensers and fragrances. The present invention further relates to products comprising an inventive composition of microparticles filled with at least one active, in particular with at least one volatile organic active, and to the use thereof, especially for controlled release of actives of low molecular weight and specifically for controlled release of aroma chemicals.</description><subject>AGRICULTURE</subject><subject>ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES</subject><subject>ANIMAL HUSBANDRY</subject><subject>BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES</subject><subject>CANDLES</subject><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</subject><subject>CHEMISTRY</subject><subject>DETERGENT COMPOSITIONS</subject><subject>DETERGENTS</subject><subject>FATTY ACIDS THEREFROM</subject><subject>FISHING</subject><subject>FOODS OR FOODSTUFFS</subject><subject>FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BYSUBCLASSES A23B - A23J</subject><subject>FORESTRY</subject><subject>HUMAN NECESSITIES</subject><subject>HUNTING</subject><subject>HYGIENE</subject><subject>MEDICAL OR VETERINARY SCIENCE</subject><subject>METALLURGY</subject><subject>PERFORMING OPERATIONS</subject><subject>PEST REPELLANTS OR ATTRACTANTS</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>PLANT GROWTH REGULATORS</subject><subject>PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES</subject><subject>PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF</subject><subject>PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL</subject><subject>RECOVERY OF GLYCEROL</subject><subject>RESIN SOAPS</subject><subject>SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY ASINGLE OTHER SUBCLASS</subject><subject>SOAP OR SOAP-MAKING</subject><subject>SPECIFIC USE OF COSMETICS OR SIMILAR TOILETPREPARATIONS</subject><subject>THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OFNUTRITIVE QUALITIES, PHYSICAL TREATMENT</subject><subject>THEIR RELEVANT APPARATUS</subject><subject>THEIR TREATMENT, NOT COVERED BY OTHER CLASSES</subject><subject>TRANSPORTING</subject><subject>TRAPPING</subject><subject>USE OF SINGLE SUBSTANCES AS DETERGENTS</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2022</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZPAMCPJ3dg0OVnDzD1IAsl1CnT393BV8PZ2D_AMcg0I8nX1cgxV8HF1c_RTCPUM8FBwVwvx9HEM8fVwV_IPcHf08nRUcnUM8w1x5GFjTEnOKU3mhNDeDgptriLOHbmpBfnxqcUFicmpeakm8a4CxpaWZmZmBo6ExEUoA6Yws2A</recordid><startdate>20220518</startdate><enddate>20220518</enddate><creator>MOHR, Thorsten</creator><creator>GARELLA, Dominik</creator><creator>KRAUSE, Wolfgang</creator><creator>OSCHMANN, Bernd Dieter</creator><creator>FRANCK, Miika</creator><scope>EVB</scope></search><sort><creationdate>20220518</creationdate><title>PROCESS FOR PRODUCING MICROPARTICLES LADEN WITH A VOLATILE ORGANIC ACTIVE</title><author>MOHR, Thorsten ; GARELLA, Dominik ; KRAUSE, Wolfgang ; OSCHMANN, Bernd Dieter ; FRANCK, Miika</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_EP3996660A13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; fre ; ger</language><creationdate>2022</creationdate><topic>AGRICULTURE</topic><topic>ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES</topic><topic>ANIMAL HUSBANDRY</topic><topic>BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES</topic><topic>CANDLES</topic><topic>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</topic><topic>CHEMISTRY</topic><topic>DETERGENT COMPOSITIONS</topic><topic>DETERGENTS</topic><topic>FATTY ACIDS THEREFROM</topic><topic>FISHING</topic><topic>FOODS OR FOODSTUFFS</topic><topic>FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BYSUBCLASSES A23B - A23J</topic><topic>FORESTRY</topic><topic>HUMAN NECESSITIES</topic><topic>HUNTING</topic><topic>HYGIENE</topic><topic>MEDICAL OR VETERINARY SCIENCE</topic><topic>METALLURGY</topic><topic>PERFORMING OPERATIONS</topic><topic>PEST REPELLANTS OR ATTRACTANTS</topic><topic>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</topic><topic>PLANT GROWTH REGULATORS</topic><topic>PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES</topic><topic>PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF</topic><topic>PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL</topic><topic>RECOVERY OF GLYCEROL</topic><topic>RESIN SOAPS</topic><topic>SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY ASINGLE OTHER SUBCLASS</topic><topic>SOAP OR SOAP-MAKING</topic><topic>SPECIFIC USE OF COSMETICS OR SIMILAR TOILETPREPARATIONS</topic><topic>THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OFNUTRITIVE QUALITIES, PHYSICAL TREATMENT</topic><topic>THEIR RELEVANT APPARATUS</topic><topic>THEIR TREATMENT, NOT COVERED BY OTHER CLASSES</topic><topic>TRANSPORTING</topic><topic>TRAPPING</topic><topic>USE OF SINGLE SUBSTANCES AS DETERGENTS</topic><toplevel>online_resources</toplevel><creatorcontrib>MOHR, Thorsten</creatorcontrib><creatorcontrib>GARELLA, Dominik</creatorcontrib><creatorcontrib>KRAUSE, Wolfgang</creatorcontrib><creatorcontrib>OSCHMANN, Bernd Dieter</creatorcontrib><creatorcontrib>FRANCK, Miika</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>MOHR, Thorsten</au><au>GARELLA, Dominik</au><au>KRAUSE, Wolfgang</au><au>OSCHMANN, Bernd Dieter</au><au>FRANCK, Miika</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS FOR PRODUCING MICROPARTICLES LADEN WITH A VOLATILE ORGANIC ACTIVE</title><date>2022-05-18</date><risdate>2022</risdate><abstract>The present invention relates to a process for producing microparticles laden with at least one active, wherein the microparticles are formed from a thermoplastic organic, polymeric material and in the unladen state, in their interior, have at least one cavity connected via pores to the surface of the microparticles, wherein (a) a composition of unladen microparticles are impregnated with a liquid comprising the active, whereby laden microparticles are obtained, which contain in the interior cavity the liquid, and (b) subjecting the laden microparticles to thermal treatment by passing a stream of free flowing laden microparticles in a carrier gas through a heated zone at a temperature of at least 20 K, in particular at least 40 K, e.g. 20 to 250 K especially 40 to 200 K above the softening temperature of the thermoplastic organic polymeric material, where the average residence time of the laden microparticles in the heated zone is not more than 60 s, in particular not more than 30 s, especially not more than 20 s or not more than 10 s, e.g. in the range of 0.1 to 60 s, in particular in the range of 0.1 to 30 s, more particularly in the range of 0.5 to 20 s and especially in the range of 1 to 10 s. The present invention further relates to compositions of microparticles filled with at least one active, in particular with at least volatile organic active, which is obtainable by a process of the invention, and to the use thereof, especially in a product selected from perfumes, washing and cleaning compositions, cosmetic compositions, personal care compositions, hygiene articles, foods, food supplements, fragrance dispensers and fragrances. The present invention further relates to products comprising an inventive composition of microparticles filled with at least one active, in particular with at least one volatile organic active, and to the use thereof, especially for controlled release of actives of low molecular weight and specifically for controlled release of aroma chemicals.</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | AGRICULTURE ANIMAL AND VEGETABLE OILS, FATS, FATTY SUBSTANCES AND WAXES ANIMAL HUSBANDRY BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES, AS HERBICIDES CANDLES CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY DETERGENT COMPOSITIONS DETERGENTS FATTY ACIDS THEREFROM FISHING FOODS OR FOODSTUFFS FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BYSUBCLASSES A23B - A23J FORESTRY HUMAN NECESSITIES HUNTING HYGIENE MEDICAL OR VETERINARY SCIENCE METALLURGY PERFORMING OPERATIONS PEST REPELLANTS OR ATTRACTANTS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL PLANT GROWTH REGULATORS PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTSTHEREOF PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL RECOVERY OF GLYCEROL RESIN SOAPS SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY ASINGLE OTHER SUBCLASS SOAP OR SOAP-MAKING SPECIFIC USE OF COSMETICS OR SIMILAR TOILETPREPARATIONS THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OFNUTRITIVE QUALITIES, PHYSICAL TREATMENT THEIR RELEVANT APPARATUS THEIR TREATMENT, NOT COVERED BY OTHER CLASSES TRANSPORTING TRAPPING USE OF SINGLE SUBSTANCES AS DETERGENTS |
| title | PROCESS FOR PRODUCING MICROPARTICLES LADEN WITH A VOLATILE ORGANIC ACTIVE |
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