METHOD FOR PRODUCING XYLYLENEDIAMINE

There is provided a method for producing xylylenediamine, including: (1) performing a first hydrogenation including hydrogenating a mixed solution including dicyanobenzene and a solvent containing liquid ammonia in a fixed-bed reactor to produce a reaction product (A); (2) performing ammonia separat...

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Hauptverfasser: IBI, Yukiya, KUMANO, Tatsuyuki
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creator IBI, Yukiya
KUMANO, Tatsuyuki
description There is provided a method for producing xylylenediamine, including: (1) performing a first hydrogenation including hydrogenating a mixed solution including dicyanobenzene and a solvent containing liquid ammonia in a fixed-bed reactor to produce a reaction product (A); (2) performing ammonia separation including separating and removing the liquid ammonia included in the reaction product (A) or (D) to produce a reaction product (B) or (E); (3) performing solid-liquid separation including subjecting the reaction product (B) or (A) to solid-liquid separation and removing a solid component to produce a reaction product (C) or (D); and (4) performing a second hydrogenation including hydrogenating the reaction product (C) or (E) in a fixed-bed reactor, in which step (2) and step (3) are performed in this order or in a reverse order after step (1), followed by step (4).
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
APPARATUS THEREFOR
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
GENERAL METHODS OF ORGANIC CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR RELEVANT APPARATUS
TRANSPORTING
title METHOD FOR PRODUCING XYLYLENEDIAMINE
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