METHOD OF PREPARING SAMPLE FOR CRYSTAL STRUCTURE ANALYSIS, METHOD OF DETERMINING ABSOLUTE CONFIGURATION OF CHIRAL COMPOUND, AND POLYNUCLEAR METAL COMPLEX MONOCRYSTAL
Provided are: a method for preparing a crystal structure analysis sample for determining an absolute configuration of a chiral compound, the method comprising bringing a single crystal of a porous compound into contact with a solvent solution that comprises a chiral compound for which the absolute c...
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creator | FUJITA Makoto ARAI Tatsuhiko INOKUMA Yasuhide |
description | Provided are: a method for preparing a crystal structure analysis sample for determining an absolute configuration of a chiral compound, the method comprising bringing a single crystal of a porous compound into contact with a solvent solution that comprises a chiral compound for which the absolute configuration is to be determined, to prepare a crystal structure analysis sample, the single crystal of the porous compound comprising a three-dimensional framework, and either or both of pores and voids that are defined by the three-dimensional framework, and are three-dimensionally arranged in an ordered manner, the three-dimensional framework being formed by one molecular chain or two or more molecular chains, or formed by one molecular chain or two or more molecular chains, and a framework-forming compound, and comprising a chiral substituent of which the absolute configuration is known, the crystal structure analysis sample having a structure in which molecules of the chiral compound are arranged in either or both of the pores and the voids of the single crystal in an ordered manner; a method for determining an absolute configuration of a chiral compound, wherein a crystal structure analysis sample obtained by the aforementioned method is used; and a single crystal of a polynuclear metal complex suitable for used the method for preparing a sample for crystal structure analysis. |
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ARAI Tatsuhiko ; INOKUMA Yasuhide</creatorcontrib><description>Provided are: a method for preparing a crystal structure analysis sample for determining an absolute configuration of a chiral compound, the method comprising bringing a single crystal of a porous compound into contact with a solvent solution that comprises a chiral compound for which the absolute configuration is to be determined, to prepare a crystal structure analysis sample, the single crystal of the porous compound comprising a three-dimensional framework, and either or both of pores and voids that are defined by the three-dimensional framework, and are three-dimensionally arranged in an ordered manner, the three-dimensional framework being formed by one molecular chain or two or more molecular chains, or formed by one molecular chain or two or more molecular chains, and a framework-forming compound, and comprising a chiral substituent of which the absolute configuration is known, the crystal structure analysis sample having a structure in which molecules of the chiral compound are arranged in either or both of the pores and the voids of the single crystal in an ordered manner; a method for determining an absolute configuration of a chiral compound, wherein a crystal structure analysis sample obtained by the aforementioned method is used; and a single crystal of a polynuclear metal complex suitable for used the method for preparing a sample for crystal structure analysis.</description><language>eng ; fre ; ger</language><subject>AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUSPOLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE ; APPARATUS THEREFOR ; CHEMISTRY ; CRYSTAL GROWTH ; INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES ; MEASURING ; METALLURGY ; PHYSICS ; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITHDEFINED STRUCTURE ; REFINING BY ZONE-MELTING OF MATERIAL ; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITHDEFINED STRUCTURE ; SINGLE-CRYSTAL-GROWTH ; TESTING ; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL ORUNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL</subject><creationdate>2017</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20171004&DB=EPODOC&CC=EP&NR=3118610A4$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20171004&DB=EPODOC&CC=EP&NR=3118610A4$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>FUJITA Makoto</creatorcontrib><creatorcontrib>ARAI Tatsuhiko</creatorcontrib><creatorcontrib>INOKUMA Yasuhide</creatorcontrib><title>METHOD OF PREPARING SAMPLE FOR CRYSTAL STRUCTURE ANALYSIS, METHOD OF DETERMINING ABSOLUTE CONFIGURATION OF CHIRAL COMPOUND, AND POLYNUCLEAR METAL COMPLEX MONOCRYSTAL</title><description>Provided are: a method for preparing a crystal structure analysis sample for determining an absolute configuration of a chiral compound, the method comprising bringing a single crystal of a porous compound into contact with a solvent solution that comprises a chiral compound for which the absolute configuration is to be determined, to prepare a crystal structure analysis sample, the single crystal of the porous compound comprising a three-dimensional framework, and either or both of pores and voids that are defined by the three-dimensional framework, and are three-dimensionally arranged in an ordered manner, the three-dimensional framework being formed by one molecular chain or two or more molecular chains, or formed by one molecular chain or two or more molecular chains, and a framework-forming compound, and comprising a chiral substituent of which the absolute configuration is known, the crystal structure analysis sample having a structure in which molecules of the chiral compound are arranged in either or both of the pores and the voids of the single crystal in an ordered manner; a method for determining an absolute configuration of a chiral compound, wherein a crystal structure analysis sample obtained by the aforementioned method is used; and a single crystal of a polynuclear metal complex suitable for used the method for preparing a sample for crystal structure analysis.</description><subject>AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUSPOLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE</subject><subject>APPARATUS THEREFOR</subject><subject>CHEMISTRY</subject><subject>CRYSTAL GROWTH</subject><subject>INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES</subject><subject>MEASURING</subject><subject>METALLURGY</subject><subject>PHYSICS</subject><subject>PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITHDEFINED STRUCTURE</subject><subject>REFINING BY ZONE-MELTING OF MATERIAL</subject><subject>SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITHDEFINED STRUCTURE</subject><subject>SINGLE-CRYSTAL-GROWTH</subject><subject>TESTING</subject><subject>UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL ORUNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2017</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjUEKwjAQRbtxIeod5gAKFkXcjunUBpJMmCRgV1IkrkQLeiXvqYWCW1d_8f97f1q8LcWGK-AavJBH0e4IAa03BDULKGlDRAMhSlIxCQE6NG3QYQk_tKJIYrUbYDwENikSKHa1PibBqNkNK9Vo-aoUW8_JVcuvqgLPpnVJGUIZhGNv6ASWHY_382Jy7W7PvBhzVkBNUTWr3D_O-dl3l3zPrzP5TVnud-Uat5s_Jh-boUZv</recordid><startdate>20171004</startdate><enddate>20171004</enddate><creator>FUJITA Makoto</creator><creator>ARAI Tatsuhiko</creator><creator>INOKUMA Yasuhide</creator><scope>EVB</scope></search><sort><creationdate>20171004</creationdate><title>METHOD OF PREPARING SAMPLE FOR CRYSTAL STRUCTURE ANALYSIS, METHOD OF DETERMINING ABSOLUTE CONFIGURATION OF CHIRAL COMPOUND, AND POLYNUCLEAR METAL COMPLEX MONOCRYSTAL</title><author>FUJITA Makoto ; 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a method for determining an absolute configuration of a chiral compound, wherein a crystal structure analysis sample obtained by the aforementioned method is used; and a single crystal of a polynuclear metal complex suitable for used the method for preparing a sample for crystal structure analysis.</abstract><oa>free_for_read</oa></addata></record> |
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language | eng ; fre ; ger |
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subjects | AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUSPOLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE APPARATUS THEREFOR CHEMISTRY CRYSTAL GROWTH INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MEASURING METALLURGY PHYSICS PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITHDEFINED STRUCTURE REFINING BY ZONE-MELTING OF MATERIAL SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITHDEFINED STRUCTURE SINGLE-CRYSTAL-GROWTH TESTING UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL ORUNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL |
title | METHOD OF PREPARING SAMPLE FOR CRYSTAL STRUCTURE ANALYSIS, METHOD OF DETERMINING ABSOLUTE CONFIGURATION OF CHIRAL COMPOUND, AND POLYNUCLEAR METAL COMPLEX MONOCRYSTAL |
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