METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHOLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA, AND WATER BY MEANS OF DISTILLATION
Process for the continuous fractional distillation of mixtures including morpholine (MO), monoaminodiglycol (ADG), ammonia and water obtained by reaction of diethylene glycol (DEG) with ammonia, which includes separating off ammonia at the top of a first distillation column K10, feeding the bottoms...
Gespeichert in:
| Hauptverfasser: | , , , , , , , |
|---|---|
| Format: | Patent |
| Sprache: | eng ; fre ; ger |
| Schlagworte: | |
| Online-Zugang: | Volltext bestellen |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | |
| container_start_page | |
| container_title | |
| container_volume | |
| creator | BUSSMANN OLIVER SCHMIDTKE HELMUT RUDLOFF MARTIN RHEUDE UDO HENKES ERHARD LEYK UWE JULIUS MANFRED VERSCH RALPH |
| description | Process for the continuous fractional distillation of mixtures including morpholine (MO), monoaminodiglycol (ADG), ammonia and water obtained by reaction of diethylene glycol (DEG) with ammonia, which includes separating off ammonia at the top of a first distillation column K10, feeding the bottoms from K10 to a second distillation column K20 in which water and organic products are separated off at the top at a temperature at the top in the range from 45 to 198° C. and a pressure in the range from 0.1 to 15 bar, feeding the bottoms from K20 to a third distillation column K30 in which MO and organic products having a boiling point of 190° C. (1.013 bar) are separated off at the bottom, feeding the MO including stream which is separated off at the top or at a side offtake of the column K30 to a fourth column K40 in which organic products having a boiling point of 128° C. (1.013 bar) are separated off at the top and MO and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom and the bottoms from K40 are fed to a fifth distillation column K55 in which MO is separated off at the top and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom. |
| format | Patent |
| fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_EP2079718B1</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>EP2079718B1</sourcerecordid><originalsourceid>FETCH-epo_espacenet_EP2079718B13</originalsourceid><addsrcrecordid>eNqNjc0KwjAQhHvxIOo77FFBwZ-DekybbbuQ7JYkRT1JkXgSFfRFfGOj-ACeZphvmOlnL4uhFg2lOAg1QiEciFtpPXhslFOBhEFKsLQPrUOfGrZx5IkrsOKaWgwxwtjKZJoCFmWJRVNlDoUYGCtdJaBsQqSSYQ07FdBBfgCLiv1nXJMPZMz3bJj1zt3lEUc_HWRQYijqWbzfjvFx707xGp9HbJbz9Xa92OSL1R-VNwAZQCg</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHOLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA, AND WATER BY MEANS OF DISTILLATION</title><source>esp@cenet</source><creator>BUSSMANN OLIVER ; SCHMIDTKE HELMUT ; RUDLOFF MARTIN ; RHEUDE UDO ; HENKES ERHARD ; LEYK UWE ; JULIUS MANFRED ; VERSCH RALPH</creator><creatorcontrib>BUSSMANN OLIVER ; SCHMIDTKE HELMUT ; RUDLOFF MARTIN ; RHEUDE UDO ; HENKES ERHARD ; LEYK UWE ; JULIUS MANFRED ; VERSCH RALPH</creatorcontrib><description>Process for the continuous fractional distillation of mixtures including morpholine (MO), monoaminodiglycol (ADG), ammonia and water obtained by reaction of diethylene glycol (DEG) with ammonia, which includes separating off ammonia at the top of a first distillation column K10, feeding the bottoms from K10 to a second distillation column K20 in which water and organic products are separated off at the top at a temperature at the top in the range from 45 to 198° C. and a pressure in the range from 0.1 to 15 bar, feeding the bottoms from K20 to a third distillation column K30 in which MO and organic products having a boiling point of <140° C. (1.013 bar) are separated off at the top or at a side offtake and ADG and organic products having a boiling point of >190° C. (1.013 bar) are separated off at the bottom, feeding the MO including stream which is separated off at the top or at a side offtake of the column K30 to a fourth column K40 in which organic products having a boiling point of 128° C. (1.013 bar) are separated off at the top and MO and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom and the bottoms from K40 are fed to a fifth distillation column K55 in which MO is separated off at the top and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom.</description><language>eng ; fre ; ger</language><subject>CHEMISTRY ; HETEROCYCLIC COMPOUNDS ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>2010</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20100407&DB=EPODOC&CC=EP&NR=2079718B1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76294</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20100407&DB=EPODOC&CC=EP&NR=2079718B1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>BUSSMANN OLIVER</creatorcontrib><creatorcontrib>SCHMIDTKE HELMUT</creatorcontrib><creatorcontrib>RUDLOFF MARTIN</creatorcontrib><creatorcontrib>RHEUDE UDO</creatorcontrib><creatorcontrib>HENKES ERHARD</creatorcontrib><creatorcontrib>LEYK UWE</creatorcontrib><creatorcontrib>JULIUS MANFRED</creatorcontrib><creatorcontrib>VERSCH RALPH</creatorcontrib><title>METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHOLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA, AND WATER BY MEANS OF DISTILLATION</title><description>Process for the continuous fractional distillation of mixtures including morpholine (MO), monoaminodiglycol (ADG), ammonia and water obtained by reaction of diethylene glycol (DEG) with ammonia, which includes separating off ammonia at the top of a first distillation column K10, feeding the bottoms from K10 to a second distillation column K20 in which water and organic products are separated off at the top at a temperature at the top in the range from 45 to 198° C. and a pressure in the range from 0.1 to 15 bar, feeding the bottoms from K20 to a third distillation column K30 in which MO and organic products having a boiling point of <140° C. (1.013 bar) are separated off at the top or at a side offtake and ADG and organic products having a boiling point of >190° C. (1.013 bar) are separated off at the bottom, feeding the MO including stream which is separated off at the top or at a side offtake of the column K30 to a fourth column K40 in which organic products having a boiling point of 128° C. (1.013 bar) are separated off at the top and MO and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom and the bottoms from K40 are fed to a fifth distillation column K55 in which MO is separated off at the top and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom.</description><subject>CHEMISTRY</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2010</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNqNjc0KwjAQhHvxIOo77FFBwZ-DekybbbuQ7JYkRT1JkXgSFfRFfGOj-ACeZphvmOlnL4uhFg2lOAg1QiEciFtpPXhslFOBhEFKsLQPrUOfGrZx5IkrsOKaWgwxwtjKZJoCFmWJRVNlDoUYGCtdJaBsQqSSYQ07FdBBfgCLiv1nXJMPZMz3bJj1zt3lEUc_HWRQYijqWbzfjvFx707xGp9HbJbz9Xa92OSL1R-VNwAZQCg</recordid><startdate>20100407</startdate><enddate>20100407</enddate><creator>BUSSMANN OLIVER</creator><creator>SCHMIDTKE HELMUT</creator><creator>RUDLOFF MARTIN</creator><creator>RHEUDE UDO</creator><creator>HENKES ERHARD</creator><creator>LEYK UWE</creator><creator>JULIUS MANFRED</creator><creator>VERSCH RALPH</creator><scope>EVB</scope></search><sort><creationdate>20100407</creationdate><title>METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHOLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA, AND WATER BY MEANS OF DISTILLATION</title><author>BUSSMANN OLIVER ; SCHMIDTKE HELMUT ; RUDLOFF MARTIN ; RHEUDE UDO ; HENKES ERHARD ; LEYK UWE ; JULIUS MANFRED ; VERSCH RALPH</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_EP2079718B13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; fre ; ger</language><creationdate>2010</creationdate><topic>CHEMISTRY</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>BUSSMANN OLIVER</creatorcontrib><creatorcontrib>SCHMIDTKE HELMUT</creatorcontrib><creatorcontrib>RUDLOFF MARTIN</creatorcontrib><creatorcontrib>RHEUDE UDO</creatorcontrib><creatorcontrib>HENKES ERHARD</creatorcontrib><creatorcontrib>LEYK UWE</creatorcontrib><creatorcontrib>JULIUS MANFRED</creatorcontrib><creatorcontrib>VERSCH RALPH</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>BUSSMANN OLIVER</au><au>SCHMIDTKE HELMUT</au><au>RUDLOFF MARTIN</au><au>RHEUDE UDO</au><au>HENKES ERHARD</au><au>LEYK UWE</au><au>JULIUS MANFRED</au><au>VERSCH RALPH</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHOLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA, AND WATER BY MEANS OF DISTILLATION</title><date>2010-04-07</date><risdate>2010</risdate><abstract>Process for the continuous fractional distillation of mixtures including morpholine (MO), monoaminodiglycol (ADG), ammonia and water obtained by reaction of diethylene glycol (DEG) with ammonia, which includes separating off ammonia at the top of a first distillation column K10, feeding the bottoms from K10 to a second distillation column K20 in which water and organic products are separated off at the top at a temperature at the top in the range from 45 to 198° C. and a pressure in the range from 0.1 to 15 bar, feeding the bottoms from K20 to a third distillation column K30 in which MO and organic products having a boiling point of <140° C. (1.013 bar) are separated off at the top or at a side offtake and ADG and organic products having a boiling point of >190° C. (1.013 bar) are separated off at the bottom, feeding the MO including stream which is separated off at the top or at a side offtake of the column K30 to a fourth column K40 in which organic products having a boiling point of 128° C. (1.013 bar) are separated off at the top and MO and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom and the bottoms from K40 are fed to a fifth distillation column K55 in which MO is separated off at the top and organic products having a boiling point of 128° C. (1.013 bar) are separated off at the bottom.</abstract><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext_linktorsrc |
| identifier | |
| ispartof | |
| issn | |
| language | eng ; fre ; ger |
| recordid | cdi_epo_espacenet_EP2079718B1 |
| source | esp@cenet |
| subjects | CHEMISTRY HETEROCYCLIC COMPOUNDS METALLURGY ORGANIC CHEMISTRY |
| title | METHOD FOR THE CONTINUOUS SEPARATION OF MIXTURES COMPRISING MORPHOLINE (MO), MONOAMINODIGLYCOL (ADG), AMMONIA, AND WATER BY MEANS OF DISTILLATION |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-22T15%3A10%3A54IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=BUSSMANN%20OLIVER&rft.date=2010-04-07&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3EEP2079718B1%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |