PREPARATION OF STABLE SILVER COLLOIDS

A method is described for producing highly stable silver colloidal solutions by reducing silver nitrate with lithium citrate. In the method, the main steps consist of: (a) heating a first quantity of water to a first predetermined temperature; (b) adding a second quantity of silver nitrate to the wa...

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Hauptverfasser: WHITE, PETER, CYRIL, HJORTKJAER, JAKOB, HOWIE
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HJORTKJAER, JAKOB, HOWIE
description A method is described for producing highly stable silver colloidal solutions by reducing silver nitrate with lithium citrate. In the method, the main steps consist of: (a) heating a first quantity of water to a first predetermined temperature; (b) adding a second quantity of silver nitrate to the water; (c) heating the mixture to a second predetermined temperature; (d) adding a third quantity of an aqueous lithium citrate solution to the mixture; (e) maintaining the mixture at the second predetermined temperature for a predetermined time; and (f) cooling the mixture. The mixing process is accompanied by constant stirring. The colloid exhibits high light-scattering properties and intense SERS or SERRS spectra with low background fluorescence levels and a long shelf life, making it particularly suitable for Raman spectroscopy.
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In the method, the main steps consist of: (a) heating a first quantity of water to a first predetermined temperature; (b) adding a second quantity of silver nitrate to the water; (c) heating the mixture to a second predetermined temperature; (d) adding a third quantity of an aqueous lithium citrate solution to the mixture; (e) maintaining the mixture at the second predetermined temperature for a predetermined time; and (f) cooling the mixture. The mixing process is accompanied by constant stirring. 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subjects CASTING
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
FERROUS OR NON-FERROUS ALLOYS
MAKING METALLIC POWDER
MANUFACTURE OF ARTICLES FROM METALLIC POWDER
METALLURGY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
POWDER METALLURGY
PRETREATMENT OF RAW MATERIALS
PRODUCTION AND REFINING OF METALS
THEIR RELEVANT APPARATUS
TRANSPORTING
TREATMENT OF ALLOYS OR NON-FERROUS METALS
WORKING METALLIC POWDER
title PREPARATION OF STABLE SILVER COLLOIDS
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