Process for producing powdery water soluble cellulose derivatives

Process for production of water-soluble cellulose derivatives (I) in the form of powder involves: (a) swelling or dissolving (I) in 50-80 wt% water (based on total weight); (b) converting the solution or gel into finely-divided solid particles by vaporising the water in a high-speed rotary impact mi...

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Hauptverfasser: KIESEWETTER, RENÉ, WEBER, GUNTER, SCHLESIGER, HARTWIG, MORNING, MARTIN, LELGEMANN, RUDOLF
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creator KIESEWETTER, RENÉ
WEBER, GUNTER
SCHLESIGER, HARTWIG
MORNING, MARTIN
LELGEMANN, RUDOLF
description Process for production of water-soluble cellulose derivatives (I) in the form of powder involves: (a) swelling or dissolving (I) in 50-80 wt% water (based on total weight); (b) converting the solution or gel into finely-divided solid particles by vaporising the water in a high-speed rotary impact mill with the aid of a heat transfer/carrier gas; (c) separating the particles from the gas; and (d) optionally, drying. Independent claims are also included for: (i) powdered (I) obtained by this process, comprising less than 5 wt% with a particle size (PD) of less than 15 microns, less than 2 wt% with a PD below 10 microns and less than 1 wt% below 5 microns; (ii) powder (I) with less than 20 wt% below 15 microns, less than 10 wt% below 10 microns and less than 2 wt% below 5 microns; (iii) powder (I) with six different particle size distributions (A-F) as obtained by sieve analysis, e.g. distribution A with 98.5-100 wt% below 0.25 mm (cumulative through fraction), 95-100 wt% below 0.2 mm, 89-98 wt% below 0.16 mm, 79-92 wt% below 0.125 mm, 65-80 wt% below 0.1 mm and 35-45 wt% below 0.063 mm.
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subjects AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F,C08G
CHEMISTRY
COMPOSITIONS BASED THEREON
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
DERIVATIVES THEREOF
GENERAL PROCESSES OF COMPOUNDING
METALLURGY
ORGANIC MACROMOLECULAR COMPOUNDS
POLYSACCHARIDES
THEIR PREPARATION OR CHEMICAL WORKING-UP
WORKING-UP
title Process for producing powdery water soluble cellulose derivatives
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