PROCESS FOR PURIFYING PHENOL

A process for improving the quality of phenol which comprises (a) introducing a liquid phenol composition comprising above about 95 weight percent phenol on a dry basis, organic acid contaminants, and organic ketone contaminants; (b) introducing water into the distillation tower, together with the p...

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1. Verfasser: FULMER, JOHN WILLIAM
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description A process for improving the quality of phenol which comprises (a) introducing a liquid phenol composition comprising above about 95 weight percent phenol on a dry basis, organic acid contaminants, and organic ketone contaminants; (b) introducing water into the distillation tower, together with the phenol stream or in a separate stream; (c) heating the phenol composition and water to a temperature sufficiently high to vaporize the water; (d) allowing the organic acid contaminant to build to a concentration whereby sufficient acid is present to catalyze a reaction between an organic ketone contaminant and phenol, thereby forming a new compound(s) and; (e) removing the said formed compound(s) from the distillation tower by hydroextractive steam distillation. f
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(c) heating the phenol composition and water to a temperature sufficiently high to vaporize the water; (d) allowing the organic acid contaminant to build to a concentration whereby sufficient acid is present to catalyze a reaction between an organic ketone contaminant and phenol, thereby forming a new compound(s) and; (e) removing the said formed compound(s) from the distillation tower by hydroextractive steam distillation. f</description><edition>4</edition><language>eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>1989</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=19891018&amp;DB=EPODOC&amp;CC=EP&amp;NR=0299239A3$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=19891018&amp;DB=EPODOC&amp;CC=EP&amp;NR=0299239A3$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>FULMER, JOHN WILLIAM</creatorcontrib><title>PROCESS FOR PURIFYING PHENOL</title><description>A process for improving the quality of phenol which comprises (a) introducing a liquid phenol composition comprising above about 95 weight percent phenol on a dry basis, organic acid contaminants, and organic ketone contaminants; (b) introducing water into the distillation tower, together with the phenol stream or in a separate stream; (c) heating the phenol composition and water to a temperature sufficiently high to vaporize the water; (d) allowing the organic acid contaminant to build to a concentration whereby sufficient acid is present to catalyze a reaction between an organic ketone contaminant and phenol, thereby forming a new compound(s) and; (e) removing the said formed compound(s) from the distillation tower by hydroextractive steam distillation. f</description><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS</subject><subject>CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>1989</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZJAJCPJ3dg0OVnDzD1IICA3ydIv09HNXCPBw9fP34WFgTUvMKU7lhdLcDApuriHOHrqpBfnxqcUFicmpeakl8a4BBkaWlkbGlo7GxkQoAQBDkSCc</recordid><startdate>19891018</startdate><enddate>19891018</enddate><creator>FULMER, JOHN WILLIAM</creator><scope>EVB</scope></search><sort><creationdate>19891018</creationdate><title>PROCESS FOR PURIFYING PHENOL</title><author>FULMER, JOHN WILLIAM</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_EP0299239A33</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng</language><creationdate>1989</creationdate><topic>ACYCLIC OR CARBOCYCLIC COMPOUNDS</topic><topic>CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>FULMER, JOHN WILLIAM</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>FULMER, JOHN WILLIAM</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS FOR PURIFYING PHENOL</title><date>1989-10-18</date><risdate>1989</risdate><abstract>A process for improving the quality of phenol which comprises (a) introducing a liquid phenol composition comprising above about 95 weight percent phenol on a dry basis, organic acid contaminants, and organic ketone contaminants; (b) introducing water into the distillation tower, together with the phenol stream or in a separate stream; (c) heating the phenol composition and water to a temperature sufficiently high to vaporize the water; (d) allowing the organic acid contaminant to build to a concentration whereby sufficient acid is present to catalyze a reaction between an organic ketone contaminant and phenol, thereby forming a new compound(s) and; (e) removing the said formed compound(s) from the distillation tower by hydroextractive steam distillation. f</abstract><edition>4</edition><oa>free_for_read</oa></addata></record>
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title PROCESS FOR PURIFYING PHENOL
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