PROCESS AND DEVICE FOR THE CONTINUOUS PRODUCTION OF ALKOXYPOLYSILOXANES
A continuous process for the preparation of alkoxypolysiloxane in which silane or a silane mixture and a mixture of hydrogen chloride-containing alcohol and water is fed continuously into the lower region of preferably cylindrical stirred reactor, the reaction product formed together with excess hyd...
Gespeichert in:
| Hauptverfasser: | , , , , , , , , |
|---|---|
| Format: | Patent |
| Sprache: | eng ; ger |
| Schlagworte: | |
| Online-Zugang: | Volltext bestellen |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | |
| container_start_page | |
| container_title | |
| container_volume | |
| creator | RAU, HARALD SCHAMBERG, ECKEHARD KOERNER, GOETZ PATZKE, HANS-JUERGEN GIESING, HERBERT KROPAC, VACLAV SPIEKER, FRITZ WEITEMEYER, CHRISTIAN QUILITSCH, HERBERT |
| description | A continuous process for the preparation of alkoxypolysiloxane in which silane or a silane mixture and a mixture of hydrogen chloride-containing alcohol and water is fed continuously into the lower region of preferably cylindrical stirred reactor, the reaction product formed together with excess hydrogen chloride-containing alcohol is drawn off continuously after residence time of 30 to 180 minutes at the upper end of the reactor and the undissolved, gaseous portion of hydrogen chloride is carried off at the head of the reactor, the temperature of the reaction mixture or the reaction product, as it flows through the reactor, being raised from a range of -17 DEG to +30 DEG C. to range of +30 DEG to +80 DEG C., the temperature gradient having to be at least 10 DEG C., and the excess alcohol and dissolved hydrogen chloride being removed outside of the reactor in a known manner from the reaction product formed, and the hydrogen chloride-containing alcohol obtained while working up to reaction product being recycled to the reactor. The invention furthermore relates to an apparatus which is particularly suitable for implementing the process. |
| format | Patent |
| fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_EP0167924B1</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>EP0167924B1</sourcerecordid><originalsourceid>FETCH-epo_espacenet_EP0167924B13</originalsourceid><addsrcrecordid>eNrjZHAPCPJ3dg0OVnD0c1FwcQ3zdHZVcPMPUgjxcFVw9vcL8fQL9Q8NVgCqcgl1DvH091Pwd1Nw9PH2j4gM8PeJDPb08Y9w9HMN5mFgTUvMKU7lhdLcDApuriHOHrqpBfnxqcUFicmpeakl8a4BBoZm5pZGJk6GxkQoAQC3GyzB</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>PROCESS AND DEVICE FOR THE CONTINUOUS PRODUCTION OF ALKOXYPOLYSILOXANES</title><source>esp@cenet</source><creator>RAU, HARALD ; SCHAMBERG, ECKEHARD ; KOERNER, GOETZ ; PATZKE, HANS-JUERGEN ; GIESING, HERBERT ; KROPAC, VACLAV ; SPIEKER, FRITZ ; WEITEMEYER, CHRISTIAN ; QUILITSCH, HERBERT</creator><creatorcontrib>RAU, HARALD ; SCHAMBERG, ECKEHARD ; KOERNER, GOETZ ; PATZKE, HANS-JUERGEN ; GIESING, HERBERT ; KROPAC, VACLAV ; SPIEKER, FRITZ ; WEITEMEYER, CHRISTIAN ; QUILITSCH, HERBERT</creatorcontrib><description>A continuous process for the preparation of alkoxypolysiloxane in which silane or a silane mixture and a mixture of hydrogen chloride-containing alcohol and water is fed continuously into the lower region of preferably cylindrical stirred reactor, the reaction product formed together with excess hydrogen chloride-containing alcohol is drawn off continuously after residence time of 30 to 180 minutes at the upper end of the reactor and the undissolved, gaseous portion of hydrogen chloride is carried off at the head of the reactor, the temperature of the reaction mixture or the reaction product, as it flows through the reactor, being raised from a range of -17 DEG to +30 DEG C. to range of +30 DEG to +80 DEG C., the temperature gradient having to be at least 10 DEG C., and the excess alcohol and dissolved hydrogen chloride being removed outside of the reactor in a known manner from the reaction product formed, and the hydrogen chloride-containing alcohol obtained while working up to reaction product being recycled to the reactor. The invention furthermore relates to an apparatus which is particularly suitable for implementing the process.</description><language>eng ; ger</language><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY ; CHEMISTRY ; COMPOSITIONS BASED THEREON ; MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS ; METALLURGY ; ORGANIC MACROMOLECULAR COMPOUNDS ; PERFORMING OPERATIONS ; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL ; THEIR PREPARATION OR CHEMICAL WORKING-UP ; THEIR RELEVANT APPARATUS ; TRANSPORTING</subject><creationdate>1990</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19900912&DB=EPODOC&CC=EP&NR=0167924B1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19900912&DB=EPODOC&CC=EP&NR=0167924B1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>RAU, HARALD</creatorcontrib><creatorcontrib>SCHAMBERG, ECKEHARD</creatorcontrib><creatorcontrib>KOERNER, GOETZ</creatorcontrib><creatorcontrib>PATZKE, HANS-JUERGEN</creatorcontrib><creatorcontrib>GIESING, HERBERT</creatorcontrib><creatorcontrib>KROPAC, VACLAV</creatorcontrib><creatorcontrib>SPIEKER, FRITZ</creatorcontrib><creatorcontrib>WEITEMEYER, CHRISTIAN</creatorcontrib><creatorcontrib>QUILITSCH, HERBERT</creatorcontrib><title>PROCESS AND DEVICE FOR THE CONTINUOUS PRODUCTION OF ALKOXYPOLYSILOXANES</title><description>A continuous process for the preparation of alkoxypolysiloxane in which silane or a silane mixture and a mixture of hydrogen chloride-containing alcohol and water is fed continuously into the lower region of preferably cylindrical stirred reactor, the reaction product formed together with excess hydrogen chloride-containing alcohol is drawn off continuously after residence time of 30 to 180 minutes at the upper end of the reactor and the undissolved, gaseous portion of hydrogen chloride is carried off at the head of the reactor, the temperature of the reaction mixture or the reaction product, as it flows through the reactor, being raised from a range of -17 DEG to +30 DEG C. to range of +30 DEG to +80 DEG C., the temperature gradient having to be at least 10 DEG C., and the excess alcohol and dissolved hydrogen chloride being removed outside of the reactor in a known manner from the reaction product formed, and the hydrogen chloride-containing alcohol obtained while working up to reaction product being recycled to the reactor. The invention furthermore relates to an apparatus which is particularly suitable for implementing the process.</description><subject>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</subject><subject>CHEMISTRY</subject><subject>COMPOSITIONS BASED THEREON</subject><subject>MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS</subject><subject>METALLURGY</subject><subject>ORGANIC MACROMOLECULAR COMPOUNDS</subject><subject>PERFORMING OPERATIONS</subject><subject>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</subject><subject>THEIR PREPARATION OR CHEMICAL WORKING-UP</subject><subject>THEIR RELEVANT APPARATUS</subject><subject>TRANSPORTING</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>1990</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZHAPCPJ3dg0OVnD0c1FwcQ3zdHZVcPMPUgjxcFVw9vcL8fQL9Q8NVgCqcgl1DvH091Pwd1Nw9PH2j4gM8PeJDPb08Y9w9HMN5mFgTUvMKU7lhdLcDApuriHOHrqpBfnxqcUFicmpeakl8a4BBoZm5pZGJk6GxkQoAQC3GyzB</recordid><startdate>19900912</startdate><enddate>19900912</enddate><creator>RAU, HARALD</creator><creator>SCHAMBERG, ECKEHARD</creator><creator>KOERNER, GOETZ</creator><creator>PATZKE, HANS-JUERGEN</creator><creator>GIESING, HERBERT</creator><creator>KROPAC, VACLAV</creator><creator>SPIEKER, FRITZ</creator><creator>WEITEMEYER, CHRISTIAN</creator><creator>QUILITSCH, HERBERT</creator><scope>EVB</scope></search><sort><creationdate>19900912</creationdate><title>PROCESS AND DEVICE FOR THE CONTINUOUS PRODUCTION OF ALKOXYPOLYSILOXANES</title><author>RAU, HARALD ; SCHAMBERG, ECKEHARD ; KOERNER, GOETZ ; PATZKE, HANS-JUERGEN ; GIESING, HERBERT ; KROPAC, VACLAV ; SPIEKER, FRITZ ; WEITEMEYER, CHRISTIAN ; QUILITSCH, HERBERT</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_EP0167924B13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; ger</language><creationdate>1990</creationdate><topic>CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY</topic><topic>CHEMISTRY</topic><topic>COMPOSITIONS BASED THEREON</topic><topic>MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS</topic><topic>METALLURGY</topic><topic>ORGANIC MACROMOLECULAR COMPOUNDS</topic><topic>PERFORMING OPERATIONS</topic><topic>PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL</topic><topic>THEIR PREPARATION OR CHEMICAL WORKING-UP</topic><topic>THEIR RELEVANT APPARATUS</topic><topic>TRANSPORTING</topic><toplevel>online_resources</toplevel><creatorcontrib>RAU, HARALD</creatorcontrib><creatorcontrib>SCHAMBERG, ECKEHARD</creatorcontrib><creatorcontrib>KOERNER, GOETZ</creatorcontrib><creatorcontrib>PATZKE, HANS-JUERGEN</creatorcontrib><creatorcontrib>GIESING, HERBERT</creatorcontrib><creatorcontrib>KROPAC, VACLAV</creatorcontrib><creatorcontrib>SPIEKER, FRITZ</creatorcontrib><creatorcontrib>WEITEMEYER, CHRISTIAN</creatorcontrib><creatorcontrib>QUILITSCH, HERBERT</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>RAU, HARALD</au><au>SCHAMBERG, ECKEHARD</au><au>KOERNER, GOETZ</au><au>PATZKE, HANS-JUERGEN</au><au>GIESING, HERBERT</au><au>KROPAC, VACLAV</au><au>SPIEKER, FRITZ</au><au>WEITEMEYER, CHRISTIAN</au><au>QUILITSCH, HERBERT</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS AND DEVICE FOR THE CONTINUOUS PRODUCTION OF ALKOXYPOLYSILOXANES</title><date>1990-09-12</date><risdate>1990</risdate><abstract>A continuous process for the preparation of alkoxypolysiloxane in which silane or a silane mixture and a mixture of hydrogen chloride-containing alcohol and water is fed continuously into the lower region of preferably cylindrical stirred reactor, the reaction product formed together with excess hydrogen chloride-containing alcohol is drawn off continuously after residence time of 30 to 180 minutes at the upper end of the reactor and the undissolved, gaseous portion of hydrogen chloride is carried off at the head of the reactor, the temperature of the reaction mixture or the reaction product, as it flows through the reactor, being raised from a range of -17 DEG to +30 DEG C. to range of +30 DEG to +80 DEG C., the temperature gradient having to be at least 10 DEG C., and the excess alcohol and dissolved hydrogen chloride being removed outside of the reactor in a known manner from the reaction product formed, and the hydrogen chloride-containing alcohol obtained while working up to reaction product being recycled to the reactor. The invention furthermore relates to an apparatus which is particularly suitable for implementing the process.</abstract><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext_linktorsrc |
| identifier | |
| ispartof | |
| issn | |
| language | eng ; ger |
| recordid | cdi_epo_espacenet_EP0167924B1 |
| source | esp@cenet |
| subjects | CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY COMPOSITIONS BASED THEREON MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS METALLURGY ORGANIC MACROMOLECULAR COMPOUNDS PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL THEIR PREPARATION OR CHEMICAL WORKING-UP THEIR RELEVANT APPARATUS TRANSPORTING |
| title | PROCESS AND DEVICE FOR THE CONTINUOUS PRODUCTION OF ALKOXYPOLYSILOXANES |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-12T08%3A21%3A23IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=RAU,%20HARALD&rft.date=1990-09-12&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3EEP0167924B1%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |