PROCESS FOR THE PREPARATION OF 3-AMINO-1-HYDROXYPROPANE-1,1-DIPHOSPHONIC ACID
1. A process for the production of 3-amino-1-hydroxypropane-1,1-diphosphonic acid by reaction of beta-alanine with an oxyacid of phosphorus and a phosphorus halide, characterized in that beta-alanine is reacted with a mixture of phosphorus trichloride and anhydrous phosphoric acid at temperatures of...
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creator | BLUM, HELMUT WORMS, KARL-HEINZ |
description | 1. A process for the production of 3-amino-1-hydroxypropane-1,1-diphosphonic acid by reaction of beta-alanine with an oxyacid of phosphorus and a phosphorus halide, characterized in that beta-alanine is reacted with a mixture of phosphorus trichloride and anhydrous phosphoric acid at temperatures of from 80 to 130 degrees C and the reaction product is subsequently hydrolyzed. |
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A process for the production of 3-amino-1-hydroxypropane-1,1-diphosphonic acid by reaction of beta-alanine with an oxyacid of phosphorus and a phosphorus halide, characterized in that beta-alanine is reacted with a mixture of phosphorus trichloride and anhydrous phosphoric acid at temperatures of from 80 to 130 degrees C and the reaction product is subsequently hydrolyzed.</description><edition>4</edition><language>eng ; ger</language><subject>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM ; CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY</subject><creationdate>1986</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19860730&DB=EPODOC&CC=EP&NR=0082472B1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19860730&DB=EPODOC&CC=EP&NR=0082472B1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>BLUM, HELMUT</creatorcontrib><creatorcontrib>WORMS, KARL-HEINZ</creatorcontrib><title>PROCESS FOR THE PREPARATION OF 3-AMINO-1-HYDROXYPROPANE-1,1-DIPHOSPHONIC ACID</title><description>1. A process for the production of 3-amino-1-hydroxypropane-1,1-diphosphonic acid by reaction of beta-alanine with an oxyacid of phosphorus and a phosphorus halide, characterized in that beta-alanine is reacted with a mixture of phosphorus trichloride and anhydrous phosphoric acid at temperatures of from 80 to 130 degrees C and the reaction product is subsequently hydrolyzed.</description><subject>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM</subject><subject>CHEMISTRY</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>1986</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZPANCPJ3dg0OVnDzD1II8XBVCAhyDXAMcgzx9PdT8HdTMNZ19PX089c11PWIdAnyj4gEqg9w9HPVNdQx1HXxDPDwDwZiP09nBUdnTxceBta0xJziVF4ozc2g4OYa4uyhm1qQH59aXJCYnJqXWhLvGmBgYGFkYm7kZGhMhBIAaekteQ</recordid><startdate>19860730</startdate><enddate>19860730</enddate><creator>BLUM, HELMUT</creator><creator>WORMS, KARL-HEINZ</creator><scope>EVB</scope></search><sort><creationdate>19860730</creationdate><title>PROCESS FOR THE PREPARATION OF 3-AMINO-1-HYDROXYPROPANE-1,1-DIPHOSPHONIC ACID</title><author>BLUM, HELMUT ; WORMS, KARL-HEINZ</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_EP0082472B13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; ger</language><creationdate>1986</creationdate><topic>ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM</topic><topic>CHEMISTRY</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><toplevel>online_resources</toplevel><creatorcontrib>BLUM, HELMUT</creatorcontrib><creatorcontrib>WORMS, KARL-HEINZ</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>BLUM, HELMUT</au><au>WORMS, KARL-HEINZ</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>PROCESS FOR THE PREPARATION OF 3-AMINO-1-HYDROXYPROPANE-1,1-DIPHOSPHONIC ACID</title><date>1986-07-30</date><risdate>1986</risdate><abstract>1. A process for the production of 3-amino-1-hydroxypropane-1,1-diphosphonic acid by reaction of beta-alanine with an oxyacid of phosphorus and a phosphorus halide, characterized in that beta-alanine is reacted with a mixture of phosphorus trichloride and anhydrous phosphoric acid at temperatures of from 80 to 130 degrees C and the reaction product is subsequently hydrolyzed.</abstract><edition>4</edition><oa>free_for_read</oa></addata></record> |
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subjects | ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM CHEMISTRY METALLURGY ORGANIC CHEMISTRY |
title | PROCESS FOR THE PREPARATION OF 3-AMINO-1-HYDROXYPROPANE-1,1-DIPHOSPHONIC ACID |
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