Process for preparing acicular iron oxide particles
This disclosure relates to a process for preparing acicular magnetic iron oxide particles by (a) adding an aqueous solution of a ferrous salt to an aqueous solution of a stoichiometric excess of alkaline hydroxide while substantially avoiding local excesses of the ferrous salt, to form an aqueous di...
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creator | PINGAUD, BERNARD JEAN |
description | This disclosure relates to a process for preparing acicular magnetic iron oxide particles by (a) adding an aqueous solution of a ferrous salt to an aqueous solution of a stoichiometric excess of alkaline hydroxide while substantially avoiding local excesses of the ferrous salt, to form an aqueous dispersion of ferrous hydroxide particles, (b) oxidizing these particles to form non-magnetic alpha ferric oxide hydrate particles, and (c) converting the non-magnetic particles to magnetic iron oxide particles by dehydration and reduction or dehydration, reduction and oxidation. The ferrous salt solution is subjected to reducing conditions prior to and/or during the addition to the alkaline hydroxide solution to reduce contaminating ferric ions that are normally present to ferrous ions. |
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The ferrous salt solution is subjected to reducing conditions prior to and/or during the addition to the alkaline hydroxide solution to reduce contaminating ferric ions that are normally present to ferrous ions.</description><language>eng ; fre ; ger</language><subject>BASIC ELECTRIC ELEMENTS ; CHEMISTRY ; COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F ; ELECTRICITY ; INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OFSOLID INORGANIC COMPOUNDS ; INDUCTANCES ; INFORMATION STORAGE ; INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORDCARRIER AND TRANSDUCER ; INORGANIC CHEMISTRY ; MAGNETS ; METALLURGY ; PHYSICS ; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES ; TRANSFORMERS</subject><creationdate>1982</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19820203&DB=EPODOC&CC=EP&NR=0045246A1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76290</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=19820203&DB=EPODOC&CC=EP&NR=0045246A1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>PINGAUD, BERNARD JEAN</creatorcontrib><title>Process for preparing acicular iron oxide particles</title><description>This disclosure relates to a process for preparing acicular magnetic iron oxide particles by (a) adding an aqueous solution of a ferrous salt to an aqueous solution of a stoichiometric excess of alkaline hydroxide while substantially avoiding local excesses of the ferrous salt, to form an aqueous dispersion of ferrous hydroxide particles, (b) oxidizing these particles to form non-magnetic alpha ferric oxide hydrate particles, and (c) converting the non-magnetic particles to magnetic iron oxide particles by dehydration and reduction or dehydration, reduction and oxidation. 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The ferrous salt solution is subjected to reducing conditions prior to and/or during the addition to the alkaline hydroxide solution to reduce contaminating ferric ions that are normally present to ferrous ions.</abstract><oa>free_for_read</oa></addata></record> |
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language | eng ; fre ; ger |
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subjects | BASIC ELECTRIC ELEMENTS CHEMISTRY COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F ELECTRICITY INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OFSOLID INORGANIC COMPOUNDS INDUCTANCES INFORMATION STORAGE INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORDCARRIER AND TRANSDUCER INORGANIC CHEMISTRY MAGNETS METALLURGY PHYSICS SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES TRANSFORMERS |
title | Process for preparing acicular iron oxide particles |
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