VERFAHREN ZUR REINIGUNG VON AROMATISCHEN BICARBONSÄUREN

Disclosed is a process for the purification of aromatic dicarboxylic acids in which the salt of an aliphatic diamine and an aromatic dicarboxylic acid is formed in an aqueous solvent, recrystallized, and contacted with an aliphatic dicarboxylic acid in an aqueous solvent such that the aromatic dicar...

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Hauptverfasser: SAMUELS, MICHAEL, ALMS, GREGORY
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ALMS, GREGORY
description Disclosed is a process for the purification of aromatic dicarboxylic acids in which the salt of an aliphatic diamine and an aromatic dicarboxylic acid is formed in an aqueous solvent, recrystallized, and contacted with an aliphatic dicarboxylic acid in an aqueous solvent such that the aromatic dicarboxylic acid is recoverable in the form of a purified precipitate. The remaining aqueous solute is a salt of the aliphatic diamine and aliphatic dicarboxylic acid and can be used as a starting material in the manufacture of certain polyamides (nylons). The invention is particularly applicable for purifying 2,6-naphthalene dicarboxylic acid, which is difficult otherwise to purify.
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The remaining aqueous solute is a salt of the aliphatic diamine and aliphatic dicarboxylic acid and can be used as a starting material in the manufacture of certain polyamides (nylons). 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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title VERFAHREN ZUR REINIGUNG VON AROMATISCHEN BICARBONSÄUREN
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