VERFAHREN ZUR HERSTELLUNG VON ANISOTROPEN KOHLENSTOFFASERN
The method for producing anisotropic carbon fibres from carbon-containing isotropic pitch comprises the following steps: a) an isotropic pitch of a size smaller than 0.1mm is released from unmeltable components at a temperature comprised between 150C and 350C, b) the pitch purified with a mononuclea...
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Zusammenfassung: | The method for producing anisotropic carbon fibres from carbon-containing isotropic pitch comprises the following steps: a) an isotropic pitch of a size smaller than 0.1mm is released from unmeltable components at a temperature comprised between 150C and 350C, b) the pitch purified with a mononuclear organic solvent amount equal to 4-6 parts by weight of solvent for one part by weight of pitch filtrate is extracted at a temperature comprised between 70 and 90C, c) the extraction residue is dried before its transformation into mesophase pitch, it is heat-treated during a period from 1 to 5 hours at a temperature comprised between 340C and 410C, and the mesophase pitch obtained is woven into fibres, d) the extraction residue is mixed before its heat treatment with 1-15% by weight of purified solvent extract by suction into a water jet. A mixture is obtained wherein the toluene soluble part is 20-40% by weight of the mixture. |
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